Teledyne 102E Additional and Updated Maintenance Procedures, Maintaining the SO2 Scrubber, Rev A1

Page 46
8.1. Additional and Updated Maintenance Procedures

INSTRUMENT MAINTENANCE

M102E/M501 TRS

 

(Addendum to M101E Manual - P/N 04740 Rev A)

8.1. Additional and Updated Maintenance Procedures

The following procedures need to be performed regularly as part of the standard maintenance of the Model 102E.

8.1.1. Maintaining the SO2 Scrubber

This section REPLACES Section 9.3.3 of the M101E Manual - P/N 04740 Rev A.

Unlike the M101E which includes an internal scrubber to remove SO2 from the sample gas before the H2S Æ SO2 conversion takes place, the M102E relies on the SO2 scrubber of the M501-TRS to perform the same function.

The SO2 scrubber of your M501-TRS utilizes a consumable compound to absorb SO2 from the sample gas before the TRS is converted to SO2. This material must be replaced periodically in order for the analyzer to continue measuring TRS accurately and reliability.

This material is capable of efficiently scrubbing SO2 for up to 1000 ppm-hours. This means that if the SO2 content of the sample gas is typically around 100 ppb, the scrubber will function for approximately 10,000 hours, a little over 13 months. If, however, the typical ambient SO2 level of the sample gas is 250 ppb, the scrubber would only last for approximately 4000 hours or about 5 ½ months.

8.1.1.1. Predicting When the SO2 Scrubber Should Be Replaced.

To determine how long the SO2 scrubber will operate efficiently:

1.Measure the amount of SO2 in the sample gas.

If your M102E has the multigas measurement options activated, this can be done by following instructions found in Section 6.8.1 of the M101E Manual (P/N 04740 Rev A) and selecting MEASURE MODE = SO2.

Let the analyzer operate for 30 minutes, then note the SO2 concentration.

2.Divide 1 000 by the SO2 concentration.

EXAMPLE: If the SO2 concentration is 125 ppb:

Operational hours

=

1000 ppm/hr ÷ 0.125 ppm

Operational hours

=

100 000 ppb/hr ÷ 125 ppb

Operational hours

=

8000 hrs

40

05514 Rev A1

Image 46
Contents ADDENDUM TO MODEL 101E OPERATORS MANUAL MODEL 102E TOTAL REDUCED SULFUR ANALYZERMODEL 501 TRS THERMAL CONVERTER withPage 05514 Rev A1 TABLE OF CONTENTSM102E/M501 TRS Addendum to M101E Manual - P/N 04740 Rev A10. TROUBLESHOOTING & REPAIR LIST OF APPENDICES8. INSTRUMENT MAINTENANCE 9. THEORY OF OPERATIONLIST OF TABLES LIST OF FIGURESPREFACE Page 1. PREFACE corner of the display any time the instrument is in SETUP modeUser Notes 1.1. Reference Numbering convention2.1.1. M501-TRS Specifications 2. SPECIFICATIONS, APPROVALS AND WARRANTY2.1. Specifications 2.2. EPA Equivalency Designation2.3. CE Mark Compliance 3.2. Unpacking the M501-TRS 3. GETTING STARTED3.1. Unpacking the M102E Never disconnect electronic circuit boards, wiring harnesses orthat the rack/enclosure itself is adequately ventilated 3.2.1. M501-TRS Ventilation Clearancethe maximum operating temperature specification for the M102E 40C Figure 3-1 M102E Internal Layout 3.3. Internal LayoutsFigure 3-2 M501-TRS Internal Layout M102E INSTRUMENT CHASSIS 3.4. Internal Pneumatic Flow of the M102E & the M501-TRSTable 3-1 TRS - SO2 Switching Valve Operating Modes M501Figure 3-4 M102E Rear Panel Layout 3.5. Rear Panel Layout for the M102E & M501-TRSAlarm Output 5 Amp3.6.1.1. M102E Analog Output Connections 3.6. Initial Setup3.6.1. Electrical Connections Figure 3-6 Analog Output ConnectorM102E PNEMATIC CONNECTERS 3.6.1.2. M501-TRS Alarm Output Connections3.6.2. Pneumatic Connections M501-TRS PNEMATIC CONNECTERSMODEL 102EThe exhaust from the instrument needs to be vented outside the SPAN GAS3.6.2.1. Connections with Internal Valve Options Installed ZERO AIRVENT Gas Dilution CalibratorVENT if input is pressurized Option Valve Option3.7.2. Functional Check of the M102E 3.7. Initial Operation3.7.1. Startup / Warm Up of the M102E Possible Warning Messages at Start-UpProcess Variable High Alarm LED Low Alarm LED3.7.3. Startup / Warm Up of the M501-TRS Display area3.8. Initial Calibration Page 4.2. Calibration Valves Options 4. OPTIONAL HARDWARE AND SOFTWARE4.1. Rack Mount Kits Options 20a, 20b, 21, 22 OPTIONAL HARDWARE AND SOFTWAREZero/Span Valve Operating States M102E INSTRUMENT CHASSIS Table 4-2 IZS Valve Operating States4.3.1. Printed Manuals P/N 4.3. Additional Manuals4.3.2. Addendum on CD Part number Figure 5-1 Analog Output Connector Key 5.1.1. M102E Analog Output Signals5. M102E OPERATING INSTRUCTIONS M102E OPERATING INSTRUCTIONS5.2.1. M102E Analog I/O Configuration 5.2. SETUP - DIAG Using the Diagnostics Functions5.1.2. Setting the M102E Gas Measurement Mode Table 5-1 M102E gas Measurement Modes5.3.1. M102E ID Code 5.3. SETUP - COMM Setting Up the M102E’s Communication Ports5.2.2. M102E Test Channel Output 5.3.2. M102E Ethernet Host NameCONTROL IN 5.4. Remote Operation of the Analyzer5.4.1. Control Inputs ZERO5.4.2.1. M102E Hessen Protocol Gas ID List 5.4.2. Using the M102E with a Hessen Protocol Network5 VDC Power Supply SPAN5.4.2.2. Setting Hessen Protocol Status Flags Table 5-6 Default Hessen Status Bit AssignmentsDO NOT OPERATE WITHOUT THE COVER OF THE M501TS CONVERTER INSTALLED 6. M501-TRS OPERATING INSTRUCTIONS6.1. Basic M501-TRS Controls Teledyne Instruments customer service6.2. To Display The Current Temperature Table 6-1 M501-TRS Temperature Controls and Definitions6.3. To Manually Adjust the Converter Oven Temperature DO NOT SET THE TEMPERATURE HIGHER THAN 1050OC6.4.1. Initiating the Autotune Process 6.4. Autotune the Temperature Controllerhas reached a stable, constant temperature 6.4.2. Aborting the Autotune Process 6.5. M501TRS Alarm Relay Adjustmentnecessary to repeat the autotune procedure Page 7.1. M102E Calibration 7. CALIBRATION PROCEDURESUSER NOTES 7.2. M501-TRS CalibrationPage 8. INSTRUMENT MAINTENANCE INSTRUMENT MAINTENANCE8.1.1.1. Predicting When the SO2 Scrubber Should Be Replaced 8.1. Additional and Updated Maintenance Procedures8.1.1. Maintaining the SO2 Scrubber 8.1.1.2. Checking the Function of the SO2 Scrubber 8.1.1.3. Changing the SO2 Scrubber MaterialPage 9.1.1. TRS Conversion 9. THEORY OF OPERATION9.1. Measurement Principle 9.1.2. SO2 Ultraviolet FluorescenceIa = I0 1 − exp− axSO2 SO2 + hv214nm ⎯⎯Ia⎯→ SO2SO2 * ⎯⎯→ SO2 + hv330nm Figure 9-1 UV Absorption in the M102E Reaction CellkSO2 * ⎯⎯F⎯→ SO2 + hv330nm F = kSO2Equation9-6 9.2.1. UV Lamp Shutter & PMT Offset 9.2. The UV Light Path9.3. Pneumatic Operation 9.3.1. Sample gas Flow9.4.1. Sensor Module PMT HOUSING9.4. Electronic Operation SAMPLE CHAMBERUV LampSample Air Housing Outlet O-Ring O-Ring Seal Seal 9.4.1.1. Sample Chamber9.4.1.2. Sample Chamber Heating Circuit Sample AirHEATER 9.4.2.1. Thermal Switch9.4.2. M501-TRS electronics P-I-D CONTROLLER9.4.2.2. Temperature Alarms and Alarm Output 10.1.1.2. M501-TRS Error Codes 10. TROUBLESHOOTING & REPAIR10.1.1. Fault Diagnosis with Warning Messages 10.1.1.1. M102E Warning MessagesTable 10-2 Test Functions - Possible Causes for Out-Of-Range Values 10.1.2. Fault Diagnosis with Test Functionsfunctioning 10.2.1. TRS Converter Not Heating 10.2. M501-TRS Trouble shooting10.3. Other Performance Problems 10.3.1. Excessive noise10.4.1. Checking the Efficiency of the M501-TRS SO2 Scrubber 10.4. Subsystem Checkout10.4.2. Checking the Efficiency of the M501-TRS TRS Æ SO2 Converter 10.5. Additional Repair Procedures 10.5.1. UV Lamp Adjustment and/or ReplacementLamp Assembly 10.5.1.1. Adjusting the UV Lamp Peaking the LampALWAYS wear UV-Protective, Safety Glasses when working with the UV Always grasp the main body of the lamp10.5.1.2. Replacing the UV Lamp Figure 10-1 Shutter Assembly - Exploded View10.5.2. Replacing the UV filter/lens Figure 10-2 Disassembling the Shutter Assembly10.5.3. Replacing the PMT, HVPS or TEC Figure 10-3 PMT Assembly - Exploded View3. Remove the reaction cell assembly 10.5.4. M102E PMT Hardware Calibration FACTORY CAL 6. Locate the Preamp board see Figure Figure 10-4 Pre-Amplifier Board LayoutAdjust the PMT until NORM PMT equals 1280 mV ± 10 mV 10.5.5. Replacing the TRS Converter Heating TubeIf a reporting range other than 500 ppb is used in this procedure NORM PMT value of twice the ppb value of the span gas EXAMPLEBe Careful 10.6. Manually Programming the M501-TRS Temperature ControllerThe ceramic bobbins at each end of the heater assembly are fragile element off10.6.1. Temperature Controller Primary Menu Parameters 115V/60Hz with a set value of 1000CTable 10-3 - Temperature Controller - Primary Parameter Settings 10.7. Technical Assistance Table 10-4 - Temperature Controller - Primary Parameter SettingsM102E/M501 TRS APPENDIX A-4 Model 102E Signal I/O Definitions APPENDIX A - Version Specific Software DocumentationAPPENDIX A-2 Model 102E Setup Variables Available Via Serial I/O M102E/M501 TRS APPENDIX A - Version Specific Software DocumentationAPPENDIX A-1 M102E Software Menu Trees, Revision A.2 SETUPENTER SETUP PASS APPENDIX A-1 M102E Software Menu Trees, Revision A.2 SAMPLEMSG 1,2 SAMPLETEST CLR 1,3SO2, 111, REPORTED ACAL1TR2, 112, REPORTED Figure A-4 Secondary Setup Menu DIAG SAMPLE ENTER SETUP PASSDIAG Table A-2 APPENDIX A-2 Setup Variables For Serial I/O, Revision A.2Deleted Setup Variables for M102E Software Revision A.2 MEASUREMODETable A-4 Warning Messages deleted from M102 Software Revision A.2 setting of STABILFREQ and STABILSAMPLESAPPENDIX A-3 Warnings and Test Functions, Revision A.2 Table A-6 Test Functions Deleted from M102 Software Revision A.2APPENDIX A-4 M102E Signal I/O Definitions, Revision A.2M102E/M501 TRS APPENDIX A-4 M102E Signal I/O Definitions, Revision A.2Rear board primary MUX analog inputs CTEMPW APPENDIX A-5 M102E iDAS Functions, Revision A.2Trigger Event FunctionA-10 APPENDIX A-5 M102E iDAS Functions, Revision A.2Table B-1 M102E Spare Parts List APPENDIX B - M102E Spare Parts ListAPPENDIX B - M102E Spare Parts List M101E Manual - P/N 04740120 Rev A05516 Rev A TELEDYNE Warranty/Repair Questionnaire Model 102EM102E/M501 TRS INSTRUMENTSTELEDYNE Table D-1 List of Included Electronic Schematics APPENDIX D - ELECTRONIC SCHEMATICSAPPENDIX D - ELECTRONIC SCHEMATICS Addendum to M101E Manual - P/N 04740 Rev AM102E/M501 TRS APPENDIX D - ELECTRONIC SCHEMATICSUser Notes 05518 Rev A