Agilent Technologies G6600-90006 manual Ncd

Page 95

Assembling the Dual Plasma Burner for Component Replacement with the

NCD

 

The following procedure can be used to assemble the Dual Plasma Burner for

 

use with the NCD or for replacement of Burner components, such as ceramic

 

tubes. Refer to Figure 2 on page 27 for proper part nomenclature. Note that the

 

lower section of the NCD Burner is identical to the lower section of the SCD

 

Burner.

 

While the use of 1/4" ferrules is optional with the SCD, the quartz tube used in the NCD

N O T E

Burner is more fragile and the use of 1/4" graphite ferrules is highly recommended.

 

 

 

 

1 Slide the 0.066" internal diameter (I.D.) double taper ferrule onto the lower

 

Burner tube. The tube should extend approximately 2 mm past the end of

 

the ferrule.

 

2 Insert the lower Burner tube and double taper ferrule into the Burner inlet

 

fitting.

 

3 Slide the 1/4" Burner adapter over the top of the lower Burner tube all the

 

way down to the Burner inlet fitting and screw it onto the fitting

 

finger-tight.

Figure 32 Ferrule Placement on Lower Burner Tube

4Slide a 1/4" Swagelok nut over the Burner adapter and then slide a 1/4" ferrule over the Burner adapter and position it into the 1/4" nut.

5Center the lower Burner tube so that it will slide into the tapered union. Insert the lower end of the tapered union fitting into the 1/4" Swagelok nut

and screw it on finger-tight. If necessary, the brazed H2 line can be gently bent out of the way. Be careful not to stress the brazed (welded) connection.

6Find the quartz combustion tube, 1/4" ferrule and quartz heater assembly.

7Insert the quartz tube into the quartz heater assembly. Position a 1/4" ferrule (flat end butted up against the top of the swivel nut) onto the quartz combustion tube. With the ferrule positioned against the swivel nut, approximately 0.5 cm of the quartz tube should extend outside the nut.

Operation and Maintenance Manual

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Contents Operation and Maintenance Manual Manual Part Number WarrantySafety Notices AcknowledgementsWA R N I N G EnglishIs not in use Español Français Deutsch Italiano Veiligheidsvoorzieningen niet meer DutchFollowing symbols are used on the equipment Contents Overview InstallationOperation Front Panel Controls and Initial StartupPump Maintenance MaintenanceIndex TroubleshootingOperation and Maintenance Manual Introduction Operation and Maintenance Manual System Description Technical Information 255 NCD SpecificationsTechnical Information 355 SCD Power requirements Physical SpecificationsVoltage Nitrogen Chemiluminescence Detector Theory of OperationSulfur Chemiluminescence Detector Dual Plasma Burner with the 355 SCD Dual Plasma ControllerDual Plasma Burner Description of Major ComponentsCross-Section of the Dual Plasma Burner for the 355 SCD Cross-Section of the Dual Plasma Burner for the 255 NCD Chemiluminescence Reaction Cell and Photomultiplier Tube Ozone Generator355 SCD Left Side 355 SCD Right Side 255 NCD Left Side View Vacuum Pump Pressure TransducerNCD Reaction Cell Chemical TrapOil Coalescing Filter FID Adapter OptionalNCD Photomultiplier Tube and Cooler Schematic for 355 SCD Schematic for 255 NCD, in Nitrogen Mode Schematic for 255 NCD, in Nitrosamine Mode Operation and Maintenance Manual Installation Overview Selecting a Location Power RequirementsCombustion Gas Requirements Environmental ConsiderationsTwo-stage pressure regulators Venting Gases Unpack and Inspect the Instrument Required Installation ToolsInstalling the Edwards RV5 Pump Oil-Sealed Vacuum Pump Set Up the Vacuum PumpWA R N I N G Ard RV5 Oil-Sealed Vacuum Pump and Associated Traps Front Side RV5 Oil- Sealed Vacuum Pump and Associated Traps Top Setting the Gas Ballast Position RV5 Installing the Welch Dry Piston Vacuum Pump Operation Notes Welch Pump Welch Dry Piston Pump Operation and Maintenance Manual SCD 230 V Unit Rear Panel Diagram Connect the Power CordInstall the Dry Compressed Air or O2 Supply Install the Signal Output Cables Additional information Install the Dual Plasma BurnerDual Plasma Controller Rear Panel Install the Dual Plasma ControllerPacked Columns and Columns with an Outside Diameter 0.8 mm Install Column ConnectionsCapillary Columns Install the Transfer Line Front Panel Controls and Initial Startup Detector Front Panel Controls Power ControlsDisplay Output Controls Signal ControlsDual Plasma Controller Front Panel Dual Plasma Controller ControlsVacuum Test Initial StartupRecorder Test Initial Checkout Detector Interface SetupIgnition Operation Start-Up Procedure Coking Detector OperationDetector Stability and Response Column BleedFluctuating Pressures Contaminated GasesTypical Operating Conditions Typical Operating ConditionsExpected Detection Limits for Chromatographic Conditions Detection LimitsComplete Shutdown Instrument Shut-DownDaily Shutdown Special Operating Modes Using the 255 NCD in Nitrosamine ModeOperation and Maintenance Manual Operation and Maintenance Manual Maintenance Operating Life of Components for Edwards RV5 Vacuum Pump Pump MaintenanceCleaning the Detector Changing the Oil Mist Filter RV5 Equipment Reaction Cell CleaningReaction Cell, PMT Housing and PMT Socket WA R N I N G Flow Sensor Calibration MDL Detector SensitivitySCD Proper Ferrule Orientation to the Large Ceramic Tube Orientation of the Double Taper Ferrule Tightening the Heater Swivel Nut Operation and Maintenance Manual NCD Proper Ferrule Orientation to the Large Quartz Tube Burner Assembly Detail Tube Replacement for the SCD Positioning the Upper Tube in the Union Fitting 100 Operation and Maintenance Manual Operation and Maintenance Manual 101 Tube Replacement for the NCD Operation and Maintenance Manual 103 NCD Tube Replacement Detail Troubleshooting Solving Detector Problems Dual Plasma Controller Fuses Power ProblemsDetector Fuse Vacuum Pump FuseFuse Positions on the Power Supply Board High Voltage Transformer Ozone Generation ProblemsPlugged Restrictor Lines Response Problems Temperature Reading Problems Troubleshooting Detector Issues Diagnosing General ProblemsDetector gases Troubleshooting Pump Issues Troubleshooting Burner Issues Index Agilent Technologies, Inc