Hach DR 5000 user manual 101

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Table of Contents

6.4 Single Wavelength (absorbance, concentration and transmittance measurements)

87

6.4.1 Set up single wavelength mode

87

6.4.2 Take single wavelength measurements (single reading)

89

6.4.3 Take single wavelength measurements (continuous readings)

89

6.5 Multi-Wavelength mode – measurements at more than one wavelength

90

6.5.1 Set the reading mode at different wavelengths

90

6.5.2 Complete a measurement in the multi wavelength mode

93

6.6 Wavelength Scan mode – recording of absorbance and transmittance spectrums

94

6.6.1 Set up the wavelength scan

94

6.6.2 Wavelength scan reading

97

6.6.2.1 Navigation of the wavelength scan graph or a wavelength scan analysis

98

6.6.3 Work with reference scans

99

6.7 Time course of absorbance/transmittance

101

6.7.1 Time course setup parameters

101

6.7.2 Time course scan reading

102

6.7.3 Analysis of time course data

103

6.7.3.1 Navigation of a time scan or a time scan analysis

104

6.8 System checks

105

6.8.1 Instrument information

105

6.8.2 Upgrade of the instrument software

106

6.8.3 Optical checks

106

6.8.3.1 Wavelength check

107

6.8.3.2 Noise check

108

6.8.3.3 Stray light check

110

6.8.3.4 Absorbance check

111

6.8.3.5 Drift check

112

6.8.3.6 Verification kit

113

6.8.4 Output checks

115

6.8.5 Lamp history

115

6.8.6 Factory service

116

6.8.7 Service time

116

6.8.8 Instrument Backup

117

Section 7 Maintenance

121

7.1 Cleaning requirements

121

7.1.1 Spectrophotometer

121

7.1.2 Display

121

7.1.3 Cuvettes/sample cells

121

7.2 Lamp replacement

122

7.2.1 Tungsten lamp replacement

122

7.2.2 Deuterium lamp (UV) replacement

123

7.3 Fuse replacement

124

7.4 Filter pad maintenance

125

7.4.1 Filter pad replacement

125

Section 8 Troubleshooting

127

Section 9 Replacement Parts

129

Section 10 Contact Information

131

Section 11 Limited Warranty

133

Index

135

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Contents January 2008, Edition Page Table of Contents Table of Contents 101 Table of Contents Section Specifications Specifications Precautionary labels Safety informationGeneral Information Use of hazard informationGeneral Information Class 1 Laser Chemical and Biological SafetySource Lamp Safety General Information Overview of productGeneral Information Operating environment Section InstallationUnpack the instrument Connection InstallationCell compartment Multi Cell Holder Top and Bottom 1 100 mm adapter optionalInstallation Multi Cell Holder Installation Installation Multi Cell HolderBeam path Beam pathChanging the language setting Power the instrument on and offStart Up Language selectionStart Up Overview Standard OperationsTips for the use of the touch screen Use of the alphanumeric keypadMain Menu options Standard Operations Main MenuOperator ID Instrument Setup modeStandard Operations Standard Operations Sample ID Display and sound preferences Date and timeVIS-Lamp and UV-Lamp Lamp ControlEffect caused by the lamp settings on the Measuring Mode Standard Operations USB connector Printer setupStandard Operations PC and printer KeyboardPrinter Setup Hach Data Trans Print dataPassword Password deactivation Standard Operations Data Log Store, recall, send and delete dataAuto/manual data storage Recall stored data from the data logTo send measurement data to a PC Send data from the data logDelete stored data from the data log Select Wavelength Scan or Time Course to recall data Data storage from wavelength scan or time courseRecall stored data from wavelength scan or time course Send data from wavelength scan or time course Option Press Wavelength Scan or Time Course and then Delete stored data from wavelength scan or time course Select a saved test/method enter user-specific basic data Stored ProgramsStored program options Stored programs optionsReading Mode Timer iconStandard Adjust Options Description Store Off/OnSet the reading mode Standard Operations Use of program timersTake single wavelength measurements single reading Set the dilution factorTake single wavelength measurements continuous readings Press OptionsMore…Dilution FactorRun a standard adjust Press Save as Default Change of the default setting of the chemical formSet the chemical form Press OptionsMoreChemical FormPress OptionsMoreReagent Blank Standard Operations Run a reagent blankMeasurement/analysis of a reagent blank Add stored programs to the favorite programs list Standard Operations Analysis of samplesCell compartment #1 Barcode ProgramsStandard Operations Complete a barcode 13 mm test/vial Changing the standard settingSelect the measuring range Select the chemical evaluation formBarcode program options Basic test-specific and sample-specific data settingsEdit Sample blankOptions Description Send Data icon Manual update of a barcode test Update/edit barcode testsProgram update options Enter the NameEnter the Measurement Process Enter the VersionTimer 1, Timer 2, Timer 3 and Timer Option 1 Manual update of test data Update an existing barcode testOption 2 Manual check/revision of test data Press OptionsMoreEditProgram a new test Upgrade of the instrument softwarePress OK to return to the System Checks menu Standard Operations Program a user method Advanced OperationsUser Programs Program Number Advanced OperationsProgram Name Program TypeConcentration resolution number of decimal places Single wavelength settingsUnits Wavelength single wavelength program typeAbsorbance formula multi-wavelength program type Multi wavelength settingsChemical form Concentration Factor Kx List of available absorbance formulasWavelength λx Calibration by entering calibration values Calibration settings for single and multi wavelength modeCalibration settings Advanced Operations Advanced Operations Advanced Operations Upper and lower limits of the measuring range Store a user programAdditional user-defined parameters and functions Chemical form 2 / chemical form 3 / chemical form Timer 1 / Timer 2 / Timer 3 / TimerDefinitions of the program points Advanced Operations Free programming program typeMeasurement process Enter a new element of a measuring sequence Content and definition of the keys Key / ZeroingKey / Reading Process Timer keyDelete an element of a measuring sequence Enter the calibration formula evaluation formulaInsert an element of a measuring sequence Enter calibration formula C1New Number Edit formula key descriptionsScreen Key Description C2 On Enter the next calibration formula C2 or CnSelect Conc. key Enter variablesSave a free programming user program 4 Add, edit and delete user programs from the favorites list Advanced Operations Select a user programDelete Add to FavoritesEdit Delete a favorite program Favorite ProgramsRecall a favorite program Method Measures to identify other interference factors ChecklistStandard Addition monitoring/checking results Sample volume Peak volume Standard additionCheck the standard solution Complete a standard additionPress OptionsMoreStandard Addition Peak volume/sample volume methodsDescription of the table of readings Advanced Operations Program Set up single wavelength modeSingle wavelength setup options Options Description Concentration resolutionConcentration factor Take single wavelength measurements continuous readings Reading modeTake single wavelength measurements single reading Multi-wavelength setup options Set the reading mode at different wavelengthsAbsorbance formula Press Absorbance Formula Concentration factor For data storage, see .3.1.1 on Wavelength scan setup options Set up the wavelength scanScale & Units Setting wavelengthOption Description Integral Cursor modeSelect view displaying table Scale & units Press Scale & Units Wavelength scan readingNavigating the wavelength scan Highlight Reference Advanced Operations Work with reference scans100 Time course setup options Time course setup parametersTime course of absorbance/transmittance 101Time & interval Time course scan readingScale & units 102103 Analysis of time course data104 Navigation of a time scan or a time scan analysisNavigating the time scan 105 System checksInstrument information 106 Advanced Operations Upgrade of the instrument softwareOptical checks 107 Wavelength check108 Noise check109 110 Stray light check111 Absorbance check112 Drift checkPress Nominal Values 113 Verification kit114 Press Verification115 Output checksLamp history 116 Advanced Operations Factory serviceService time 117 Instrument Backup118 Restore backup data119 120 Cleaning requirements MaintenanceSpectrophotometer DisplayMaintenance Lamp replacementTungsten lamp replacement 122123 Deuterium lamp UV replacement124 Fuse replacement125 Filter pad maintenanceFilter pad replacement 126 Base of DR 5000 with filter grid127 Section Troubleshooting128 TroubleshootingDescription Cat.-No Section Replacement Parts129 130 Replacement Parts131 Contact Information132 Contact InformationLimitations Limited WarrantyLimitation of Remedies 133134 Limited Warranty135 Index136