Agilent Technologies G6600-90006 manual Install Column Connections, Capillary Columns

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Step 9: Install Column Connections

The Burner operates under reduced pressure and there will be a slight vacuum on the end of the column. If a higher outlet pressure for the column outlet is desired, fused silica capillary restrictors may be attached to the end of the analytical column (both capillary and packed) prior to making the Detector connection.

Capillary Columns

Place the column nut over the end of the capillary column. Place the appropriate fused silica adapter ferrule onto column. Remove a few centimeters from the end to remove any particles that may have entered the column. Insert the GC column into the Burner by 108-109 mm from the upper end of the nut (114-115 mm if measured from the flat bottom of the nut). Do not force the column. The pathway is narrow and may take several tries to seat it correctly. Tighten the column nut finger tight, or until sealed using a 7/16" open-end wrench to back-up the hydrogen inlet fitting to prevent it from slipping.

108-109 mm

114-115 mm

Figure 20 Measuring Column Insertion

Packed Columns and Columns with an Outside Diameter > 0.8 mm

Connect a short piece (0.5 m or less) of deactivated fused silica tube, for example 0.32 mm internal diameter, to the Detector end of the column. Follow the procedure for capillary column connection as above.

Operation and Maintenance Manual

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Contents Operation and Maintenance Manual Safety Notices WarrantyAcknowledgements Manual Part NumberWA R N I N G EnglishIs not in use Español Français Deutsch Italiano Veiligheidsvoorzieningen niet meer DutchFollowing symbols are used on the equipment Contents Overview InstallationOperation Front Panel Controls and Initial StartupPump Maintenance MaintenanceIndex TroubleshootingOperation and Maintenance Manual Introduction Operation and Maintenance Manual System Description Technical Information 355 SCD SpecificationsTechnical Information 255 NCD Power requirements Physical SpecificationsVoltage Sulfur Chemiluminescence Detector Theory of OperationNitrogen Chemiluminescence Detector Dual Plasma Burner with the 355 SCD Dual Plasma ControllerDual Plasma Burner Description of Major ComponentsCross-Section of the Dual Plasma Burner for the 355 SCD Cross-Section of the Dual Plasma Burner for the 255 NCD Chemiluminescence Reaction Cell and Photomultiplier Tube Ozone Generator355 SCD Left Side 355 SCD Right Side 255 NCD Left Side View Vacuum Pump Pressure TransducerOil Coalescing Filter Chemical TrapFID Adapter Optional NCD Reaction CellNCD Photomultiplier Tube and Cooler Schematic for 355 SCD Schematic for 255 NCD, in Nitrogen Mode Schematic for 255 NCD, in Nitrosamine Mode Operation and Maintenance Manual Installation Overview Selecting a Location Power RequirementsCombustion Gas Requirements Environmental ConsiderationsTwo-stage pressure regulators Venting Gases Unpack and Inspect the Instrument Required Installation ToolsInstalling the Edwards RV5 Pump Oil-Sealed Vacuum Pump Set Up the Vacuum PumpWA R N I N G Ard RV5 Oil-Sealed Vacuum Pump and Associated Traps Front Side RV5 Oil- Sealed Vacuum Pump and Associated Traps Top Setting the Gas Ballast Position RV5 Installing the Welch Dry Piston Vacuum Pump Operation Notes Welch Pump Welch Dry Piston Pump Operation and Maintenance Manual SCD 230 V Unit Rear Panel Diagram Connect the Power CordInstall the Dry Compressed Air or O2 Supply Install the Signal Output Cables Additional information Install the Dual Plasma BurnerDual Plasma Controller Rear Panel Install the Dual Plasma ControllerCapillary Columns Install Column ConnectionsPacked Columns and Columns with an Outside Diameter 0.8 mm Install the Transfer Line Front Panel Controls and Initial Startup Detector Front Panel Controls Power ControlsDisplay Output Controls Signal ControlsDual Plasma Controller Front Panel Dual Plasma Controller ControlsVacuum Test Initial StartupRecorder Test Initial Checkout Detector Interface SetupIgnition Operation Start-Up Procedure Detector Stability and Response Detector OperationColumn Bleed CokingFluctuating Pressures Contaminated GasesTypical Operating Conditions Typical Operating ConditionsExpected Detection Limits for Chromatographic Conditions Detection LimitsDaily Shutdown Instrument Shut-DownComplete Shutdown Special Operating Modes Using the 255 NCD in Nitrosamine ModeOperation and Maintenance Manual Operation and Maintenance Manual Maintenance Operating Life of Components for Edwards RV5 Vacuum Pump Pump MaintenanceCleaning the Detector Changing the Oil Mist Filter RV5 Equipment Reaction Cell CleaningReaction Cell, PMT Housing and PMT Socket WA R N I N G Flow Sensor Calibration MDL Detector SensitivitySCD Proper Ferrule Orientation to the Large Ceramic Tube Orientation of the Double Taper Ferrule Tightening the Heater Swivel Nut Operation and Maintenance Manual NCD Proper Ferrule Orientation to the Large Quartz Tube Burner Assembly Detail Tube Replacement for the SCD Positioning the Upper Tube in the Union Fitting 100 Operation and Maintenance Manual Operation and Maintenance Manual 101 Tube Replacement for the NCD Operation and Maintenance Manual 103 NCD Tube Replacement Detail Troubleshooting Solving Detector Problems Detector Fuse Power ProblemsVacuum Pump Fuse Dual Plasma Controller FusesFuse Positions on the Power Supply Board High Voltage Transformer Ozone Generation ProblemsPlugged Restrictor Lines Response Problems Temperature Reading Problems Troubleshooting Detector Issues Diagnosing General ProblemsDetector gases Troubleshooting Pump Issues Troubleshooting Burner Issues Index Agilent Technologies, Inc