Agilent Technologies G6600-90006 manual Index

Page 117

Index

C

Calibration of Flow Sensor, 88

Ceramic Tube Replacement, 98

Column Insertion Distance, 61

D

Detection Limits, 76 Detector

cleaning, 83

display output controls, 65 initial check, 69 operating conditions, 75 operation, 73

power controls, 64 schematic, NCD, 36

schematic, NCD (nitrosamine mode), 37 schematic, SCD, 35

shut down, 77 signal controls, 65 start-up procedure, 72

Dry Piston Pump installation, 52

Dual Plasma Burner assembling for NCD, 95 assembling for SCD, 90

cross-section illustration for NCD, 27 cross-section illustration for SCD, 26 installing, 59

overview, 25

tube replacement for NCD, 102 tube replacement for SCD, 98

Dual Plasma Controller controls and settings, 66 front panel illustration, 66 installing, 60 operating conditions, 75 overview, 24

rear panel illustration, 60

E

Edwards oil-sealed pump ballast position, 51 installation, 46

F

FID Adapter

overview, 33

Flow Sensor Calibration, 88

Fluidics overview, 42 Fuses

replacing, 107, 108

I

Installation

column connections, 61 Dry piston pump, 52 Dual Plasma Burner, 59 Dual Plasma Controller, 60 Edwards oil-sealed pump, 46 gases, 42, 43

initial connections, 46 overview, 40 oxidant supply, 57 power requirements, 41 required tools, 45 selecting a location, 41 signal output cables, 58 transfer line, 62 Vacuum Pump, 46 Welch dry piston pump, 52

M

Maintenance

changing oil mist filter, 84 cleaning the detector, 83 pump, 82

Minimum Detection Limit (MDL), 89

O

Operating Conditions, 75

Ozone Generator

overview, 28

troubleshooting, 109

P

Pressure Regulator, use of, 43

Q

Quartz Tube Replacement, 102

R

Recorder test, 68

S

Schematic for NCD, 36

for NCD (nitrosamine mode), 37 for SCD, 35

Sensitivity

minimum detection limit, 89 NCD specifications, 20 SCD specifications, 20

Sensor Calibration, 88 Shut-down procedure, 77 Signal Output Cables

installation, 58 Special Operating Modes

nitrosamine, 78

nonhydrocarbon gaseous samples, 78 Specifications, 20

Start-up Procedure, 72 System schematic, 42 System Stabilization, 73 System Startup, initial, 67

T

Temperature

set-point vs. thermocouple reading, 112 Theory of Operation, 23 Troubleshooting

burner issues, 116 detector, 106 detector issues, 113 general problems, 113 ozone, 109

power and fuses, 107, 108 pump issues, 115

table of problems and causes, 113 Tube Replacement

for NCD, 102 for SCD, 98

V

Vacuum Pump overview, 32

W

Welch Dry Piston Pump installation, 52 operation notes, 53

Operation and Maintenance Manual

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Contents Operation and Maintenance Manual Safety Notices WarrantyAcknowledgements Manual Part NumberWA R N I N G EnglishIs not in use Español Français Deutsch Italiano Veiligheidsvoorzieningen niet meer DutchFollowing symbols are used on the equipment Contents Overview InstallationOperation Front Panel Controls and Initial StartupPump Maintenance MaintenanceIndex TroubleshootingOperation and Maintenance Manual Introduction Operation and Maintenance Manual System Description Specifications Technical Information 355 SCDTechnical Information 255 NCD Power requirements Physical SpecificationsVoltage Theory of Operation Sulfur Chemiluminescence DetectorNitrogen Chemiluminescence Detector Dual Plasma Burner with the 355 SCD Dual Plasma ControllerDual Plasma Burner Description of Major ComponentsCross-Section of the Dual Plasma Burner for the 355 SCD Cross-Section of the Dual Plasma Burner for the 255 NCD Chemiluminescence Reaction Cell and Photomultiplier Tube Ozone Generator355 SCD Left Side 355 SCD Right Side 255 NCD Left Side View Vacuum Pump Pressure TransducerOil Coalescing Filter Chemical TrapFID Adapter Optional NCD Reaction CellNCD Photomultiplier Tube and Cooler Schematic for 355 SCD Schematic for 255 NCD, in Nitrogen Mode Schematic for 255 NCD, in Nitrosamine Mode Operation and Maintenance Manual Installation Overview Selecting a Location Power RequirementsCombustion Gas Requirements Environmental ConsiderationsTwo-stage pressure regulators Venting Gases Unpack and Inspect the Instrument Required Installation ToolsInstalling the Edwards RV5 Pump Oil-Sealed Vacuum Pump Set Up the Vacuum PumpWA R N I N G Ard RV5 Oil-Sealed Vacuum Pump and Associated Traps Front Side RV5 Oil- Sealed Vacuum Pump and Associated Traps Top Setting the Gas Ballast Position RV5 Installing the Welch Dry Piston Vacuum Pump Operation Notes Welch Pump Welch Dry Piston Pump Operation and Maintenance Manual SCD 230 V Unit Rear Panel Diagram Connect the Power CordInstall the Dry Compressed Air or O2 Supply Install the Signal Output Cables Additional information Install the Dual Plasma BurnerDual Plasma Controller Rear Panel Install the Dual Plasma ControllerInstall Column Connections Capillary ColumnsPacked Columns and Columns with an Outside Diameter 0.8 mm Install the Transfer Line Front Panel Controls and Initial Startup Detector Front Panel Controls Power ControlsDisplay Output Controls Signal ControlsDual Plasma Controller Front Panel Dual Plasma Controller ControlsVacuum Test Initial StartupRecorder Test Initial Checkout Detector Interface SetupIgnition Operation Start-Up Procedure Detector Stability and Response Detector OperationColumn Bleed CokingFluctuating Pressures Contaminated GasesTypical Operating Conditions Typical Operating ConditionsExpected Detection Limits for Chromatographic Conditions Detection LimitsInstrument Shut-Down Daily ShutdownComplete Shutdown Special Operating Modes Using the 255 NCD in Nitrosamine ModeOperation and Maintenance Manual Operation and Maintenance Manual Maintenance Operating Life of Components for Edwards RV5 Vacuum Pump Pump MaintenanceCleaning the Detector Changing the Oil Mist Filter RV5 Equipment Reaction Cell CleaningReaction Cell, PMT Housing and PMT Socket WA R N I N G Flow Sensor Calibration MDL Detector SensitivitySCD Proper Ferrule Orientation to the Large Ceramic Tube Orientation of the Double Taper Ferrule Tightening the Heater Swivel Nut Operation and Maintenance Manual NCD Proper Ferrule Orientation to the Large Quartz Tube Burner Assembly Detail Tube Replacement for the SCD Positioning the Upper Tube in the Union Fitting 100 Operation and Maintenance Manual Operation and Maintenance Manual 101 Tube Replacement for the NCD Operation and Maintenance Manual 103 NCD Tube Replacement Detail Troubleshooting Solving Detector Problems Detector Fuse Power ProblemsVacuum Pump Fuse Dual Plasma Controller FusesFuse Positions on the Power Supply Board High Voltage Transformer Ozone Generation ProblemsPlugged Restrictor Lines Response Problems Temperature Reading Problems Troubleshooting Detector Issues Diagnosing General ProblemsDetector gases Troubleshooting Pump Issues Troubleshooting Burner Issues Index Agilent Technologies, Inc
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