Agilent Technologies G6600-90006 manual Installation, Overview

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3 Installation

Overview 40

 

 

 

 

 

 

 

Step 1: Selecting a Location

41

 

 

 

 

 

Power Requirements

41

 

 

 

 

 

 

Figure 10. Drawing of the Detector with Dual Plasma Burner and Controller

42

Environmental Considerations

42

 

 

 

 

Combustion Gas Requirements

42

 

 

 

 

Step 2: Unpack and Inspect the Instrument

45

 

 

Required Installation Tools

45

 

 

 

 

Step 3: Set Up the Vacuum Pump

46

 

 

 

 

Installing the Edwards RV5 Pump Oil-Sealed Vacuum Pump 46

 

Figure 11. RV5 Oil-Sealed Vacuum Pump and Associated Traps (Front Side)

49

Figure 12. RV5 Oil-Sealed Vacuum Pump and Associated Traps (Back Side)

49

Figure 13. RV5 Oil- Sealed Vacuum Pump and Associated Traps (Top) 50

 

Figure 14. RV-5Oil-S ealed Vacuum Pump Exhaust Line 51

 

Installing the Welch Dry Piston Vacuum Pump

52

 

Figure 15. The Welch Dry Piston Pump

54

 

 

Figure 16. Oil Drain Kit with Ballast Control

54

 

Step 4: Connect the Power Cord

56

 

 

 

 

Figure 17. SCD Rear Panel Diagram

56

 

 

Step 5: Install the Dry Compressed Air or O2 Supply 57

 

Step 6: Install the Signal Output Cables

58

 

 

Standard Cable Connection

58

 

 

 

 

HP 3390 Series Integrator Cable Connection

58

 

HP 3396 Integrator Cable Connection

 

58

 

 

HP 5890 GC Analog Input Board

58

 

 

 

 

Agilent 6890 GC Analog Input Board

 

58

 

 

Step 7: Install the Dual Plasma Burner

59

 

 

Figure 18. Dimensions of GC Liner Cut-Outs

59

 

Step 8: Install the Dual Plasma Controller

 

60

 

 

Figure 19. Dual Plasma Controller Rear Panel

60

 

Step 9: Install Column Connections

61

 

 

 

 

Capillary Columns

61

 

 

 

 

 

 

Figure 20. Measuring Column Insertion

61

 

 

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Operation and Maintenance Manual

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Contents Operation and Maintenance Manual Warranty Safety NoticesAcknowledgements Manual Part NumberEnglish WA R N I N GIs not in use Español Français Deutsch Italiano Dutch Veiligheidsvoorzieningen niet meerFollowing symbols are used on the equipment Contents Installation OverviewFront Panel Controls and Initial Startup OperationMaintenance Pump MaintenanceTroubleshooting IndexOperation and Maintenance Manual Introduction Operation and Maintenance Manual System Description Specifications Technical Information 355 SCDTechnical Information 255 NCD Physical Specifications Power requirementsVoltage Theory of Operation Sulfur Chemiluminescence DetectorNitrogen Chemiluminescence Detector Dual Plasma Controller Dual Plasma Burner with the 355 SCDDescription of Major Components Dual Plasma BurnerCross-Section of the Dual Plasma Burner for the 355 SCD Cross-Section of the Dual Plasma Burner for the 255 NCD Ozone Generator Chemiluminescence Reaction Cell and Photomultiplier Tube355 SCD Left Side 355 SCD Right Side 255 NCD Left Side View Pressure Transducer Vacuum PumpChemical Trap Oil Coalescing FilterFID Adapter Optional NCD Reaction CellNCD Photomultiplier Tube and Cooler Schematic for 355 SCD Schematic for 255 NCD, in Nitrogen Mode Schematic for 255 NCD, in Nitrosamine Mode Operation and Maintenance Manual Installation Overview Power Requirements Selecting a LocationEnvironmental Considerations Combustion Gas RequirementsTwo-stage pressure regulators Venting Gases Required Installation Tools Unpack and Inspect the InstrumentSet Up the Vacuum Pump Installing the Edwards RV5 Pump Oil-Sealed Vacuum PumpWA R N I N G Ard RV5 Oil-Sealed Vacuum Pump and Associated Traps Front Side RV5 Oil- Sealed Vacuum Pump and Associated Traps Top Setting the Gas Ballast Position RV5 Installing the Welch Dry Piston Vacuum Pump Operation Notes Welch Pump Welch Dry Piston Pump Operation and Maintenance Manual Connect the Power Cord SCD 230 V Unit Rear Panel DiagramInstall the Dry Compressed Air or O2 Supply Install the Signal Output Cables Install the Dual Plasma Burner Additional informationInstall the Dual Plasma Controller Dual Plasma Controller Rear PanelInstall Column Connections Capillary ColumnsPacked Columns and Columns with an Outside Diameter 0.8 mm Install the Transfer Line Front Panel Controls and Initial Startup Power Controls Detector Front Panel ControlsSignal Controls Display Output ControlsDual Plasma Controller Controls Dual Plasma Controller Front PanelInitial Startup Vacuum TestRecorder Test Detector Interface Setup Initial CheckoutIgnition Operation Start-Up Procedure Detector Operation Detector Stability and ResponseColumn Bleed CokingContaminated Gases Fluctuating PressuresTypical Operating Conditions Typical Operating ConditionsDetection Limits Expected Detection Limits for Chromatographic ConditionsInstrument Shut-Down Daily ShutdownComplete Shutdown Using the 255 NCD in Nitrosamine Mode Special Operating ModesOperation and Maintenance Manual Operation and Maintenance Manual Maintenance Pump Maintenance Operating Life of Components for Edwards RV5 Vacuum PumpCleaning the Detector Changing the Oil Mist Filter RV5 Reaction Cell Cleaning EquipmentReaction Cell, PMT Housing and PMT Socket WA R N I N G Flow Sensor Calibration Detector Sensitivity MDLSCD Proper Ferrule Orientation to the Large Ceramic Tube Orientation of the Double Taper Ferrule Tightening the Heater Swivel Nut Operation and Maintenance Manual NCD Proper Ferrule Orientation to the Large Quartz Tube Burner Assembly Detail Tube Replacement for the SCD Positioning the Upper Tube in the Union Fitting 100 Operation and Maintenance Manual Operation and Maintenance Manual 101 Tube Replacement for the NCD Operation and Maintenance Manual 103 NCD Tube Replacement Detail Troubleshooting Solving Detector Problems Power Problems Detector FuseVacuum Pump Fuse Dual Plasma Controller FusesFuse Positions on the Power Supply Board Ozone Generation Problems High Voltage TransformerPlugged Restrictor Lines Response Problems Temperature Reading Problems Diagnosing General Problems Troubleshooting Detector IssuesDetector gases Troubleshooting Pump Issues Troubleshooting Burner Issues Index Agilent Technologies, Inc