Hach 3654 Portable H2/N2 Analyzer manual Calibrations, Accessories and Attachments

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2 of 66Table of Contents - 3654 Portable H2/N2 Analyzer

 

 

3.4.2

Measurement Units

30

 

 

3.4.3

Membrane Selection

31

 

 

3.4.4

Automatic Data Acquisition - Setting Sampling Intervals .....31

 

 

3.4.5

Calibration Medium

32

 

 

3.4.6 Locking Out the Instrument’s CAL Button

32

 

 

3.4.7

Rolling Average

32

 

 

3.4.8

Automatic Shutdown

33

 

 

3.4.9

Measurement Mode

33

4

Calibrations

 

 

 

4.1

Barometric Pressure Sensor Calibration

35

 

4.2

Sensor Calibration

36

 

 

4.2.1

Calibration Setup

37

 

 

4.2.2 Calibration In H2 or N2 at Atmospheric Pressure

38

 

 

4.2.3 Calibration In H2 or N2 at Elevated Pressure

39

 

 

4.2.4 Calibrating In a Liquid H2 or N2 Solution

40

5

Accessories and Attachments

 

 

5.1

Model 32311 Flow Meter

41

 

5.2

Model 32939 External Power Supply

42

6

Maintenance and Troubleshooting

 

 

6.1

Power Supply

43

 

6.2

Sensor Maintenance

43

 

 

6.2.1

Maintenance Schedule

43

 

 

6.2.2 Testing the Sensor Condition

43

 

 

6.2.3

Mounting Dual Membranes

44

 

6.3

Membrane Replacement

44

 

 

6.3.1

Removing the Membrane

44

 

 

6.3.2

Installing the Membrane

45

 

6.4

Purge Gas Cylinder Refill

48

 

 

6.4.1

N2 Purge Gas

48

 

 

6.4.2

CO2 Purge Gas

49

 

 

6.4.3 Filling the Purge Gas Cylinder

49

 

6.5

Troubleshooting - Instrument

50

 

 

6.5.1

Serial Test

50

 

 

6.5.2

Keyboard Test

50

 

 

6.5.3

Display Test

51

 

 

6.5.4

Clock Settings

51

 

 

6.5.5

Analog Voltages View

52

 

 

6.5.6

Measurements View

52

 

6.6

Troubleshooting - Operation

53

 

 

6.6.1

Program Identification

53

 

 

6.6.2

Diagnostics Messages

53

 

 

6.6.3

Continuous Purge

53

 

 

6.6.4

Troubleshooting Table

54

 

 

 

 

 

ORBISPHERE

 

 

 

Operator Manual

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Contents Operator Manual Page Product Recycling Information Orbisphere Product Disposal Following only applies to European customersBoard Analog Board Spacer External Connector Restriction of Hazardous SubstancesTable of Contents Calibrations Accessories and AttachmentsMaintenance and Troubleshooting Appendix a Glossary SpecificationsPart Lists Table of Contents 3654 Portable H2/N2 Analyzer Safety Conventions Manual OverviewAbout this Manual Revision HistoryService and Repairs Safety PrecautionsSafety Recommendations Precautionary Labels AcknowledgementsOrbisphere Installation What you have ReceivedAtmospheric Pressure Equilibrium WIN3654 PC Program InstallationSensor Installation External Power Supply optional Purge Gas ConnectionConnections Instrument PC ConnectionPin RS232 Signal Use Flow Chamber Installation Installation Completion Check List Flow Chamber Dissolved Gas MeasurementsOrbisphere Operating Instructions Operating ControlsMeasurement Phase on Taking Measurements Select Gas Measurement PhaseMeasurement Mode Storing Measurements In the Instrument Automatic Data AcquisitionManual Data Acquisition Downloading Stored Values Storing and Accessing Measurements From a ComputerViewing Stored Measurements Saving Values Altering the Sampling Point DescriptionsCopying Values Printing Values Clearing Stored ValuesMonitoring Measurements In Real-Time Timebase Updating Rate Maximum Samples 10 divisionsAfter Use and Storage Options Setup Main Menu BasicsOptions Setup 3654 Portable H2/N2 Analyzer Reviewing Instrument Configuration Configuring the InstrumentGas Measurement Phase Analyzer PC ConnectionMeasurement Units Automatic Data Acquisition Setting Sampling Intervals Membrane SelectionRolling Average Calibration MediumLocking Out the Instrument’s CAL Button Automatic Shutdown Orbisphere Calibrations Barometric Pressure Sensor CalibrationSensor Calibration Calibration Method Time Benefits Drawbacks ReferenceCalibration Setup Calibration In H2 or N2 at Atmospheric Pressure Calibration In H2 or N2 at Elevated Pressure Calibrating In a Liquid H2 or N2 Solution Accessories and Attachments Model 32311 Flow MeterModel 32939 External Power Supply Maintenance and Troubleshooting Power SupplySensor Maintenance Maintenance ScheduleRemoving the Membrane Membrane ReplacementMounting Dual Membranes Installing the Membrane Orbisphere Place the membrane holding ring on the installation tool tip Purge Gas Cylinder Refill 1 N2 Purge Gas2 CO2 Purge Gas Filling the Purge Gas CylinderKeyboard Test Troubleshooting InstrumentSerial Test Clock Settings Display TestAnalog Voltages View Measurements ViewTroubleshooting Operation Diagnostics MessagesProgram Identification Continuous PurgeTroubleshooting Table Symptom Cause Possible SolutionSpecifications Instrument SpecificationsSensor Specifications Sensor Type 31 270 HSensor Type 31 272 H 31 570 N PFA Etfe EctfeSpecifications 3654 Portable H2/N2 Analyzer Instrument Configurations TC Sensor and Parts on Configured SystemPart Lists Analyzer Spare PartsSensor Spare Parts Appendix a Glossary Common UnitsTerms and Definitions UnitGlossary 3654 Portable H2/N2 Analyzer Annex Tables and IllustrationsAnnex 3654 Portable H2/N2 Analyzer User Notes