Hach 3654 Portable H2/N2 Analyzer manual Installation, What you have Received

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3654 Portable H2/N2 Analyzer - Installation

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1 Installation

This section provides necessary information to set up the instrument. If you have any questions or experience any difficulties, do not hesitate to contact your Hach Ultra representative regarding this procedure.

1.1 What you have Received

The ORBISPHERE 3654 portable analyzer includes the following major components:

An instrument, model 3654/xxx, with keypad, display, and handle.

A membrane-covered thermal conductivity (TC) sensor, either model 3127x for H2 measurement or model 31570 for N2 measurement.

A flow chamber, either model 32013A with flow adjustment valve for N2 analyzers, or model 32015 without flow adjustment valve for H2 analyzers.

A WIN3654 program on a CD with a PC communications cable.

Also included with your shipment are two C-type batteries, a recharge kit in a plastic case containing materials to maintain your sensor and a model 32824A refilling hose to refill the purge gas cylinder

Fig 1-1:ORBISPHERE 3654 Portable Analyzer

Locate the instrument close to the sample being analyzed, and to the Personal Computer (PC) if one is being used. A LEMO-6 connector for RS-232 serial output to a PC is on the right side of the instrument (see Fig 1-1above).

Make sure you install a fully charged set of batteries, or connect the instrument to an external power source (see “External Power Supply (optional)” on page 11), before switching the instrument on and exposing the sensor’s membrane to any liquid.

Operator Manual

ORBISPHERE

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Contents Operator Manual Page Product Recycling Information Orbisphere Following only applies to European customers Product DisposalRestriction of Hazardous Substances Board Analog Board Spacer External ConnectorTable of Contents Accessories and Attachments Maintenance and TroubleshootingCalibrations Specifications Part ListsAppendix a Glossary Table of Contents 3654 Portable H2/N2 Analyzer Revision History Safety ConventionsManual Overview About this ManualSafety Precautions Safety RecommendationsService and Repairs Acknowledgements Precautionary LabelsOrbisphere What you have Received InstallationWIN3654 PC Program Installation Sensor InstallationAtmospheric Pressure Equilibrium Instrument PC Connection External Power Supply optionalPurge Gas Connection ConnectionsPin RS232 Signal Use Flow Chamber Installation Installation Completion Check List Dissolved Gas Measurements Flow ChamberOrbisphere Operating Controls Operating InstructionsMeasurement Phase on Select Gas Measurement Phase Measurement ModeTaking Measurements Automatic Data Acquisition Storing Measurements In the InstrumentManual Data Acquisition Storing and Accessing Measurements From a Computer Viewing Stored MeasurementsDownloading Stored Values Altering the Sampling Point Descriptions Copying ValuesSaving Values Clearing Stored Values Printing ValuesTimebase Updating Rate Maximum Samples 10 divisions Monitoring Measurements In Real-TimeAfter Use and Storage Main Menu Basics Options SetupOptions Setup 3654 Portable H2/N2 Analyzer Analyzer PC Connection Reviewing Instrument ConfigurationConfiguring the Instrument Gas Measurement PhaseMeasurement Units Membrane Selection Automatic Data Acquisition Setting Sampling IntervalsCalibration Medium Locking Out the Instrument’s CAL ButtonRolling Average Automatic Shutdown Orbisphere Barometric Pressure Sensor Calibration CalibrationsCalibration Method Time Benefits Drawbacks Reference Sensor CalibrationCalibration Setup Calibration In H2 or N2 at Atmospheric Pressure Calibration In H2 or N2 at Elevated Pressure Calibrating In a Liquid H2 or N2 Solution Model 32311 Flow Meter Accessories and AttachmentsModel 32939 External Power Supply Maintenance Schedule Maintenance and TroubleshootingPower Supply Sensor MaintenanceMembrane Replacement Mounting Dual MembranesRemoving the Membrane Installing the Membrane Orbisphere Place the membrane holding ring on the installation tool tip 1 N2 Purge Gas Purge Gas Cylinder RefillFilling the Purge Gas Cylinder 2 CO2 Purge GasTroubleshooting Instrument Serial TestKeyboard Test Display Test Clock SettingsMeasurements View Analog Voltages ViewContinuous Purge Troubleshooting OperationDiagnostics Messages Program IdentificationSymptom Cause Possible Solution Troubleshooting TableInstrument Specifications SpecificationsSensor Type 31 270 H Sensor SpecificationsPFA Etfe Ectfe Sensor Type 31 272 H 31 570 NSpecifications 3654 Portable H2/N2 Analyzer Analyzer Spare Parts Instrument ConfigurationsTC Sensor and Parts on Configured System Part ListsSensor Spare Parts Unit Appendix a GlossaryCommon Units Terms and DefinitionsGlossary 3654 Portable H2/N2 Analyzer Tables and Illustrations AnnexAnnex 3654 Portable H2/N2 Analyzer User Notes