SSI America 90-2581 REV B manual 3.5Rear Panel Remote Input, 3.6Symbols

SSI America 90-2581 REV B manual Pump Features, fFast & easy setup SSI America 90-2581 REV B manual Wetted Pump Materials, Self-FlushingPump Head, Microprocessor advanced control SSI America 90-2581 REV B manual Self-Flushand Seal Life SSI America 90-2581 REV B manual Flow Rates SSI America 90-2581 REV B manual Installation, 2.1Unpacking and Inspection, 2.2Location/Environment SSI America 90-2581 REV B Self-Flush, Pump, Connect wash solution inlet and outlet tubing, into, Open Prime-Purgevalve by SSI America 90-2581 REV B manual Solvent Out-gassingand Sparging, 2.4Electrical Connection, 2.5Solvent Preparation SSI America 90-2581 REV B manual Cavitation, Filtration, Initial system pressurization Daily, 2.6.1Mobile Phase Reservoirs SSI America 90-2581 REV B manual Self-FlushSolution, Inlet Tubing and Filters, Priming the Pump and the Flushing Lines SSI America 90-2581 REV B manual 2.7.1Isopropanol Flush, Packaging for Shipping, 2.7Preparation for Storage or Shipping SSI America 90-2581 REV B manual Operation, 3.1.1Control Panel SSI America 90-2581 REV B manual SSI America 90-2581 REV B manual 3.5Rear Panel Remote Input, 3.6Symbols SSI America 90-2581 REV B manual Theory Of Operation, 4.1.1Liquid System Flow Path, Pump Cycle, Pulse Damping SSI America 90-2581 REV B manual Microprocessor Control, DC Power Supply, Remote Interfacing, Motor Stall Detector SSI America 90-2581 REV B manual SSI America 90-2581 REV B manual Maintenance, Inlet Filters, 5.2.1Removing a Pump Head, 5.1Filter Replacement SSI America 90-2581 REV B manual Remove the inlet line from the inlet check valve SSI America 90-2581 REV B manual Outlet Flushing Check Valve SSI America 90-2581 REV B manual Outlet Flushing SSI America 90-2581 REV B manual Cleaning the Pump Head Assembly SSI America 90-2581 REV B manual SSI America 90-2581 REV B manual Replacing Piston Seals SSI America 90-2581 REV B Remove the pump head as described in .2.1. Use caution so as not to damage the sapphire piston SSI America 90-2581 REV B manual Changing the Piston, Condition the new seal as described in Section SSI America 90-2581 REV B manual 5.2.5Replacing the Pump Head, 5.3Conditioning New Seals SSI America 90-2581 REV B manual 5.5.1Removing the Pulse Damper, Pulse Damper Refurbishing, 5.5Pulse Damper Replacement SSI America 90-2581 REV B manual Pulse Damper Installation, 5.6Cleaning the Pump SSI America 90-2581 REV B manual 5.7Lubrication, 5.8Other Pump Maintenance SSI America 90-2581 REV B manual 7-14 SSI America 90-2581 REV B manual 5.9Fuse Replacement SSI America 90-2581 REV B manual Unplug the unit 2.Remove the cover SSI America 90-2581 REV B manual Quick Guide to Problem Solving, You Notice, This May Mean, Possible Cause, You Should SSI America 90-2581 REV B manual List Of Replacement Parts SSI America 90-2581 REV B manual Seal Kit, Aqueous, 5mL SSI America 90-2581 REV B Appendix A, A.1.1 Hardware Implementation, Part Description, Part Number, A.1.2 Hand-Shaking
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3.5Rear Panel Remote Input

Align Refill Switch Mode: The signal that initiates the refill phase can be displayed during power-up by pressing and holding the PRIME and the UP-ARROW buttons when the power is switched on. Release the buttons when the display displays "rFL". When the slotted disk allows the light beam to pass from the emitter to the detector on the slotted optical switch a pulse will be generated which signals the beginning of refill. When this pulse occurs the three horizontal segments displayed at the top of the display will turn off and the three horizontal segments at the bottom of the display will turn on. To exit this mode, press the RUN/STOP button.

Serial Port Loopback Test Mode: If an external device will not communicate to the pump via the serial port, the serial port loopback test can be used to verify that the serial port is functioning properly. During power-up press and hold the UP-ARROW and the DOWN- ARROW buttons when the power is switched on and then release the buttons. The display must display "C00" for the first half of the test to pass. Plug in the serial port loop back plug (A modular plug with pins 2 & 5 jumpered together and pins 3 & 4 jumpered together.). The display must read "C11" for the second half of the test to pass. To exit this mode, press the RUN/STOP button.

3.5Rear Panel Remote Input

An RS-232 modular jacks are provided on the back panel. A computer, with appropriate software, can be used as a remote controlling device for pump operation via this connection.

See Appendix A for details on connection and operation.

3.6Symbols

The following symbols may appear on back panel of the unit:

Caution: To avoid chemical or electrical hazards, always observe safe laboratory practices while operating this equipment.

Caution: To avoid electrical shock and possible injury, remove the power cord from the back panel of this equipment before performing any type of service procedures.

Note: The user shall be made aware that, if equipment is used in a manner not specified by the manufacturer, the protection provided by the equipment may be impaired.

3-9

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Contents Binary Solvent Delivery Module Operators ManualPage 1.INTRODUCTION 1.1.1 Pump Features fFast & easy setup1.1.3 Self-FlushingPump Head 1.1.2 Wetted Pump MaterialsMicroprocessor advanced control 1.1.4 Self-Flushand Seal Life It is recommended that the Self Flush feature be used to improve seal life in a number of applications. In particular, as stated above if pumping Buffers, Acids/Bases or any inorganic solution near saturation, the pump should utilize the Self Flush feature. With every piston stroke, an extremely thin film of solution is pulled back past the seal. If this zone is dry without use of Self Flush, then crystals will form with continuous operation, which will ultimately damage the sealFlow Rates 2.INSTALLATION 2.1Unpacking and Inspection2.2Location/Environment 2.3Fluid Connections & PrimingSELF-FLUSH PUMPConnect wash solution inlet and outlet tubing opaque to the flush housing as shown2.4Electrical Connection 2.5.1 Solvent Out-gassingand Sparging2.5Solvent Preparation 2.6.1Mobile Phase Reservoirs 2.5.2 Cavitation2.5.3 Filtration 2.5.4 Initial system pressurization Daily2.6.2 Self-FlushSolution 2.6.3 Inlet Tubing and Filters2.6.4 Priming the Pump and the Flushing Lines 2.6.6 Long Term Pressure Calibration Accuracy2.7.2 Packaging for Shipping 2.7.1Isopropanol Flush2.7Preparation for Storage or Shipping 3.OPERATION 3.1.1Control PanelNon-volatileMemory Reset If the pump is operating erratically, there is the possibility that the memory has been corrupted. To reset the memory and restore the pump to its default parameters, press and hold the UP-ARROWbutton when the power is switched on. Release the button when the display reads rES. The parameters stored in non-volatilememory, i.e., the flowrate, the pressure compensation, the voltage/frequency select, the lower pressure limit, and the upper pressure limit will be set to the factory default values. The head type setting is the only parameter not changed by the non-volatilememory reset function. If the firmware is upgraded to a newer version, a non- volatile memory reset will automatically occur the first time the power is switched on 3.6Symbols 3.5Rear Panel Remote Input4.THEORY OF OPERATION 4.1.1Liquid System Flow Path4.1.2 Pump Cycle 4.1.3 Pulse Damping4.2.2 DC Power Supply 4.2.1 Microprocessor Control4.2.3 Remote Interfacing 4.2.4 Motor Stall DetectorPage 5.MAINTENANCE 5.1.1 Inlet Filters5.2.1Removing a Pump Head 5.1Filter Replacement3.Remove the inlet line from the inlet check valve OUTLET FLUSHING CHECK VALVE OUTLET FLUSHING 5.2.2 Cleaning the Pump Head Assembly 1.Inspect the piston seal cavity in the pump head. Remove any foreign material using a cotton swab, or equivalent, and avoid scratching the sealing surfaces. Repeat for the self-flushhousing. Be sure no fibers from the cleaning swab remain in the components3.If the check valves have been removed, tighten the check valves on stainless steel pumps to 75 inch-poundsor enough to seal at maximum pressure. Do not exceed maximum torque. For Bioclean PEEK pumps, tighten each check valve firmly by hand. Do not go ¼ turn past finger tight 5.2.3 Replacing Piston Seals Lower than normal pressure, pressure variations, and leaks in the pumping system can all indicate possible problems with the piston seal. Depending on the fluid or mobile phase used, piston seal replacement is often necessary after 1000 hours of running time1.Remove the pump head as described in Section 5.2.1. Use caution so as not to damage the sapphire piston 5.2.4 Changing the Piston 5.Condition the new seal as described in Section5.2.5Replacing the Pump Head 5.3Conditioning New Seals5.5.1Removing the Pulse Damper 5.5.2 Pulse Damper Refurbishing5.4Check Valve Cleaning and Replacement 5.5Pulse Damper Replacement5.5.3 Pulse Damper Installation 5.6Cleaning the Pump5.8Other Pump Maintenance 5.7Lubrication7-14 5.9Fuse Replacement 1.Unplug the unit 2.Remove the cover 6.PROBLEM SOLVING Quick Guide to Problem SolvingYou Notice This May Mean7.LIST OF REPLACEMENT PARTS 880201 Seal Kit, Aqueous, 5mL APPENDIX A A.1.1 Hardware ImplementationPart Description Part NumberA.1.3 Command Interpreter“/” character Page A.2.1 Pressure Fault and Motor Stall Fault Output A4-pinterminal board connector and a 10-pinterminal board connector are provided on the back panel. Any device capable of providing the proper run/stop logic level, flowrate control frequency, or flowrate control voltage can be used as a remote controlling device for pump operation via this connection. The terminal board connectors can be removed for ease of connecting wires, if desired, by pulling firmly rearward and should be reinserted firmly afterwardA.2.2 General Information on Inputs the EVENT 1 terminal and the EVENT 2 and EVENT 3 terminals is affected. EVENT 2 is Normally Closed connected to EVENT 1 until a fault occurs and then opens. EVENT 3 is Normally Open not connected to EVENT 1 until a fault occurs and then closesA.2.4 Run and Stop Inputs The PUMP-RUN, PUMP-STOP,and ENABLE IN inputs operate from an internal 5 VDC source and each one draws approximately 0.008 amps when connected to COM. To activate either the PUMP- RUN, PUMP-STOP,or ENABLE IN input connect it to COM. Any device capable of switching 0.008 amps can be connected between the PUMP-RUN, PUMP-STOP,or ENABLE IN input and COM, such as: a switch contact, a relay contact, an open collector output, an open drain output, or any output with a high logic level output of 3.8 to 6.0 volts and a low logic level output of 0.0 to 0.5 volts. A switch contact or a relay contact is preferred since this type of connection will provide isolation between the pump and the controlling device. The COM terminal is internally connected to the pumps chassis ground and should be connected to the controlling devices ground or zero volt terminal when the controlling device has an open collector output, an open drain output, or any output with logic level outputA.2.4 Enable Input When activated ENABLE IN is at a low logic level, the ENABLE IN input disables flowrate control on the front panel and enables flowrate control on the back panelAPPENDIX B EZ GRIP FITTING GUIDEScientific Systems Inc Warranty Statement A-10
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