Agilent Technologies G6600-90006 manual Power Problems, Detector Fuse, Vacuum Pump Fuse

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Power Problems

The first step in the determination of a power related problem is to verify power to the pump, Controller, and Detector itself. The inability to establish power may be as trivial as a blown fuse. Fuse requirements and positions on the Detector are indicated in see Figure 47 and Table 4.

Repeated fuse failure is an indication of a more serious situation.

Detector Fuse

If the Standby LED does not illuminate when the unit is plugged in, and multiple fuses fail on the Detector, disconnect the power cord and contact Agilent.

Vacuum Pump Fuse

Repeated blown fuses of the vacuum pump indicate a pump oil problem. If the vacuum pump has not been in operation for some time or if water accumulated in the vacuum pump has not been properly removed, the pump may be difficult to start, or may require more power than normal, and this may blow the main AC fuse. Disconnect the main power cord from the AC outlet and from the back panel of the Detector. Replace the pump oil. Connect the pump power cord to an AC outlet in the lab to start it. Allow the pump to operate for 10 to

15 minutes, after which the pump may be plugged back into the rear panel of the Detector. If fuses blow after the pump oil has been changed, the pump has been damaged. Contact Agilent for further information.

The dry piston pump may require a short break-in time when new or after seals have been changed. It can be operated for a few hours by plugging it into a wall outlet. When turned off, it is necessary to allow the pump pressure to reach atmospheric conditions before restarting.

Also note that the dry piston pump is equipped with a thermal fuse; connecting the pump to a power supply that exceeds 110 V ±10% will result in the pump shutting down.

Dual Plasma Controller Fuses

If the Controller will not power on, confirm that the power cord is firmly seated at both ends. Also make certain that there is power to the outlet at the wall, surge protector, or circuit breaker. If the power cord is seated correctly and power is available to the Controller, the fuse in the power entry module (just above the power switch) on the back of the Controller may have blown. Make sure that the actual line voltage and the setting on the Controller match.

To replace the fuse in the power entry module, follow these steps:

1Unplug the power cord from the back of the Controller.

2Use a small flat-head screwdriver to pry open the fuse cover on the power entry module on the back of the Controller.

Operation and Maintenance Manual

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Contents Operation and Maintenance Manual Manual Part Number WarrantySafety Notices AcknowledgementsWA R N I N G EnglishIs not in use Español Français Deutsch Italiano Veiligheidsvoorzieningen niet meer DutchFollowing symbols are used on the equipment Contents Overview InstallationOperation Front Panel Controls and Initial StartupPump Maintenance MaintenanceIndex TroubleshootingOperation and Maintenance Manual Introduction Operation and Maintenance Manual System Description Technical Information 255 NCD SpecificationsTechnical Information 355 SCD Power requirements Physical SpecificationsVoltage Nitrogen Chemiluminescence Detector Theory of OperationSulfur Chemiluminescence Detector Dual Plasma Burner with the 355 SCD Dual Plasma ControllerDual Plasma Burner Description of Major ComponentsCross-Section of the Dual Plasma Burner for the 355 SCD Cross-Section of the Dual Plasma Burner for the 255 NCD Chemiluminescence Reaction Cell and Photomultiplier Tube Ozone Generator355 SCD Left Side 355 SCD Right Side 255 NCD Left Side View Vacuum Pump Pressure TransducerNCD Reaction Cell Chemical TrapOil Coalescing Filter FID Adapter OptionalNCD Photomultiplier Tube and Cooler Schematic for 355 SCD Schematic for 255 NCD, in Nitrogen Mode Schematic for 255 NCD, in Nitrosamine Mode Operation and Maintenance Manual Installation Overview Selecting a Location Power RequirementsCombustion Gas Requirements Environmental ConsiderationsTwo-stage pressure regulators Venting Gases Unpack and Inspect the Instrument Required Installation ToolsInstalling the Edwards RV5 Pump Oil-Sealed Vacuum Pump Set Up the Vacuum PumpWA R N I N G Ard RV5 Oil-Sealed Vacuum Pump and Associated Traps Front Side RV5 Oil- Sealed Vacuum Pump and Associated Traps Top Setting the Gas Ballast Position RV5 Installing the Welch Dry Piston Vacuum Pump Operation Notes Welch Pump Welch Dry Piston Pump Operation and Maintenance Manual SCD 230 V Unit Rear Panel Diagram Connect the Power CordInstall the Dry Compressed Air or O2 Supply Install the Signal Output Cables Additional information Install the Dual Plasma BurnerDual Plasma Controller Rear Panel Install the Dual Plasma ControllerPacked Columns and Columns with an Outside Diameter 0.8 mm Install Column ConnectionsCapillary Columns Install the Transfer Line Front Panel Controls and Initial Startup Detector Front Panel Controls Power ControlsDisplay Output Controls Signal ControlsDual Plasma Controller Front Panel Dual Plasma Controller ControlsVacuum Test Initial StartupRecorder Test Initial Checkout Detector Interface SetupIgnition Operation Start-Up Procedure Coking Detector OperationDetector Stability and Response Column BleedFluctuating Pressures Contaminated GasesTypical Operating Conditions Typical Operating ConditionsExpected Detection Limits for Chromatographic Conditions Detection LimitsComplete Shutdown Instrument Shut-DownDaily Shutdown Special Operating Modes Using the 255 NCD in Nitrosamine ModeOperation and Maintenance Manual Operation and Maintenance Manual Maintenance Operating Life of Components for Edwards RV5 Vacuum Pump Pump MaintenanceCleaning the Detector Changing the Oil Mist Filter RV5 Equipment Reaction Cell CleaningReaction Cell, PMT Housing and PMT Socket WA R N I N G Flow Sensor Calibration MDL Detector SensitivitySCD Proper Ferrule Orientation to the Large Ceramic Tube Orientation of the Double Taper Ferrule Tightening the Heater Swivel Nut Operation and Maintenance Manual NCD Proper Ferrule Orientation to the Large Quartz Tube Burner Assembly Detail Tube Replacement for the SCD Positioning the Upper Tube in the Union Fitting 100 Operation and Maintenance Manual Operation and Maintenance Manual 101 Tube Replacement for the NCD Operation and Maintenance Manual 103 NCD Tube Replacement Detail Troubleshooting Solving Detector Problems Dual Plasma Controller Fuses Power ProblemsDetector Fuse Vacuum Pump FuseFuse Positions on the Power Supply Board High Voltage Transformer Ozone Generation ProblemsPlugged Restrictor Lines Response Problems Temperature Reading Problems Troubleshooting Detector Issues Diagnosing General ProblemsDetector gases Troubleshooting Pump Issues Troubleshooting Burner Issues Index Agilent Technologies, Inc