IBM M/02-212 operating instructions General Description, Use of the Rheometer, Measuring Principle

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I. General Description

In this chapter you get general information concerning use and measurement principle of your R/S Rheometer.

I.1 Use of the Rheometer

The R/S Rheometer system provides possibility of Newtonian fluids viscosity measurements, recording of flow curves as well as determination of viscosity functions of non-Newtonian fluids in steady shear flows. Furthermore, it assures carrying out of measurements in non-stationary shear flows and the measurements of viscoelastic substances values in creep processes. The R/S Rheometer is used in quality control, production control and researches

I.2 Measuring Principle

The R/S Rheometer is a rotational-shear rate /shear stress-rheometer.

Concentric cylinders, measuring cones and plates are available as measuring system. The measuring- sample is positioned in measuring gap between the stationary measuring cup and the rotating measuring bob (Searle-principle), respectively between the rotating cone or plate and the stationary lower plate (cone/plate-, cone/cone-measuring-system).

The measuring drive developed for this instrument operates with a high dynamic precision-drive- system with optical encoder without gearing and without mechanical force transducers, so torque is measured without deflection.

The R/S Rheometer measuring drive is applicable for carrying out rotational measurements with pre-set of speed (shear rate) and pre-set of torque (shear stress).

In case of shear rate pre-set the torque acting on rotating measuring bob/cone/plate by measuring substance flow resistance is measured (shear stress is measured).

In case of shear stress pre-set resulting speed of rotating measuring bob/cone/plate is measured (shear rate).

Shear stress measurements can be carried out with R/S Rheometer in order to determine flow behavior of plastic substances and enables exact measurement of yield point without shearing the measuring substance.

The types of measurements

-rotation measurement with controlled shear rate (CSR)

-rotation measurement with controlled shear stress (CSS)

can be carried out in manual (without PC support) or in connection with a computer system with the software RHEO 2000.

The creep measurements requires computer system with software RHEO 2000.

Brookfield Engineering Labs., Inc.

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M/02-212

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Contents Brookfield R/S Rheometer Brookfield Engineering Labs., Inc 02-212 Contents Appendix Measuring Principle General DescriptionUse of the Rheometer II.1 R/S Rheometer II. System ConfigurationRheometer main instrument minimum configuration II.3 Computer System II.2 Measuring DevicesIII.1 Stand Mounting III. Instrument InstallationHints for height adjustment of the stand III.2 Electrical Connections III.2.1 Temperature Sensor Pt100III.2.3 Printer Connection III.2.2 AC-AdaptorIII.2.4 Computer Connection Use data link cable of Brookfield delivery onlyFTK-CC III.3 Mounting of temperature controlled measuring devicesThermostat connection to temperature control device FTK-CC III.3.2 Mounting of the measuring device ME-CP/PP Thermostat connection to temperature control device FTK-CCBrookfield Engineering Labs., Inc 02-212 Brookfield Engineering Labs., Inc 02-212 Mounting III.3.3 Mounting of the cooling device KEIV.3 Cleaning IV. Environment, handling, cleaning and maintenanceIV.1 Operating environment, Storage IV.2 HandlingIV.4 Maintenance Measurement directly in the substance Measuring SystemsDepth of immersion Measurement with substance in measuring systemMeasurement with temperature control device FTK-CC Turn left Turn right Lower Lift Brookfield Engineering Labs., Inc 02-212 Voltage check VCC15.25 VI. Operation and Menue SystemRheometer Ver .02 #xxxxxx 07.05.98 Brookfield Brookfield VI.1 KeyboardKey-function dependent to executed operation Zero-point calibration VI.2 Menu System of R/S RheometerDefine/edit program Print programs from memoryMenu handling CONFIGURATION-,emie Set time/date Set RS232 Param LanguageVI.3 Selecting from Lists Main-menue Run Single Run Program RemoteSelect Measuring system CC48 CC45 VI.4 Input of numerical values and alphanumeric textsInput Values Val.1/s0100.00 Nr. of MP010 Times Input Values Val.1/s0200.00 Nr. of MP010 Times0100Input Values Val.1/s0290.00 Nr. of MP Times0100 Input Values Val.1/s0200.00 Nr. of MP Times0100VI.5.1 MAIN-Menue → Run Single VI.5 Menue entries Main menueProg. Running Wait for 1.MP Output of MPs to No output device Memory Menu ST StartVI.5.2 MAIN-Menue → Run Program Program end Single mode Total time100s Total #MP10No valid program Enter program first Select program Prog xyz Test Prog ÖlProg. running Wait for 1.MP #1 Output of MPs to Printer Memory MenueVI.5.3 Main menue → Remote VI.5.5 Main menue → ConfigurationVI.5.4 Main menue → Utilities Program end Test Total time200s Total #MP40VI.6.2 Utilities → Edit Programs VI.6 Menue entries in the Utilities-MenueVI.6.1 Utilities → Zero Calibration D1/s=ft Select Meas. system CC45 CC25 CC14 Select Prog to edit Prog xyz Test NEWNr. of steps Select Input-Mode -D1/s Nrpm TauPaEdit Program name Range-Error Range-Error Start-Value min 0.90 maxInput Step Nr time s VI.6.4 Utilities → Measuring systems VI.6.3 Utilities → Print ProgramsTest Press OK to save Printer not ready OK cont. ST stopEnter Meas. Sys. #4 Name CP25 tauprom 01.1418 kgamma VI.6.5 Utilities → Print memoryPress OK to save Name CC25 tauprom 01.1418 kgamma Sel. Output-device Printer RS232VI.6.6 Utilities → Clear memory VI.6.7 Utilities → Measure temperatureVI.7.1 Configuration → Set output mode VI.7 Menu entries of the Configuration menuService, Service2 for service personnel only Select output device No output device Printer RS232VI.7.4 Configuration → Set Time/Date VI.7.2 Configuration → MeasCount modeVI.7.3 Configuration → Reset meascount RS232 4800,8,n,1 Change RS232-Par.? Okyes Stno VI.7.5 Configuration → Set RS232 ParameterNew Time/Date 1715 Press OK to save VI.7.7 Configuration → Service, Service VI.7.6 Configuration → LanguageVI.8 Serial Data transfer via Interface RS232 Baudrate -4800 9600Brookfield Engineering Labs., Inc 02-212 Brookfield Engineering Labs., Inc 02-212 VII. Measurements VII.1 Measuring in manual modeMeasurement control Measurement with FTK-CCVII.2 Measuring in Remote-mode Measurement in remote control modeVIII. Technical data Measured or evaluated values Weight Temperature rangeIX. Guarantee Given ranges are standard values not maximum values A1Data sheets of standard measuring systemsDG DIN Table Plate/Plate measuring systems DIN Measuring system C25-1 C25-2 C50-1 C50-2 C75-1 C75-2Range Error A2 Error messagesPrinter Error Range error End value min 0.90 maxBreak torque max! Single mode Total MP Total time Zero Calibration ErrorError #3 Zero cal. error Please retry cal ST stop Break Speed MAX Break Speed max! Single mode Total MP Total timePC Side A3 Pin-layout of the serial data cableRheometer side General information A4 Requirements to the mains connecting cablesUSA and Canada Other countriesEnglishGermanEnglishGerman A5 Language cross referenceGerman menue system of RC20 Index

M/02-212 specifications

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