Teledyne 6750 100 mg/Liter 1000 mg/Liter, Ethylene Glycol, Methanol, Ethanol, Acetone, Sucrose

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Total Organic Carbon Analyzer	Setup and Operation

Table 4-1: Preparation of Standards (TOC/TIC)

	ORGANIC COMPOUNDS			100 mg/Liter			1000 mg/Liter
				TOC (AS CARBON)			TOC (AS CARBON)

	Ethylene Glycol			.233 ml/L H20			2.33 ml/L H20
	Methanol			.337 ml/L H20			3.37 ml/L H20
	Ethanol			.242 ml/L H20			2.42 ml/L H20
	Acetone			.204 ml/L H20			2.04 ml/L H20
	Carbon Tetrachloride			.807 ml/L H20			8.07 ml/L H20
	Sucrose			.238 gm/L H20			2.38 gm/L H20
	Urea			.500 gm/L H20			5.00 gm/L H20
	Acetic Acid			.250 gm/L H20			2.50 gm/L H20
	KHP (Potassium acid			.212 gm/L H20			2.12 gm/L H20
	phthalate)

	Glycine			.313 gm/L H20			3.13 gm/L H20
	Sodium Stearate			.141 gm/L H20			1.41 gm/L H20
	Succinic Acid			.246 gm/L H20			2.46 gm/L H20
	Sodium Oxalate			.555 gm/L H20			5.55 gm/L H20

	INORGANIC COMPOUNDS			50 mg/Liter
	INORGANIC COMPOUNDS			TIC (AS CARBON)
				TIC (AS CARBON)

Sodium Carbonate	.442 gm/L H20
Potassium Carbonate	.575 gm/L H20
Ammonium Carbonate	.475 gm/L H20

Add amounts shown (in milliliters or grams) to clean dry, one liter volumetric flask and dilute to one (1) liter with distilled, deionized water.

4.Reagent Preparation:

PREPARATION OF ONE MOLAR SODIUM PERSULFATE SOLUTION (OXIDIZING REAGENT)

Teledyne Analytical Instruments

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Contents Teledyne Analytical Instruments ModelCopyright 2005 Teledyne Instruments/ Analytical Instruments ModelTotal Organic Carbon Analyzer Specific Model InformationSafety Messages Total Organic Carbon Analyzer Table of Contents Maintenance Setup and OperationIndex Teledyne Analytical Instruments AppendixModel 6750 TOC Analyzer Front door removed List of FiguresDC Power Supply Module List of Tables Combustible GAS Usage Introduction Main Features of the AnalyzerTotal Organic Carbon Analyzer Introduction Typical Applications OptionsIntended Use of the Analyzer Introduction ModelModel 6750 TOC Analyzer Front door removed Operator InterfaceIntroduction Model Teledyne Analytical Instruments Overview Theory of OperationBackground Total Organic Carbon Analyzer Theory of OperationNpoc or TOC Direct Method Theory of Operation ModelConclusion TOC Measurement Basics UV/Heated Persulfate Method of Analysis Comparison of TOC Measurement Technologies Sample Handling Subsystems Principles of OperationSample Handling for TOC -Direct Sample Handling TOC-True Inorganic Carbon Removal/Analysis TOC analysis in a continuous, on-line TOC analyzerOxidation Relationship Between TIC and pHOxidation Reactions 10 Model 6750 Ndir Unit Ndir CO2 Gas DetectionElectronic Signal Processing, Display and Control BENCHMARK/AUTO-VALIDATION Theory of Operation Model Teledyne Analytical Instruments Total Organic Carbon Analyzer Installation InstallationUnpacking the Analyzer Mounting the AnalyzerAnalyzer Dimensions Installation ModelElectrical Connections Power ConnectionElectrical Connections to the Model Analog OutputsGas/liquid Connections Alarm Connections4 RS-232 Serial Connection Liquid ConnectionsGas Connections Gas and Liquid Connections to the AnalyzerGas Carrier Connections Checking the SystemInstallation Model Teledyne Analytical Instruments Total Organic Carbon Analyzer Setup and Operation Setup and OperationAnalyzer Startup Drain Connections Setup and Operation ModelMenus Run ModeParameter Menu Alarm Settings Stream Sequencer 5 D/DBPR Detailed Calibration Procedures Ethylene Glycol 100 mg/Liter 1000 mg/LiterMethanol EthanolPreparation of Phosphoric Acid Solution Total Organic Carbon Analyzer Setup and Operation RUN Screen OperationHistorical Data ShutdownSetup and Operation Model Compupter-aided Testing MaintenanceTotal Organic Carbon Analyzer Maintenance Maintenance Model TroubleshootingNdir Gas Calibration Module ServiceIR Calibration Ndir Service Installing Calibration AdapterRemoving the Ndir Unit P/N ST36000 Total Organic Carbon Analyzer Maintenance Maintenance Model To Reassemble Use alternate tightening sequence Removing the Master Interface Board Master Interface Board P/N ST13042-1DC Power Supply Module 4 D. C. Power SupplyReplacing CE Computer CE Computer P/NUV Lamp P/N ST20009 UV Lamp ReplacementRemoving the UV Reactor Assembly UV Reactor Assembly P/N ST20003-1UV Power Supply Mass Flow Controller P/N ST18001A 10 Removing the UV Power SupplyMetering Valve P/N ST16050 11 Mass Flow ControllerSparger P/N ST20025 12 Metering Valve13 Sparger Pumps Maintenance Model 14 Removing the Pump Maintenance Model System Diagnostics 13 4-20 mA Adjustment ProcedureSetting 100 MV Control Voltage Appendix 1SpecificationsTotal Organic Carbon Analyzer Appendix Sample requirements Appendix ModelDescription Image Parts ListingAppendix Model Total Organic Carbon Analyzer Appendix Appendix Model Total Organic Carbon Analyzer Appendix Auto CAL OptionDbpr Option True Dual Range Option not an electronic scalingAppendix Model AS-BUILT Drawings Appendix Model Teledyne Analytical Instruments Total Organic Carbon Analyzer Index IndexModbus Index ModelPump mounting screw Index Model