GE CTR 80 manual General Operation, Bath Fluid, Temperature Range, Viscosity, Specific Heat

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8 General Operation

8 General Operation

8.1Bath Fluid

Many fluids work with the CTR –80 bath. Choosing a fluid requires consider- ation of many important characteristics of the fluid. Among these are tempera- ture range, viscosity, specific heat, thermal conductivity, thermal expansion, electrical resistivity, fluid lifetime, safety, and cost. If the viscosity becomes too great, the stirrer may not function.

8.1.1Temperature Range

One of the most important characteristics to consider is the temperature range of the fluid. Few fluids work well throughout the complete temperature range of the bath. The temperature at which the bath is operated must always be within the safe and useful temperature range of the fluid. Set the cutout to meet the temperature limits of the selected fluid. The lower temperature range of the fluid is determined by the freeze point of the fluid or the temperature at which the viscosity becomes too great. The upper temperature is usually limited by vaporization, flammability, or chemical breakdown of the fluid. Vaporization of the fluid at higher temperatures may affect temperature stability because of cool condensed fluid dripping into the bath from the lid.

8.1.2Viscosity

Viscosity is a measure of the thickness of a fluid, how easily it can be poured and mixed. Viscosity affects the temperature stability of the bath. With low vis- cosity, fluid mixing is better which creates a more uniform temperature throughout the bath. This improves the bath response time which allows it to maintain a more constant temperature. For good control the viscosity should be less than ten centistokes. Twenty centistokes is about the upper limit of allow- able viscosity. Viscosities greater than this cause very poor control stability and may also overheat or damage the stirring motor. With oils viscosity may vary greatly with temperature.

When using fluids with higher viscosities the controller proportional band may need to be increased to compensate for the reduced response time (see Sec- tion9.6). Otherwise the temperature may begin to oscillate.

8.1.3Specific Heat

Specific heat is the measure of the heat storage ability of the fluid. Specific heat, to a small degree, affects the control stability. It also affects the heating and cooling rates. Generally, a lower specific heat means quicker heating and cooling. The proportional band may require some adjustment depending on the specific heat of the fluid.

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GE Kaye World Headquarters Table of Contents Parts and Controls General OperationController Operation Maintenance Trouble Shooting Digital Communication InterfaceWiring Diagram Figures Tables Symbols Used Before You StartSafety Information Canadian Standards AssociationBurn Hazard Bath Fluids Cold Baths Customer Service Information World HeadquartersIntroduction Specifications Environmental ConditionsIn-Warranty Repairs Hardware Warranty and AssistanceInstrument Warranty After-Warranty RepairsCustomer Support Agreement Equipment Maintenance AgreementsCustomer Support Customer Site AssistanceQuick Start UnpackingSet-up Power Setting the TemperatureAccess set-point selection Set-point 1, 25.0C currently used Bath Environment InstallationDrain Valve Installation Instructions Dry-out PeriodFilling With Fluid Necessary General Comparison CalibrationBath Use Calibration of Multiple Probes Parts and Controls Control PanelBath Tank and Lid Back PanelBack Panel Bath Fluid Temperature RangeGeneral Operation ViscosityThermal Expansion SafetyThermal Conductivity Electrical ResistivityWater Distilled CostCommonly Used Fluids EthanolFluid Characteristics Table Mineral OilSilicone Oil Dow Corning 200.05, 200.10 Limitations and Disclaimer Table of Various Bath FluidsStirring HeaterRefrigeration Temperature Controller OperationImportant Refrigerant Information General Operation Controller Operation Bath TemperatureTemperature Set-point Programmable Set-pointsDisplay Temperature Temperature Scale Units Set-point ValueScan Scan ControlScan Rate Heater Power Secondary MenuProportional Band New proportional band setting Cutout CO= 80CHigh Limit Controller ConfigurationOperating Parameters Low LimitSerial Interface Parameters CoolingDuplex Mode Baud RateSample Period Calibration Parameters LinefeedAlpha Hard Cutout11.2 R0 DeltaDigital Communication Interface Serial CommunicationsRS-232 Cable Wiring for WiringSetup IBM PC and CompatiblesSerial Operation Interface CommandsDuplex Mode Sample PeriodSecondary Menu Lfeed=on Lf=on Calibration Equipment Calibration ProcedureCalibration Procedure CalibrationCalibration Procedure Maintenance Maintenance Trouble Shooting TroubleshootingLow Voltage Directive Safety CE CommentsEMC Directive Wiring Diagram Revisions