Agilent Technologies 1100 Series manual Purge Valve Assembly, Purge-Valve Assembly

Page 177

Parts and Materials

Purge Valve Assembly

Purge Valve Assembly

Table 23

Purge-Valve Assembly

 

 

 

 

 

 

 

 

Item

Description

Part Number

 

 

 

 

 

 

 

 

Purge valve — complete assembly

G1311-60009

 

1

Valve body

No part number

 

2

PTFE frit (pack of 5)

01018-22707

 

3

Gold seal

5001-3707

 

4

Cap (pack of 4)

5062-2485

 

 

 

 

Figure 38

Purge-Valve Assembly

 

1

2

3

4

177

Page 176 Page 178
Image 177
Page 176 Page 178
Contents Reference Manual Warranty Agilent 1100 Series Quaternary Pump This Book Status Indicators Installing the PumpError Messages Leak Test Pressure TestOverview of Main Assemblies Exchanging Internal Parts 127Introduction to the Quaternary Pump Cable Overview 181Control Module Screens for the Quaternary Pump Contents Contents Installing the Pump Power Consideration Power CordsSite Requirements Environment Bench SpacePhysical Specifications Type Comments Quaternary Pump Checklist Description Quantity Delivery ChecklistUnpacking the Quaternary Pump Damaged PackagingAccessory Kit Contents Quaternary Pump Accessory Kit Contents-Vacuum Degasser Recommended Stack Configuration Front View Optimizing the Stack ConfigurationStack containing the autosampler Installing the Quaternary Pump PreparationsParts required Rear of Quaternary Pump Front panel is turned off Settings, see Setting the 8-bit Configuration Switch onTwo wrenches 1/4-5/16 inch for capillary connections Flow Connections of the Quaternary PumpToxic or hazardous solvents are used Removing the Front CoverFlow Connections of the Quaternary Pump Mcgv Priming and Purging the System Priming with the Pump Activity Solvent Comments Optimizing Performance Hints for Successful Use of the Quaternary Pump Procedure on Solvent Information Cleaning the Solvent Filters Prevent Blocking of Solvent FiltersChecking the Solvent Filters Operational Hints for the Vacuum Degasser Operational Hints for the Vacuum DegasserOperational Hints for the Multi Channel Gradient Valve Mcgv When to use the Continuous Seal Wash Option When to Use Alternative Seals Optimize the Compressibility Compensation SettingSolvent pure Compressibility 10-6/bar Optimize the Compressibility Compensation Setting Troubleshooting and Test Functions Troubleshooting and Test Functions Location of Status Indicators Status IndicatorsPump Status Indicator Power Supply IndicatorError Messages Timeout Shut-Down Remote Timeout Synchronization Lost Leak Leak sensor in the quaternary pump has failed open circuit Leak Sensor OpenLeak sensor in the quaternary pump has failed short circuit Leak Sensor ShortCompensation Sensor Open Compensation Sensor Short Fan Failed Open Cover Replace the top cover and foam Restart Without CoverZero Solvent Counter Pressure Above Upper Limit Pressure Below Lower Limit Pressure Signal Missing Missing Pressure Reading Pump Configuration Valve Fuse Inlet-Valve Fuse Valve 0 Failed valve a Valve FailedMotor-Drive Power Encoder Missing Inlet-Valve Missing Temperature Out of Range Temperature Limit Exceeded Position for restarting Servo Restart FailedBroken plunger Pump Head MissingIndex Limit Index Adjustment Index Missing Stroke Length Initialization Failed Wait Timeout Description Pressure TestPressure Test Positioning the blank nutRunning the test from the ChemStation Running the Pressure TestRunning the test from the Control Module Inside the flow path definitely will cause the test to failRunning the Pressure Test If the pressure test fails Evaluating the ResultsPotential Causes of Pressure Test Failure Potential Cause Pump Corrective ActionPotential Cause Autosampler Leak Test Half of the ramp Start the test and follow the instructions Tools required ¼ inch wrench Parts and materialsRunning the Leak Test Leak Test Pressure Profile No Pressure increase at Ramp Potential Cause Corrective ActionPotential Cause First plateau positive, second and third plateau negative All plateaus negativeFirst plateau negative, second plateau positive Ramp 3 does not reach limitThird plateau negative pressure drop 2 bar/min Evaluating the Results Repairing the Pump Exchanging Internal Parts Simple RepairsCleaning the Quaternary Pump Using the ESD Strap Using the ESD StrapOverview Overview of Repair ProceduresSimple Repair Procedures Typical Frequency Simple Repair ProceduresCartridge or the Active Inlet Valve Exchanging the Active Inlet ValveRemoving the Active Inlet Valve Exchanging the Valve CartridgeReplacing the Active Inlet Valve 105 Exchanging the Outlet Ball Valve 107 Purge Valve Exchanging the Purge Valve Frit orExchanged Head Assembly Removing and Disassembling the PumpDamage the pump drive 111 When required Exchanging the Pump Seals and Seal Wear-in ProcedureFor the seal wear-in procedure Tools requiredSeal Wear-in Procedure Will definetely damage the normal phase application seals0905-1420 Exchanging the Pump Seals and Seal Wear-in Procedure Parts Exchanging the PlungersInstalling the Continuous Seal Wash Option 117 Lifetime of the seals 119 Exchanging the Wash SealsExchanging the Wash Seals Mm hexagonal key Pump head grease Reassembling the Pump Head AssemblyReassembling the Pump Head Assembly Procedure Exchanging the Multi-Channel GradientValve Mcgv 124 125 Exchanging the optional Interface Board Exchanging Internal Parts Remove the solvent cabinet from the quaternary pump Removing the Top Cover and Foam129 130 Exchanging the Low Pressure Pump Main Board LPM Board LPM Board ConnectorsMcgv Connector DescriptionWA R NI N G T E Entering the Type Command using the Control Module Entering the Type CommandEntering the Type Command using the ChemStation Entering the Serial Number using the Control ModuleEntering the Serial Number Entering the Serial Number using the ChemStation Replacing the Quaternary Pump’s Firmware Exchanging the Damper Disconnect the two damper capillaries Reconnect the two damper capillaries Fan and arrow on the bottom foam Exchanging the Fan142 Part required Exchanging the Pump Drive144 Reinstall the pump head and fix with the two screws Tubings and cables Preparation for this procedure Exchanging the Power Supply148 149 150 Exchanging the Power Supply Exchanging the Leak Sensor 153 Part required Exchanging the Status Light PipeAssembling the Main Cover Cover kit contains all parts, but it is not assembledMay not be able to remove the side from the top part Procedure Located in its correct place Replacing the Top Cover and FoamTools required Screwdriver Pozidriv #1 Location of foam in the light switch 158 Parts and Materials Overview of Main Assemblies Overview of Main Assemblies Repair Parts Pump Housing and Main Assemblies Front ViewRepair Parts Pump Housing and Main Assemblies Rear View Control Module B-version Solvent Cabinet Solvent Cabinet Parts Description Part NumberSolvent Cabinet Parts Bottle Head Assembly Bottle-Head Assembly Parts Description Part NumberBottle-Head Assembly Parts Hydraulic Path Hydraulic Path Description Part NumberHydraulic Flow Path of the Quaternary Pump Cover Parts Cover Parts Description Part NumberCover Parts Sheet Metal Kit Sheet Metal Kit Description Part NumberSheet Metal Kit Foam Parts Foam Parts DescriptionFoam Parts Power and Status Light Pipes Power and Status Light Pipes Description Part NumberPower and Status Light Pipes Leak Parts Leak Parts Description Part NumberLeak Parts Pump Head Assembly Description Part Number Pump Head Assembly173 Pump Head Assembly with Seal Wash Option 175 Outlet Ball Valve Assembly Outlet Ball Valve Assembly Description Part NumberOutlet Ball Valve Assembly Purge Valve Assembly Purge-Valve Assembly Description Part NumberPurge-Valve Assembly Active Inlet Valve Assembly Description Part Number Active Inlet Valve AssemblyTools and Accessories Description Part Number Accessory Kit G1311-68705Seal Wash Option Description Part Number Seal Wash Option KitCables Overview Type Description Part Number Cable OverviewAuxiliary CablesExternal ContactsAnalog Cables Agilent 1100 to 3390/2/3 IntegratorsAgilent 1100 to 3394/6 Integrators Agilent 1100 to General Purpose Agilent 1100 to BNC ConnectorAgilent 1100 to 3390 Integrators Remote CablesAgilent 1100 to 3394 Integrators Agilent 1100 to 3392/3 IntegratorsAgilent 1100 to 3396 Series II / 3395A Integrators Agilent 1100 to 3396A IntegratorsAgilent 1100 to 3396 Series III / 3395B Integrators TTL Connector Pin Active 01046-60202 AgilentBCD Cables Agilent 1100 to 3396 Integrators Auxiliary Cable Can CableAgilent 1100 Series Degasser to general purposes Connector Pin G1103-61611 Color External Contact CableAgilent 1100 Series Interface Board to general purposes Agilent 1100 module to PC RS-232 Cable Kit 34398A RS-232 Cable KitRecommended Cables LAN Cables196 Introduction to the Quaternary Pump Overview of the Quaternary Pump Introduction to the Quaternary Pump199 How does the Pump Work? 201 Quaternary Pump Details How Does Compressibility Compensation Work?How Does Variable Stroke Volume Work? Electrical Connections 205 Instrument Layout EMF Counters Early Maintenance Feedback EMFPump Liquimeter Seal Wear CountersSetting the EMF Limits Using the EMF CountersLow pressure pump main board LPM, see ElectronicsLow-Pressure Pump Main Board LPM Block Diagram Signal Explanations Onboard BatteryFan Drive Electronic Fuses212 Interconnection Diagram Low Pressure Main Board LPM Firmware Description Resident SystemMain System Firmware Updates Optional Interface Boards BCD Board2110-0004 LAN Boards Agilent Order Number Supported networks LAN BoardAgilent 1100 Series Interfaces Agilent 1100 Series InterfacesGpib Interface Analog Signal OutputCan Interface Regulations, see Cable Overview onRS-232C APG Remote InterfacePin Signal Description APG Remote Signal DistributionRS-232C Connection Table Pin Direction FunctionRS-232 Cable Bit Configuration Switch Setting the 8-bit Configuration SwitchCommunication Settings for RS-232C Communication Gpib Default AddressesDefault Addresses for Agilent Series 1100 Modules Module Address Binary AddressBaudrate Settings Stay Resident Settings Forced Cold-Start SettingsParity Settings Forced cold start has been completedStay Resident Settings Main Power Supply MPS Block Diagram Main Power Supply AssemblyMain Power Supply Specifications 230 Control Module Screens for the Quaternary Pump Information/help Major keys on the Agilent 1100 Control ModuleEnter MenuScreens available from the Analysis screen Setup View Pump ON/OFF Settings Screens available from the Analysis screen Fillings to their current state Analog -Status Screens available from the Analysis screen 241 System screen Screens available from the System screenSystem Screens available from the Records screen Counters after exchanging parts that are subject to wear Screens available from the Records screen 247 Maintenance logbook Screens available from the Records screen Schematics Tests screen Diagnostics and TestsPressure Test Specifications Type Specification Performance Specifications255 256 Warranty Statement Limitation of WarrantyAll Chemical Analysis Products Responsibilities of the Customer Limitation of Remedies and LiabilityDays Onsite Responsibilities of Agilent TechnologiesSafety Information GeneralOperation Safety Symbols Safety SymbolsSymbol Description WA R NI N G CA U T IO N Lithium Batteries Information Radio Interference Sound EmissionManufacturer’s Declaration Solvents Flow CellAgilent Technologies on Internet Index 268 269 270 Page This Book
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1100 Series specifications

Agilent Technologies 1100 Series is a highly regarded lineup of high-performance liquid chromatography (HPLC) systems designed to meet the demanding needs of laboratories in various fields including pharmaceuticals, environmental testing, and food safety. Known for its versatility, reliability, and advanced technology, the 1100 Series has established itself as a benchmark for analytical performance.

One of the standout features of the Agilent 1100 Series is its modular architecture. This design allows users to configure the system according to specific analytical requirements. The components such as pumps, detectors, and autosamplers can be mixed and matched to create a tailored solution, ensuring maximum efficiency and optimal performance. This modularity also facilitates easy upgrades and maintenance, significantly extending the life cycle of the instrument.

At the heart of the 1100 Series is its advanced pumping technology. The system utilizes precise, high-pressure pumps that ensure a consistent flow rate and excellent reproducibility, essential for accurate quantification of analytes. The binary and quaternary pump options provide flexibility in method development, enabling users to perform gradient elution with ease.

The Agilent 1100 Series also boasts a range of detectors, including UV/VIS, fluorescence, and refractive index detectors. Each detector is designed to enhance sensitivity and specificity, enabling the detection of a wide array of compounds. The UV/VIS detector, in particular, is known for its reliable performance and user-friendly interface, which simplifies method setup and data analysis.

Another critical aspect of the 1100 Series is its autosampler. The system's autosamplers provide high throughput and automatic sample handling, which significantly reduces human error and increases productivity. The intelligent design allows for temperature control and reliable sample injection, ensuring optimal results.

In terms of software, the 1100 Series is supported by Agilent’s OpenLAB software, which offers an intuitive platform for method development, data acquisition, and analysis. This software integrates seamlessly with the HPLC hardware, making it easier for scientists to manage workflows and maintain compliance with regulatory requirements.

Overall, the Agilent Technologies 1100 Series represents a significant advancement in liquid chromatography, bringing together ideal characteristics such as modularity, precision, versatility, and sophistication. Its commitment to innovation and quality makes it a preferred choice for laboratories seeking reliable analytical solutions.
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