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General procedures
Recovery of liquid in sample cell to Vessel
Off/Run switch Turbo control panel
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Muon Liquid Handling System
User Guide
C. Johnson, S.P. Cottrell et al
Version 0.2
- 1 -
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Contents
Muon Liquid Handling System User Guide
C. Johnson, S.P. Cottrell et al Version
Contents
1.1 Layout of the liquid handling system
1 Getting Started
1.3 Layout of the pump
1.2 Layout of the in situ sample stick
Roughing/ Turbo switch Pressure reading Turbo
Off/Run switch Turbo control panel
Pump Rotary Pump
system
2.1 Sample loading
2 General procedures
2.2 Evacuation of the system
2.2.2 Removing air from Vessel
2.2.1 Removing air from Vessel
2.2.3 Removing air from Vessel
2.2.4 Evacuation of the sample cell
2.3 Freeze-Pump-Thawcycle
2.4Liquid transfers
Switch the pump to its roughing mode
2.4.5 Recovery of liquid in sample cell to Vessel
2.4.4 Recovery of liquid in sample cell to Vessel
2.4.6 Recovery of liquid in sample cell to Vessel
All the liquid may not return in a single pass and repeating the evacuation procedure may be required. However, some liquid may be present in the system and care should be taken during evacuation that the trap does not become blocked. The liquid may also be encouraged to leave the sample cell by using a small amount of gas
3 Example Experiment