Hach Membrane Monitoring and Maintenance for Optimal Performance

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Maintenance and Troubleshooting - 3654 Portable H2/N2 Analyzer

 

 

6.2.3 Mounting Dual Membranes

In order to prevent unwanted stretching of the membrane on a hydrogen sensor it is recommended to simultaneously mount a support membrane beneath the primary membrane.

The primary membrane, or top membrane, determines the rate at which the H2 gas enters the measurement chamber of the sensor. The secondary membrane, or support membrane on the bottom, is extremely permeable and is installed to stabilize the position of the primary membrane.

Two primary membrane types are used for H2 measurement depending on the type of application:

29561A - used for waste gas, off gas and dH2 in a boiling water reactor

2952A - used for dH2 in reactor cooling systems of a pressurized water reactor.

The support or secondary membrane for all H2 measurement applications is the 29562A.

As two membranes will be mounted together, the mounting ring used must be part number 29229 which is designed for a thickness of 50 microns or more. Mounting ring part number 29228 is designed for a single membrane and should not be used for mounting dual membranes.

6.3Membrane Replacement

Note:

After replacing a membrane, the sensor must always be re-calibrated. Allow the sensor to settle for 30 minutes in measurement phase to allow measurements to stabilize, before performing the sensor calibration.

6.3.1 Removing the Membrane

It is recommended to leave the sensor in place in the instrument when changing the membrane. It is not necessary to remove it.

To remove the membrane, follow the steps below:

First remove the flow chamber from the sensor by turning the flow chamber locking pin (see position in Fig 1-1 on page 9) counter-clockwise and gently lifting the flow chamber off the sensor.

CAUTION:

A thermistor at the top of the sensor (illustrated right) is used to measure the sample temperature. Do not bend or damage this component by trying to twist the flow chamber off the sensor.

ORBISPHERE

Operator Manual

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Contents Operator Manual Page Product Recycling Information Orbisphere Product Disposal Following only applies to European customersBoard Analog Board Spacer External Connector Restriction of Hazardous SubstancesTable of Contents Calibrations Accessories and AttachmentsMaintenance and Troubleshooting Appendix a Glossary SpecificationsPart Lists Table of Contents 3654 Portable H2/N2 Analyzer About this Manual Safety ConventionsManual Overview Revision HistoryService and Repairs Safety PrecautionsSafety Recommendations Precautionary Labels AcknowledgementsOrbisphere Installation What you have ReceivedAtmospheric Pressure Equilibrium WIN3654 PC Program InstallationSensor Installation Connections External Power Supply optionalPurge Gas Connection Instrument PC ConnectionPin RS232 Signal Use Flow Chamber Installation Installation Completion Check List Flow Chamber Dissolved Gas MeasurementsOrbisphere Operating Instructions Operating ControlsMeasurement Phase on Taking Measurements Select Gas Measurement PhaseMeasurement Mode Storing Measurements In the Instrument Automatic Data AcquisitionManual Data Acquisition Downloading Stored Values Storing and Accessing Measurements From a ComputerViewing Stored Measurements Saving Values Altering the Sampling Point DescriptionsCopying Values Printing Values Clearing Stored ValuesMonitoring Measurements In Real-Time Timebase Updating Rate Maximum Samples 10 divisionsAfter Use and Storage Options Setup Main Menu BasicsOptions Setup 3654 Portable H2/N2 Analyzer Gas Measurement Phase Reviewing Instrument ConfigurationConfiguring the Instrument Analyzer PC ConnectionMeasurement Units Automatic Data Acquisition Setting Sampling Intervals Membrane SelectionRolling Average Calibration MediumLocking Out the Instrument’s CAL Button Automatic Shutdown Orbisphere Calibrations Barometric Pressure Sensor CalibrationSensor Calibration Calibration Method Time Benefits Drawbacks ReferenceCalibration Setup Calibration In H2 or N2 at Atmospheric Pressure Calibration In H2 or N2 at Elevated Pressure Calibrating In a Liquid H2 or N2 Solution Accessories and Attachments Model 32311 Flow MeterModel 32939 External Power Supply Sensor Maintenance Maintenance and TroubleshootingPower Supply Maintenance ScheduleRemoving the Membrane Membrane ReplacementMounting Dual Membranes Installing the Membrane Orbisphere Place the membrane holding ring on the installation tool tip Purge Gas Cylinder Refill 1 N2 Purge Gas2 CO2 Purge Gas Filling the Purge Gas CylinderKeyboard Test Troubleshooting InstrumentSerial Test Clock Settings Display TestAnalog Voltages View Measurements ViewProgram Identification Troubleshooting OperationDiagnostics Messages Continuous PurgeTroubleshooting Table Symptom Cause Possible SolutionSpecifications Instrument SpecificationsSensor Specifications Sensor Type 31 270 HSensor Type 31 272 H 31 570 N PFA Etfe EctfeSpecifications 3654 Portable H2/N2 Analyzer Part Lists Instrument ConfigurationsTC Sensor and Parts on Configured System Analyzer Spare PartsSensor Spare Parts Terms and Definitions Appendix a GlossaryCommon Units UnitGlossary 3654 Portable H2/N2 Analyzer Annex Tables and IllustrationsAnnex 3654 Portable H2/N2 Analyzer User Notes