Teledyne 200AH 7.12. Recommendations for CEM Applications

Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2

7-14

Table 7-12: Converter Efficiency - Automatic Calculation

Step

Number Action Comment

1. Preparation Make sure a calibration is completed before setting up

Converter efficiency.

2. Press

CAL-CONC-CON-NO2 Enter the expected NO2 concentration, then press ENTR.

3. Input a known

concentration of NO2

calibration gas.

Allow reading to stabilize for 10 minutes.

4. Press CAL-ENTR By pressing ENTR the M200AH will calculate the ratio of

the observed to expected NO2 and will use that ratio to

compensate future NO2 readings. The calculated value can be

seen by pressing the SET button.

NOTE: The CAL button will come on only if the Instrument is

measuring NO2 gas and ratio is between the limits of 0.80 - 1.20.

5. Press EXIT EXIT will return instrument to SAMPLE mode.

Method 2. If the converter efficiency is determined by some external means, the value can be

directly entered. Press CAL-CONC-CON-SET, then key in the ratio and press ENTR, then

EXIT.

7.12. Recommendations for CEM Applications

7.12.1. Calibration Gasses

The following is our recommendation for calibration gasses and equipment for the M200AH.

Regulator Specifications:

Ultra high purity, two-stage stainless steel body with stainless steel diaphragms, Tefzel and

Teflon seats and seals, CGA 660 type. Gauges are 0-4000 psig inlet with 0-100 psig outlet.

Nitric Oxide Calibration Gas specifications:

Use NO in nitrogen, EPA protocol 1, NIST traceable (long lead item, order early) for CEMS

Certification Test gas and acid rain applications.

Use NO in nitrogen at 80% of calibration range  2% for routine calibration.

Example: Order 80 ppm NO in N2 if calibrating the 0-100 ppm range.

Contents

Main INSTRUCTION MANUAL MODEL 200AH NITROGEN OXIDES ANALYZER Page SAFETY MESSAGES Page Table of Contents 3. SPECIFICATIONS, WARRANTY.................................................................. 3-1 4. THE M200AH NOX ANALYZER................................................................... 4-1 6. OPTIONAL HARDWARE AND SOFTWARE................................................ 6-1 7. CALIBRATION AND ZERO/SPAN CHECKS ...............................................7-1 9. TROUBLESHOOTING AND ADJUSTMENTS.............................................. 9-1 Page Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 vii LIST OF FIGURES Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 viii LIST OF TABLES Page Page 1. HOW TO USE THIS MANUAL Page 2. GETTING STARTED 2.1. Unpacking 2.2. Electrical and Pneumatic Connections Page Page Page Page Page 2.3. Initial Operation Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 2-8 Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 2-9 Step 2 - Calibrate the instrument for NOX: Zero/Span Calibration Procedure Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 2-10 Zero/Span Calibration Procedure (Continued) Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 2-11 Step 3 - Review Quality of calibration: Calibration Quality Check Procedure Step 4 - The M200AH is now ready to measure sample gas. Page Page Page Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 2-15 Table 2-1: Final Test and Calibration Values (table continued) Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 2-16 Table 2-1: Final Test and Calibration Values (Continued) Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 3-1 3. SPECIFICATIONS, WARRANTY 3.1. Specifications NOX Specifications O2 Option 3.2. Warranty 4. THE M200AH NOX ANALYZER 4.1. Principle of Operation 4.1.1. NOX Measurement hv NO * NO 4.1.2. Oxygen Measurement (Option) Page Page 4.2. Operation Summary 4.2.1. NOX Sensor Module, Reaction Cell, Detector 4.2.2. Oxygen Sensor Module (Option) 4.2.3. Pneumatic Sensor Board 4.2.4. Computer Hardware and Software 4.2.5. V/F Board 4.2.6. Front Panel 4.2.7. Power Supply Module 4.2.8. Pump, Valves, Pneumatic System Page Page 4.2.9. Ozone Generator 4.2.10. NO2 - NO Converter Page 5. SOFTWARE FEATURES 5.1. Index to Front Panel Menus Page Page Page Page Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 5-6 5.1.1. Sample Menu Table 5-1: M200AH Sample Menu Structure Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 5-7 5.1.2. Set-Up Menu Table 5-2: M200AH Setup Menu Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 5-8 Table 5-2: M200AH Setup Menu (Continued) Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 5-9 Table 5-3: M200AH Setup Menu Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 5-10 Table 5-4: M200AH Setup Menu 5.2. Sample Mode 5.2.1. Test Functions Page Page Page 5.2.2. CAL, CALS, CALZ, Calibration Functions Page 5.3. Set-Up Mode 5.3.1. Configuration Information (CFG) 5.3.2. Automatic Calibration (AutoCal) 5.3.3. Data Acquisition System (DAS) Page 5.3.4. Range Menu Page Page 5.3.5. Password Enable 5.3.6. Time of Day Clock 5.3.7. Diagnostic Mode Page 5.4. M200AH Operating Modes 5.4.1. NO/NOx/NO2 Switching Mode 5.4.2. NOX Only Mode 5.4.3. NO Only Mode 5.5. 4-20 mA Current Loop 5.6. Status Output 5.7. RS-232 Interface 5.7.1. Setting up the RS-232 Interface Page Page 5.7.2. Command Summary Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 5-32 Table 5-12: RS-232 Command Summary Page Page Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 5-35 5.7.3. TEST Commands and Messages Table 5-15: RS-232 Test Messages 5.7.4. WARNING Commands and Messages 5.7.5. CALIBRATION Commands and Messages 5.7.6. DIAGNOSTIC Commands and Messages 5.7.7. DAS Commands and Messages Page 5.7.8. VARIABLES Commands and Messages Page 6. OPTIONAL HARDWARE AND SOFTWARE 6.1. Rack Mount Options 6.2. Zero/Span Valves Option Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 6-3 6.2.1. Autocal - Setup Zero/Span Valves Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 6-4 Table 6-3: Action of MODE Field in AutoCal 6.3. Oxygen Sensor Option 6.4. Isolated 4-20 mA Current Loop Option 6.5. Molybdenum Converter Option 6.6. External Desiccant Canister Option 6.7. Alternate Bypass Flow Orifice Option 6.8. M501 External Converter Option Page 7. CALIBRATION AND ZERO/SPAN CHECKS Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 7-2 Table 7-1: Types of Zero/Span Check and Calibration 7.1. Manual NOX Zero/Span Check or Cal With Zero/Span Gas in the Sample Port Page Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 7-5 Table 7-4: Manual Span Calibration Procedure - Span Gas Thru Sample Port 7.2. Manual O2 Zero/Span Check or Cal With Zero/Span Gas in the Sample Port 7.3. Manual Zero/Span Check with Zero/Span Valves Option Page 7.4. Dynamic Zero/Span Calibration Using AutoCal 7.5. Use of Zero/Span Valves with Remote Contact Closure 7.6. NO Only Mode Calibration 7.7. NOX Only Mode Calibration 7.8. Calibration Requirements for AutoRange or Remote Range 7.9. Calibration Requirements for Independent Range 7.10. Calibration Quality 7.11. Converter Efficiency Compensation 7.12. Recommendations for CEM Applications 7.12.1. Calibration Gasses 7.12.2. Calibration Frequency 7.12.3. Converter Efficiency Page 8. MAINTENANCE 8.1. Maintenance Schedule 8.2. Replacing the Sample Particulate Filter Page 8.3. Replacing the Converter Page 8.4. Cleaning the Reaction Cell Page Page 8.5. Pneumatic Line Inspection Page Page Page 8.6. Leak Check Procedure 8.7. Light Leak Check Procedure 8.8. Prom Replacement Procedure 9. TROUBLESHOOTING AND ADJUSTMENTS 9.1. Operation Verification - Diagnostic Techniques 9.1.1. Fault Diagnosis with TEST Variables Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 9-3 Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 9-4 Table 9-1: Test Functions (Continued) Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 9-5 Table 9-1: Test Functions (Continued) Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 9-6 Table 9-1: Test Functions (Continued) Test Function Factory Set-Up Comment Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 9-7 Table 9-1: Test Functions (Continued) Test Function Factory Set-Up Comment 9.1.2. Fault Diagnosis with WARNING Messages Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 9-9 Table 9-2: Front Panel Warning Messages 9.1.3. Fault Diagnosis using DIAGNOSTIC Mode Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 9-11 Table 9-3: Summary of Diagnostic Modes Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 9-12 9.1.3.1. Signal I/O Diagnostics Table 9-4: Diagnostic Mode - Signal I/O Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 9-13 Table 9-4: Diagnostic Mode - Signal I/O (Continued) Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 9-14 Table 9-4: Diagnostic Mode - Signal I/O (Continued) Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 9-15 Table 9-4: Diagnostic Mode - Signal I/O (Continued) Page 9.1.4. M200AH Internal Variables Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 9-18 Table 9-5: Model 200AH Variables Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 9-19 9.1.5. Test Channel Analog Output 9.1.6. Factory Calibration Procedure Page Page Page 9.2. Performance Problems 9.2.1. AC Power Check 9.2.2. Flow Check 9.2.3. No Response to Sample Gas 9.2.4. Negative Output 9.2.5. Excessive Noise 9.2.6. Unstable Span 9.2.7. Unstable Zero 9.2.8. Inability to Span 9.2.9. Inability to Zero 9.2.10. Non-Linear Response 9.2.11. Slow Response 9.2.12. Analog Output Doesn't Agree With Display Concentration 9.3. Subsystem Troubleshooting and Adjustments 9.3.1. Computer, Display, Keyboard Page Page 9.3.2. RS-232 Communications Page Page 9.3.3. Voltage/Frequency (V/F) Board Page Page Page Page Page 9.3.4. Status/Temp Board Page 9.3.5. Power Supply Module Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 9-46 Table 9-9: Power Supply Module Subassemblies Page Page 9.3.6. Ozone Generator Page Page Page 9.3.7. Flow/Pressure Sensor Page Page Page Page 9.3.8. NOX Sensor Module Page Page Page Page 9.3.9. Z/S Valves 9.3.10. Pneumatic System Teledyne API Model 200AH NOX Analyzer Instruction Manual, 06492, Rev. G2 A-1 APPENDIX A ELECTRICAL SCHEMATICS Table A-1: Electrical Schematics Page APPENDIX B SPARE PARTS AND EXPENDABLES Page Page SPARE PARTS LIST LEVEL 1 SPARES KIT (WITH MINI-HICON CONVERTER) LEVEL 1 SPARES KIT (WITH MOLYBDENUM CONVERTER)