Instruction Manual

748467-A January 2002

Model MicroCEM

Opto-Pneumatic Method

In the opto-pneumatic method, a thermal radiator generates the infrared radiation which passes through the chopper wheel. This radiation alternately passes through the filter cell and reaches the measuring and reference side of the analysis cell with equal intensity. After passing another filter cell, the radiation reaches the pneumatic detector.

The pneumatic detector compares and evaluates the radiation from the measuring and reference sides of the analysis cell and converts them into voltage signals proportional to their respective inten- sity.

The pneumatic detector consists of a gas- filled absorption chamber and a compensation chamber which are connected by a flow channel in which a Microflow filament sensor is mounted. This is shown in Figure 1-2.

In principle the detector is filled with the infrared active gas to be measured and is only sensitive to this distinct gas with its characteristic absorption spectrum. The absorption chamber is sealed with a window which is transparent for infrared ra- diation. The window is usually Calcium Fluoride (CaF2).

Absorption chamber

Flow channel with

Microflow sensor

When the infrared radiation passes through the reference side of the analysis cell into the detector, no pre-absorption occurs. Thus, the gas inside the absorption chamber is heated, expands and some of it passes through the flow channel into the compensation chamber.

When the infrared radiation passes through the open measurement side of the analysis cell into the detector, a part of it is absorbed depending on the gas concentration. The gas in the absorption chamber is, therefore, heated less than in the case of radiation coming from the reference side. Absorption chamber gas becomes cooler, gas pressure in the absorption chamber is reduced and some gas from the compensation chamber passes through the flow channel into the absorption chamber.

The flow channel geometry is designed in such a way that it hardly impedes the gas flow by restriction. Due to the radiation of the chopper wheel, the different radiation intensities lead to periodically repeated flow pulses within the detector.

The Microflow sensor evaluates these flow pulses and converts them into electrical pulses which are processed into the corresponding analyzer output.

CaF2 Window

Compensation chamber

Figure 1-2. Opto-Pneumatic Gas Detector

1-4

Description and Specifications

Rosemount Analytical Inc. A Division of Emerson Process Management