Teledyne Calibration Procedures, User Notes, 7.1. M102E Calibration, 7.2. M501-TRS Calibration

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M102E/M501 TRS

CALIBRATION PROCEDURES

(Addendum to M101E Manual - P/N 04740 Rev A)

7. CALIBRATION PROCEDURES

7.1. M102E Calibration

Calibration of the M102E should be performed according to the procedures described in Chapters 7 & 8 of the M101E Manual - P/N 04740 Rev A.

NOTE

It is recommended that the M102E be calibrated in TRS gas measurement mode using

H2S as a span gas.

If you are using the M102E for US-EPA controlled monitoring of SO2, see Chapter 8 of the M101E Manual (P/N 04740 Rev A) for information on the EPA calibration protocol.

7.2. M501-TRS Calibration

The M501-TRS converter does not require field calibration.

USER NOTES:

05514 Rev A1

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Contents with MODEL 102E TOTAL REDUCED SULFUR ANALYZERMODEL 501 TRS THERMAL CONVERTER ADDENDUM TO MODEL 101E OPERATORS MANUALPage Addendum to M101E Manual - P/N 04740 Rev A TABLE OF CONTENTSM102E/M501 TRS 05514 Rev A19. THEORY OF OPERATION LIST OF APPENDICES8. INSTRUMENT MAINTENANCE 10. TROUBLESHOOTING & REPAIRLIST OF TABLES LIST OF FIGURESPREFACE Page corner of the display any time the instrument is in SETUP mode 1. PREFACE1.1. Reference Numbering convention User Notes2.2. EPA Equivalency Designation 2. SPECIFICATIONS, APPROVALS AND WARRANTY2.1. Specifications 2.1.1. M501-TRS Specifications2.3. CE Mark Compliance Never disconnect electronic circuit boards, wiring harnesses or 3. GETTING STARTED3.1. Unpacking the M102E 3.2. Unpacking the M501-TRSthat the rack/enclosure itself is adequately ventilated 3.2.1. M501-TRS Ventilation Clearancethe maximum operating temperature specification for the M102E 40C Figure 3-1 M102E Internal Layout 3.3. Internal LayoutsFigure 3-2 M501-TRS Internal Layout M501 3.4. Internal Pneumatic Flow of the M102E & the M501-TRSTable 3-1 TRS - SO2 Switching Valve Operating Modes M102E INSTRUMENT CHASSIS5 Amp 3.5. Rear Panel Layout for the M102E & M501-TRSAlarm Output Figure 3-4 M102E Rear Panel LayoutFigure 3-6 Analog Output Connector 3.6. Initial Setup3.6.1. Electrical Connections 3.6.1.1. M102E Analog Output ConnectionsM501-TRS PNEMATIC CONNECTERS 3.6.1.2. M501-TRS Alarm Output Connections3.6.2. Pneumatic Connections M102E PNEMATIC CONNECTERS102E MODELSPAN GAS The exhaust from the instrument needs to be vented outside theZERO AIR 3.6.2.1. Connections with Internal Valve Options InstalledVENT Gas Dilution CalibratorVENT if input is pressurized Valve Option OptionPossible Warning Messages at Start-Up 3.7. Initial Operation3.7.1. Startup / Warm Up of the M102E 3.7.2. Functional Check of the M102EDisplay area High Alarm LED Low Alarm LED3.7.3. Startup / Warm Up of the M501-TRS Process Variable3.8. Initial Calibration Page OPTIONAL HARDWARE AND SOFTWARE 4. OPTIONAL HARDWARE AND SOFTWARE4.1. Rack Mount Kits Options 20a, 20b, 21, 22 4.2. Calibration Valves OptionsZero/Span Valve Operating States Table 4-2 IZS Valve Operating States M102E INSTRUMENT CHASSIS4.3.1. Printed Manuals P/N 4.3. Additional Manuals4.3.2. Addendum on CD Part number M102E OPERATING INSTRUCTIONS 5.1.1. M102E Analog Output Signals5. M102E OPERATING INSTRUCTIONS Figure 5-1 Analog Output Connector KeyTable 5-1 M102E gas Measurement Modes 5.2. SETUP - DIAG Using the Diagnostics Functions5.1.2. Setting the M102E Gas Measurement Mode 5.2.1. M102E Analog I/O Configuration5.3.2. M102E Ethernet Host Name 5.3. SETUP - COMM Setting Up the M102E’s Communication Ports5.2.2. M102E Test Channel Output 5.3.1. M102E ID CodeZERO 5.4. Remote Operation of the Analyzer5.4.1. Control Inputs CONTROL INSPAN 5.4.2. Using the M102E with a Hessen Protocol Network5 VDC Power Supply 5.4.2.1. M102E Hessen Protocol Gas ID ListTable 5-6 Default Hessen Status Bit Assignments 5.4.2.2. Setting Hessen Protocol Status FlagsTeledyne Instruments customer service 6. M501-TRS OPERATING INSTRUCTIONS6.1. Basic M501-TRS Controls DO NOT OPERATE WITHOUT THE COVER OF THE M501TS CONVERTER INSTALLEDTable 6-1 M501-TRS Temperature Controls and Definitions 6.2. To Display The Current TemperatureDO NOT SET THE TEMPERATURE HIGHER THAN 1050OC 6.3. To Manually Adjust the Converter Oven Temperature6.4.1. Initiating the Autotune Process 6.4. Autotune the Temperature Controllerhas reached a stable, constant temperature 6.4.2. Aborting the Autotune Process 6.5. M501TRS Alarm Relay Adjustmentnecessary to repeat the autotune procedure Page 7.2. M501-TRS Calibration 7. CALIBRATION PROCEDURESUSER NOTES 7.1. M102E CalibrationPage INSTRUMENT MAINTENANCE 8. INSTRUMENT MAINTENANCE8.1.1.1. Predicting When the SO2 Scrubber Should Be Replaced 8.1. Additional and Updated Maintenance Procedures8.1.1. Maintaining the SO2 Scrubber 8.1.1.3. Changing the SO2 Scrubber Material 8.1.1.2. Checking the Function of the SO2 ScrubberPage 9.1.2. SO2 Ultraviolet Fluorescence 9. THEORY OF OPERATION9.1. Measurement Principle 9.1.1. TRS ConversionFigure 9-1 UV Absorption in the M102E Reaction Cell SO2 + hv214nm ⎯⎯Ia⎯→ SO2SO2 * ⎯⎯→ SO2 + hv330nm Ia = I0 1 − exp− axSO2kSO2 * ⎯⎯F⎯→ SO2 + hv330nm F = kSO2Equation9-6 9.3.1. Sample gas Flow 9.2. The UV Light Path9.3. Pneumatic Operation 9.2.1. UV Lamp Shutter & PMT OffsetSAMPLE CHAMBERUV Lamp PMT HOUSING9.4. Electronic Operation 9.4.1. Sensor ModuleSample Air 9.4.1.1. Sample Chamber9.4.1.2. Sample Chamber Heating Circuit Sample Air Housing Outlet O-Ring O-Ring Seal SealP-I-D CONTROLLER 9.4.2.1. Thermal Switch9.4.2. M501-TRS electronics HEATER9.4.2.2. Temperature Alarms and Alarm Output 10.1.1.1. M102E Warning Messages 10. TROUBLESHOOTING & REPAIR10.1.1. Fault Diagnosis with Warning Messages 10.1.1.2. M501-TRS Error CodesTable 10-2 Test Functions - Possible Causes for Out-Of-Range Values 10.1.2. Fault Diagnosis with Test Functionsfunctioning 10.3.1. Excessive noise 10.2. M501-TRS Trouble shooting10.3. Other Performance Problems 10.2.1. TRS Converter Not Heating10.4.1. Checking the Efficiency of the M501-TRS SO2 Scrubber 10.4. Subsystem Checkout10.4.2. Checking the Efficiency of the M501-TRS TRS Æ SO2 Converter 10.5.1. UV Lamp Adjustment and/or Replacement 10.5. Additional Repair ProceduresAlways grasp the main body of the lamp 10.5.1.1. Adjusting the UV Lamp Peaking the LampALWAYS wear UV-Protective, Safety Glasses when working with the UV Lamp AssemblyFigure 10-1 Shutter Assembly - Exploded View 10.5.1.2. Replacing the UV LampFigure 10-2 Disassembling the Shutter Assembly 10.5.2. Replacing the UV filter/lensFigure 10-3 PMT Assembly - Exploded View 10.5.3. Replacing the PMT, HVPS or TEC3. Remove the reaction cell assembly 10.5.4. M102E PMT Hardware Calibration FACTORY CAL Figure 10-4 Pre-Amplifier Board Layout 6. Locate the Preamp board see FigureNORM PMT value of twice the ppb value of the span gas EXAMPLE 10.5.5. Replacing the TRS Converter Heating TubeIf a reporting range other than 500 ppb is used in this procedure Adjust the PMT until NORM PMT equals 1280 mV ± 10 mVelement off 10.6. Manually Programming the M501-TRS Temperature ControllerThe ceramic bobbins at each end of the heater assembly are fragile Be Careful115V/60Hz with a set value of 1000C 10.6.1. Temperature Controller Primary Menu ParametersTable 10-3 - Temperature Controller - Primary Parameter Settings Table 10-4 - Temperature Controller - Primary Parameter Settings 10.7. Technical Assistance05514 Rev A1 M102E/M501 TRS APPENDIX A - Version Specific Software Documentation APPENDIX A - Version Specific Software DocumentationAPPENDIX A-2 Model 102E Setup Variables Available Via Serial I/O APPENDIX A-4 Model 102E Signal I/O DefinitionsAPPENDIX A-1 M102E Software Menu Trees, Revision A.2 SAMPLE SETUPENTER SETUP PASS APPENDIX A-1 M102E Software Menu Trees, Revision A.2CLR 1,3 SAMPLETEST MSG 1,2SO2, 111, REPORTED ACAL1TR2, 112, REPORTED Figure A-4 Secondary Setup Menu DIAG SAMPLE ENTER SETUP PASSDIAG MEASUREMODE APPENDIX A-2 Setup Variables For Serial I/O, Revision A.2Deleted Setup Variables for M102E Software Revision A.2 Table A-2Table A-6 Test Functions Deleted from M102 Software Revision A.2 setting of STABILFREQ and STABILSAMPLESAPPENDIX A-3 Warnings and Test Functions, Revision A.2 Table A-4 Warning Messages deleted from M102 Software Revision A.2APPENDIX A-4 M102E Signal I/O Definitions, Revision A.2M102E/M501 TRS APPENDIX A-4 M102E Signal I/O Definitions, Revision A.2Rear board primary MUX analog inputs Function APPENDIX A-5 M102E iDAS Functions, Revision A.2Trigger Event CTEMPWAPPENDIX A-5 M102E iDAS Functions, Revision A.2 A-10M101E Manual - P/N 04740120 Rev A APPENDIX B - M102E Spare Parts ListAPPENDIX B - M102E Spare Parts List Table B-1 M102E Spare Parts ListAddendum to M101E Manual - P/N 04740 Rev A INSTRUMENTS Warranty/Repair Questionnaire Model 102EM102E/M501 TRS TELEDYNEINSTRUMENTS Addendum to M101E Manual - P/N 04740 Rev A APPENDIX D - ELECTRONIC SCHEMATICSAPPENDIX D - ELECTRONIC SCHEMATICS Table D-1 List of Included Electronic Schematics05518 Rev A APPENDIX D - ELECTRONIC SCHEMATICSUser Notes M102E/M501 TRS