Teledyne 6750 Model, Copyright 2005 Teledyne Instruments/ Analytical Instruments

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Model 6750

Copyright © 2005 Teledyne Instruments/ Analytical Instruments

All Rights Reserved. No part of this manual may be reproduced, transmitted, transcribed, stored in a retrieval system, or translated into any other language or computer language in whole or in part, in any form or by any means, whether it be electronic, mechanical, magnetic, optical, manual, or otherwise, without the prior written consent of Teledyne Instruments/ Analytical Instruments, 16830 Chestnut Street, City of Industry, CA 91749- 1580.

Warranty

This equipment is sold subject to the mutual agreement that it is warranted by us free from defects of material and of construction, and that our liability shall be limited to replacing or repairing at our factory (without charge, except for transportation), or at customer plant at our option, any material or construction in which defects become apparent within one year from the date of shipment, except in cases where quotations or acknowledgements provide for a shorter period. Components manufactured by others bear the warranty of their manufacturer. This warranty does not cover defects caused by wear, accident, misuse, neglect or repairs other than those performed by TI/AI or an authorized service center. We assume no liability for direct or indirect damages of any kind and the purchaser by the acceptance of the equipment will assume all liability for any damage which may result from its use or misuse.

We reserve the right to employ any suitable material in the manufacture of our apparatus, and to make any alterations in the dimensions, shape or weight of any parts, in so far as such alterations do not adversely affect our warranty.

Important Notice

This instrument provides measurement readings to its user, and serves as a tool by which valuable data can be gathered. The information provided by the instrument may assist the user in eliminating potential hazards caused by his process; however, it is essential that all personnel involved in the use of the instrument or its interface, with the process being measured, be properly trained in the process itself, as well as all instrumentation related to it.

The safety of personnel is ultimately the responsibility of those who control process conditions. While this instrument may be able to provide early warning of imminent danger, it has no control over process conditions, and it can be misused. In particular, any alarm or control systems installed must be tested and understood, both as to how they operate and as to how they can be defeated. Any safeguards required such as locks, labels, or redundancy, must be provided by the user or specifically requested of TI/AI at the time the order is placed.

Therefore, the purchaser must be aware of the hazardous process conditions. The purchaser is responsible for the training of personnel, for providing hazard warning methods and instrumentation per the appropriate standards, and for ensuring that hazard warning devices and instrumentation are maintained and operated properly.

Teledyne Instruments/ Analytical Instruments, the manufacturer of this instrument, cannot accept responsibility for conditions beyond its knowledge and control. No statement expressed or implied by this document or any information disseminated by the manufacturer or its agents, is to be construed as a warranty of adequate safety control under the user’s process conditions.

Teledyne Analytical Instruments

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Contents Model Teledyne Analytical InstrumentsModel Copyright 2005 Teledyne Instruments/ Analytical InstrumentsSpecific Model Information Total Organic Carbon AnalyzerSafety Messages Total Organic Carbon Analyzer Table of Contents Setup and Operation MaintenanceAppendix Index Teledyne Analytical InstrumentsList of Figures Model 6750 TOC Analyzer Front door removedDC Power Supply Module List of Tables Combustible GAS Usage Total Organic Carbon Analyzer Introduction Main Features of the AnalyzerIntroduction Intended Use of the Analyzer OptionsTypical Applications Introduction ModelOperator Interface Model 6750 TOC Analyzer Front door removedIntroduction Model Teledyne Analytical Instruments Background Theory of OperationOverview Total Organic Carbon Analyzer Theory of OperationTheory of Operation Model Npoc or TOC Direct MethodConclusion TOC Measurement Basics UV/Heated Persulfate Method of Analysis Comparison of TOC Measurement Technologies Subsystems Principles of Operation Sample HandlingSample Handling for TOC -Direct Sample Handling TOC-True TOC analysis in a continuous, on-line TOC analyzer Inorganic Carbon Removal/AnalysisRelationship Between TIC and pH OxidationOxidation Reactions Ndir CO2 Gas Detection 10 Model 6750 Ndir UnitElectronic Signal Processing, Display and Control BENCHMARK/AUTO-VALIDATION Theory of Operation Model Teledyne Analytical Instruments Unpacking the Analyzer InstallationTotal Organic Carbon Analyzer Installation Mounting the AnalyzerInstallation Model Analyzer DimensionsPower Connection Electrical ConnectionsAnalog Outputs Electrical Connections to the Model4 RS-232 Serial Connection Alarm ConnectionsGas/liquid Connections Liquid ConnectionsGas and Liquid Connections to the Analyzer Gas ConnectionsChecking the System Gas Carrier ConnectionsInstallation Model Teledyne Analytical Instruments Analyzer Startup Setup and OperationTotal Organic Carbon Analyzer Setup and Operation Setup and Operation Model Drain ConnectionsRun Mode MenusParameter Menu Alarm Settings Stream Sequencer 5 D/DBPR Detailed Calibration Procedures Methanol 100 mg/Liter 1000 mg/LiterEthylene Glycol EthanolPreparation of Phosphoric Acid Solution Total Organic Carbon Analyzer Setup and Operation Operation RUN ScreenShutdown Historical DataSetup and Operation Model Total Organic Carbon Analyzer Maintenance MaintenanceCompupter-aided Testing Troubleshooting Maintenance ModelModule Service Ndir Gas CalibrationIR Calibration Installing Calibration Adapter Ndir ServiceRemoving the Ndir Unit P/N ST36000 Total Organic Carbon Analyzer Maintenance Maintenance Model To Reassemble Use alternate tightening sequence Master Interface Board P/N ST13042-1 Removing the Master Interface Board4 D. C. Power Supply DC Power Supply ModuleCE Computer P/N Replacing CE ComputerUV Lamp Replacement UV Lamp P/N ST20009UV Reactor Assembly P/N ST20003-1 Removing the UV Reactor AssemblyUV Power Supply 10 Removing the UV Power Supply Mass Flow Controller P/N ST18001A11 Mass Flow Controller Metering Valve P/N ST1605012 Metering Valve Sparger P/N ST2002513 Sparger Pumps Maintenance Model 14 Removing the Pump Maintenance Model 13 4-20 mA Adjustment Procedure System DiagnosticsSetting 100 MV Control Voltage Total Organic Carbon Analyzer Appendix 1SpecificationsAppendix Appendix Model Sample requirementsParts Listing Description ImageAppendix Model Total Organic Carbon Analyzer Appendix Appendix Model Total Organic Carbon Analyzer Appendix Option Auto CALTrue Dual Range Option not an electronic scaling Dbpr OptionAppendix Model AS-BUILT Drawings Appendix Model Teledyne Analytical Instruments Index Total Organic Carbon Analyzer IndexIndex Model ModbusPump mounting screw Index Model