Agilent Technologies 5975 manual Carrier and Reagent Gas Requirements

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Carrier and Reagent Gas Requirements

Table 6 lists the specifications for the carrier and reagent gases. Pressures and flows are as measured at the bulkhead fittings on the back of the instrument, not at the gas supply. We recommend that additional shut-off valves be installed near the instruments.

Table 6

Carrier and reagent gas requirements

 

 

 

 

 

 

 

 

 

Purity

Typical pressure range,

Typical flow, mL/min

 

 

 

kPa (psi)

 

 

 

 

 

Helium (required)

99.9995% or better and

345 to 550 (50 to 80)

20 to 50 (column and split flow)

 

 

hydrocarbon-free

 

 

 

 

 

 

Methane reagent gas

Research or SFC grade,

103 to 172 (15 to 25)

1 to 2

(required for CI operation)

99.999%

 

 

 

 

 

 

Isobutane reagent gas

Instrument grade,

103 to 172 (15 to 25)

1 to 2

(optional)

 

99.99%

 

 

 

 

 

 

Ammonia reagent gas

Research or SFC grade,

34 to 55 (5 to 8)

1 to 2

(optional)

 

99.9995%

 

 

 

 

 

 

Carbon dioxide reagent gas

SFC Grade,

103 to 138 (15 to 20)

1 to 2

(optional)

 

99.995%

 

 

 

 

 

 

 

WA R N I N G

Methane is flammable and ammonia is corrosive and toxic. Read and follow the

safety information that comes with the gases.

 

Site Preparation Guide

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Contents Series Mass Selective Detectors U TI O N WA R N I N G Contents Power Cords General Information Instrument Identification Model number Product number Pump type Ionization modeMSD versions Many internal parts of the MSD carry dangerous voltages Important Safety WarningsMany parts are dangerously hot Electrostatic discharge is a threat to MSD electronicsWhen hydrogen gas is supplied to the instrument Hydrogen SafetyChemical Safety Information Safety and Regulatory CertificationsSymbols Sound emission declaration Electromagnetic compatibilityRecycling the Product CleaningSite Preparation Customer responsibility OverviewAgilent responsibility Compliance must exist prior to installationAnalysis Consulting services Other documentation Series MSD Troubleshooting and Maintenance ManualSeries MSD Series GC Computer with monitor Space and Weight RequirementsALS tray Product dimensions Telephone Communications RequirementsSite LAN network Voltage ranges of major components Electrical RequirementsConfiguration Measurement Nominal voltage Power configurationsRequired Power requirementsSupply Outlets Power consumption Product Line voltageSupply Outlets Power consumption Circuit rating Required Power plugs and cordOther electrical considerations Temperature Humidity relative Temperature, humidity, and altitudeAir Conditioning and Environmental Requirements Exhaust venting Airborne dustFume exhaust hood Purity Typical pressure range Typical flow, mL/min KPa psi Carrier and Reagent Gas RequirementsRegulators, tubing, and fittings Laboratory Supply Requirements Cleaning solventsData system supplies Part number Spare parts and consumablesMiscellaneous consumables Commonly used tools Chemical ConsumablesFerrules 5062-3506 Delivery and unloading Receiving the SystemInspecting for damage Unpacking StorageInstallation Installation and VerificationVerification Sensitivity specifications Power Cords Power Cords Page Agilent Technologies