Compaq mar345 ItemDescription First image no, No. of images, Exp. time, Oscillations, Starting ϕ

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mar345 Program Manual

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Table continued from previous page.

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ItemDescription

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First image no.

Image number of first image. Range is 1 through 999.

No. of images

Number of images to be collected. Range is 1 through 999.

Exp. time

Exposure time in seconds. In DOSE mode, the actual time

 

may be different from the desired exposure time.

Oscillations

Number of ϕ− oscillations per image. One oscillation is

 

stronlgy recommended for exposure times < 15 min.

∆ ϕ per image

ϕ movement per image.

Starting ϕ

ϕ position to start data collection.

Distance

Distance crystal to detector.

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For convenience, the program calculates the maximum resolution possible from the chosen distance and the chosen scan mode (image plate diameter).

The image names are created according to the following convention:

directory / root_TYPE_XXX.extension

TYPE is:

not used in Single Data Set mode

1, 2, 3 or 4 in Multiple Data Set mode

INDEX

in Index Crystal mode

A or B

in MAD Data mode

e.g. /images/zeo_001.mar1200 e.g. /images/zeo_1_001.mar1200 e.g. /images/zeo_INDEX_001.mar1200 e.g. /images/zeo_A_001.mar1200

XXX is a three digit image number like 027,

extension is:mar1200, mar1600, mar1800, mar2000, mar2300, mar2400, mar3000 or mar345 for Output format "mar345", depending on the Scan mode chosen.

In Index Crystal mode "First image number" is replaced by "ϕ increment" (see above). The starting image will always be 001 and the following images will have numbers that will be calculated from their ϕ −position relative to image number 001 according to:

XXX = i * ϕ increment / ∆ ϕ + 1

(i=0,1,2,3...)

e.g. with ϕ increment = 90.0 and ∆ ϕ = 2.0, XXX = 1, 46, 91,

136, etc.

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Contents Mar research All Rights Reserved Mar345 Program Manual Version February 24Contents Introduction Computer RequirementsEnvironment Running mar345 Command LineOutput Files Input FilesMar.lp Basic Concepts and RulesMar.log Mar.spyStarting Up User Interface Main WindowMenu Bar Windows Submenu Menu BarScanner Status Area Scanner Command Area Editing Data Collection Parameters Directory Scan modeCollect mode ItemDescription TitleOscillations ItemDescription First image noNo. of images Exp. timeWavelength variable Loading and Saving Data Collection Parameters Moving Distance and Phi Stopping Data Collection Starting Data CollectionSingle Scan Shutter TimerHardware Status Getting Help14 X−ray Setup Errors and Warnings Display Window Image DisplayShow/Hide statistics Options SubmenuFiles ColorsNext image Reset colorsDo not/Keep color scales Turn On/Off 3D−plotImage Area Mar345 Program Manual Zoom Buttons Work AreaInformation Areas Load ButtonsRainbow Window TitleColors Window Blue scalesMax MinCross−Section Window No. of peaksMessage area Lower horizontal axis Moved using the right mouse buttonVertical axis Upper horizontal axisStrategies Data CollectionImageroot.html Checking ParametersEnd of Data Collection Imageroot.SUMMARYReason TroubleshootingNo. Description MessageTabel from previous 1101 Appendix Configuration File Calibration Files