Teledyne 356WA instruction manual Required Equipment, Sample Conditioning, Recorder /Meter Readout

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1 Introduction

Model 356WA

 

 

 

 

1.2Required Equipment

For proper operation, the analyzer may require accessory equipment, particularly in the area of sample conditioning. The need for additional equipment is dictated by the conditions of each application.

1.2.1 Sample Conditioning

The sample must be free of entrained solids and condensable vapors, and be at a relatively constant pressure between 1 and 100 psig. However, more efficient operation is obtained with pressures in the range of 5 to 10 psig. Pressure surges can carry fluid from the humidifier into the cell and impair cell operation. Filters, scrubbers, or pressure regulators are often necessary, depending on local conditions.

1.Filters. If filters are necessary, they should be conveniently located near the analyzer, and installed in a fashion which permits easy removal for periodic cleaning or replacement.

2.Scrubbers. If the sample contains small quantities of acidic

anhydrides (SO2, etc.) or mercaptans (H2S, etc.) they will react with the electrolyte or the cathode, and must be removed. A

caustic scrubber is usually effective.

3.Pressure regulators. While the analyzer will accept pressures to 100 psig, a range of 5 to 10 psig is recommended. In addition, pressure surges can affect instrument operation. In either case, the use of a pressure regulator is advisable. Install the regulator as close to the sample point as possible to reduce sample travel time to a minimium. The regulator should incorporate a metallic diaphragm to prevent the diffusion of atmospheric oxygen into the sample.

1.2.2 Recorder /Meter Readout

The meter installed on the 356WA is either analog or digital. The recorder used for analyzer signal readout is usually of the self-balancing potentiometric type. It should have an input inpedance of 10 Ω or higher. Output is 0 to 1VDC or less (optional: 1 to 5, 4 to 20, or 10 to 50 mADC).

1-2

Teledyne Analytical Instruments

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Contents Trace Oxygen Analyzer Teledyne Analytical InstrumentsModel 356WA Copyright 1999 Teledyne Analytical InstrumentsMaintenance & Troubleshooting Trace Oxygen Analyzer Table of Contents IntroductionInstallation Operational TheoryAppendix Trace Oxygen Analyzer Introduction Method of OperationRequired Equipment Sample ConditioningRecorder /Meter Readout Sensor HumidifierFlow System Flow System Schematic Operational Theory Trace Oxygen Analyzer Installation LocationElectrical Connections Sample Connections Typical System LayoutGND Gas Connections to Back of Analyzer Detector Cell Trace Oxygen Analyzer OperationsFilling the Reservoir Cell PackagingTypical Model 306WA With 2 Alarm Option Cell Installation Cell Compartment Components Throttle Valve Humidity ControlCalibrator Assembly Power Warm-Up and StabilizationCalibration Operations Flowmeter and Humidifier Cell Electrolyte LevelReservoir Electrolyte Replacement CellLead Electrode Cell Assembly Screen Assembly Reservoir and Humidifier ColumnTo Reinstall Removing the Humidifier ColumnLeak Detection Procedure Leak DetectionCell Leak Trace Oxygen Analyzer Teledyne Analytical Instruments Symptom Cause What To Do Symptom Cause What To DoTrace Oxygen Analyzer Maintenance & Troubleshooting Trace Oxygen Analyzer Appendix Specifications Spare Parts List QTY DescriptionTrace Oxygen Analyzer Appendix Drawing ListCalibration Data Calibration ConsiderationsDegrees C = 5 F Degrees K = C + Pmm-Hg = 760 2.50 per 100 ft. of altitude Trace Oxygen Analyzer Appendix Ambient Temperature K Vapor Pressure of Water mm Hg Vapor Pressure of WaterFrom 288-308K