Agilent Technologies G6600-90006 manual Wa R N I N G

Page 47

11Remove the drain plug and the bonded seal from the oil mist filter. The bonded seal looks like a metal washer with a black inner o-ring.

12Install the bonded seal to the oil mist filter drain adapter. The drain adapter looks like a drain plug with a small plastic nozzle.

13Screw the black drain adapter and bonded seal into the oil mist filter.

14Remove the plastic protective cover from the pump exhaust port. Place the centering o-ring on the pump exhaust port (see Figure 13).

15Place the oil mist filter onto the o-ring on the pump exhaust port. Install the filter so that the gray half is above the white half of the filter (see Figure 11 and Figure 12).

16Position the oil mist filter so the drain adapter points toward the gas ballast inlet (see Figure 11 and Figure 12).

17Fit the clamping ring onto the adapter and oil mist filter and hand tighten.

18Turn the gray plastic gas ballast knob counterclockwise to position II. Press the knob down against the spring and continue to turn counterclockwise until the knob is free. Remove knob from the pump. Confirm that the spring is still in place.

19Locate the tall aluminum gas ballast control assembly, and install the small o-ring into the groove on the shaft.

20Insert the gas ballast control assembly into the pump, pressing down against the spring, and turn it clockwise until the nozzle on the assembly is directly over the mark on the top of the pump.

21Cut approximately 3/4 of the black silicone oil return line and insert the steel restrictor approximately half-way into the line. If needed, use a small screwdriver or other small tool to aid in positioning the restrictor.

22Fit one end of the oil return line to the drain adapter on the oil mist filter. Fit the other end of the line to the nozzle on the gas ballast adapter. Ensure that the tubing is not tight and has no tight bends. Secure the line at each end, using the black hose clips provided.

23Add oil to the pump via either of the two oil fill caps. The oil level should be between one-third and one-half when viewed in the oil sight glass. Replace the oil fill cap prior to operation of the pump.

WA R N I N G

Do not operate the vacuum pump with the oil level below the minimum oil level mark or

above the maximum oil level mark.

 

 

 

24Place a hose clamp over the black heat shrink end of the 6’ Tygon vacuum hose, and connect the hose to the barbed fitting labeled Exhaust on the back of the Detector. Tighten the hose clamp securely.

25The SCD should be placed near the GC and be accessible from the rear in order to connect the electrical power and the recorder signal cable.

Operation and Maintenance Manual

47

Image 47
Contents Operation and Maintenance Manual Manual Part Number WarrantySafety Notices AcknowledgementsWA R N I N G EnglishIs not in use Español Français Deutsch Italiano Veiligheidsvoorzieningen niet meer DutchFollowing symbols are used on the equipment Contents Overview InstallationOperation Front Panel Controls and Initial StartupPump Maintenance MaintenanceIndex TroubleshootingOperation and Maintenance Manual Introduction Operation and Maintenance Manual System Description Technical Information 255 NCD SpecificationsTechnical Information 355 SCD Power requirements Physical SpecificationsVoltage Nitrogen Chemiluminescence Detector Theory of OperationSulfur Chemiluminescence Detector Dual Plasma Burner with the 355 SCD Dual Plasma ControllerDual Plasma Burner Description of Major ComponentsCross-Section of the Dual Plasma Burner for the 355 SCD Cross-Section of the Dual Plasma Burner for the 255 NCD Chemiluminescence Reaction Cell and Photomultiplier Tube Ozone Generator355 SCD Left Side 355 SCD Right Side 255 NCD Left Side View Vacuum Pump Pressure TransducerNCD Reaction Cell Chemical TrapOil Coalescing Filter FID Adapter OptionalNCD Photomultiplier Tube and Cooler Schematic for 355 SCD Schematic for 255 NCD, in Nitrogen Mode Schematic for 255 NCD, in Nitrosamine Mode Operation and Maintenance Manual Installation Overview Selecting a Location Power RequirementsCombustion Gas Requirements Environmental ConsiderationsTwo-stage pressure regulators Venting Gases Unpack and Inspect the Instrument Required Installation ToolsInstalling the Edwards RV5 Pump Oil-Sealed Vacuum Pump Set Up the Vacuum PumpWA R N I N G Ard RV5 Oil-Sealed Vacuum Pump and Associated Traps Front Side RV5 Oil- Sealed Vacuum Pump and Associated Traps Top Setting the Gas Ballast Position RV5 Installing the Welch Dry Piston Vacuum Pump Operation Notes Welch Pump Welch Dry Piston Pump Operation and Maintenance Manual SCD 230 V Unit Rear Panel Diagram Connect the Power CordInstall the Dry Compressed Air or O2 Supply Install the Signal Output Cables Additional information Install the Dual Plasma BurnerDual Plasma Controller Rear Panel Install the Dual Plasma ControllerPacked Columns and Columns with an Outside Diameter 0.8 mm Install Column ConnectionsCapillary Columns Install the Transfer Line Front Panel Controls and Initial Startup Detector Front Panel Controls Power ControlsDisplay Output Controls Signal ControlsDual Plasma Controller Front Panel Dual Plasma Controller ControlsVacuum Test Initial StartupRecorder Test Initial Checkout Detector Interface SetupIgnition Operation Start-Up Procedure Coking Detector OperationDetector Stability and Response Column BleedFluctuating Pressures Contaminated GasesTypical Operating Conditions Typical Operating ConditionsExpected Detection Limits for Chromatographic Conditions Detection LimitsComplete Shutdown Instrument Shut-DownDaily Shutdown Special Operating Modes Using the 255 NCD in Nitrosamine ModeOperation and Maintenance Manual Operation and Maintenance Manual Maintenance Operating Life of Components for Edwards RV5 Vacuum Pump Pump MaintenanceCleaning the Detector Changing the Oil Mist Filter RV5 Equipment Reaction Cell CleaningReaction Cell, PMT Housing and PMT Socket WA R N I N G Flow Sensor Calibration MDL Detector SensitivitySCD Proper Ferrule Orientation to the Large Ceramic Tube Orientation of the Double Taper Ferrule Tightening the Heater Swivel Nut Operation and Maintenance Manual NCD Proper Ferrule Orientation to the Large Quartz Tube Burner Assembly Detail Tube Replacement for the SCD Positioning the Upper Tube in the Union Fitting 100 Operation and Maintenance Manual Operation and Maintenance Manual 101 Tube Replacement for the NCD Operation and Maintenance Manual 103 NCD Tube Replacement Detail Troubleshooting Solving Detector Problems Dual Plasma Controller Fuses Power ProblemsDetector Fuse Vacuum Pump FuseFuse Positions on the Power Supply Board High Voltage Transformer Ozone Generation ProblemsPlugged Restrictor Lines Response Problems Temperature Reading Problems Troubleshooting Detector Issues Diagnosing General ProblemsDetector gases Troubleshooting Pump Issues Troubleshooting Burner Issues Index Agilent Technologies, Inc