Teledyne Model 300EU manual Initial Calibration, Pre-Calibration Stabilization, Calibration Gases

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3.5. INITIAL CALIBRATION

M300EU	GETTING STARTED
(Addendum to M300EU Manual - P/N 04145)

3.5. INITIAL CALIBRATION

3.5.1. PRE-CALIBRATION STABILIZATION

Before initially calibrating the M300EU it must be allowed to operate for a minimum of 12 hours.

After this stabilization period is complete and just prior to performing the initial calibration, manually initiate an auto-reference measurement by following the instructions in Section 6.4.

3.5.2. BASIC CO CALIBRATION SETUP

NOTE

The following procedure assumes that the instrument does not have any of the available Zero/Span

Valve Options installed.

To perform the following calibration you must have sources for zero air and span gas available for input into the sample port on the back of the analyzer. See Section 3.1.3 of the M300E/EM Operators Manual (P/N 04288) for instructions for connecting these gas sources.

NOTE

All Gas lines should be PTFE (Teflon), FEP, glass, stainless steel or brass

3.5.2.1. Calibration Gases

The information found in Section 3.1.3.2 of the M300E/EM Operators Manual (P/N 04288) is applicable to the M300EU with the following exception:

ZERO AIR

A gas that is similar in chemical composition to the earth’s atmosphere but scrubbed of all components that might affect the analyzers readings, in this case CO and water vapor.

For the M300EU this gas MUST include at least 5% O2 (required for the proper operation of the analyzer’s CO scrubber).

For analyzers without an IZS or external zero air scrubber option, a zero air generator such as the Teledyne Instruments Model 701 can be used.

NOTE

The zero air generator MUST be equipped with a hydrocarbon (HC) & CO scrubber option.

For the Teledyne Instruments M701, this is Option 2B

05514 Rev A1

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Contents 9480 CARROLL PARK DRIVE SAN DIEGO, CALIFORNIA USA ADDENDUM TO M300E/EM MANUAL P/NMODEL 300EU CO ANALYZER WITH AUTO-REFERENCE TELEDYNE INSTRUMENTS ADVANCED POLLUTION INSTRUMENTATION DIVISION TAPIPage GENERAL SAFETY HAZARD SAFETY MESSAGESUSER NOTES M300EUAddendum to M300E/EM Manual P/N TABLE OF CONTENTS LIST OF TABLES LIST OF FIGURESAPPENDIX A-4 Model 300EU Signal I/O Definitions, Revision K.6 LIST OF APPENDICESAddendum to M300E/EM Manual P/N any time the instrument is in SETUP mode 1. INTRODUCTION1.1. REFERENCE NUMBERING CONVENTION 1.2. M300EU OVERVIEWAddendum to M300E/EM Manual P/N 05514 Rev A1 2. SPECIFICATIONS, APPROVALS AND WARRANTY2.1. SPECIFICATIONS M300EU Basic Unit Specifications05831 Rev 2.4. WARRANTY2.2. EPA EQUIVALENCY DESIGNATION 2.3. CE MARK COMPLIANCEOPTICAL BENCH 3. GETTING STARTED3.1. UNPACKING THE M300EU 3.2. M300EU ANALYZER LAYOUTFigure 3-2 M300EU Internal Gas Flow 3.3.1. POWER CONNECTION3.3. ELECTRICAL CONNECTIONS M300EUAnalog Output Data Type Default Settings 3.3.2. ANALOG OUTPUT ConnectionsFigure 3-3 M300EU Analog Output Connector Output # 3.3.3. CONNECTING THE STATUS OUTPUTSAnalog Output Pin Outs Table 3-3 Status Output Pin AssignmentsMESSAGE 3.4. INITIAL OPERATION OF THE M300EU3.4.1. STARTUP AND WARM UP OF THE M300EU 3.4.2. WARNING MESSAGESThe Test functions available from the front panel of the M300EU are 3.4.3. FUNCTIONAL CHECK3.5.2.1. Calibration Gases 3.5.2. BASIC CO CALIBRATION SETUP3.5. INITIAL CALIBRATION 3.5.1. PRE-CALIBRATION STABILIZATIONSTEP 3 - SET CO SPAN GAS CONCENTRATION 3.5.3. BASIC CO CALIBRATION PROCEDURESTEP 1 - SET LIMITS STEP 2 - DILUTION RATIO4. FREQENTLY ASKED QUESTIONS & GLOSSARY Addendum to M300E/EM Manual P/N 300E 5. OPTIONAL HARDWARE AND SOFTWAREOPTION DESCRIPTIONM300EU Internal Pneumatic Flow- Zero/Span Valves OPT 50A 5.1. CALIBRATION VALVE OPTIONS FOR THE M300EU5.1.1. ZERO SPAN VALVES OPT 50A TOLL-FREE FAX TEL E-MAIL api-sales@teledyne.comSAMPLE CHAMBER 5.1.2. ZERO SPAN VALVES WITH IZS OPT 51BScrubber 5.1.3. Zero Span Valves with IZS and Shutoff VALVE OPT 51B 6. M300EU OPERATING INSTRUCTIONS reference gas path 6.2. OPERATING MODESM300EU Operating Modes sample gas stream is being routed through the CO scrubber of the autoAUTO-REF RANGE = 50.000 PPM 6.2.1. AUTO-REFERENCE MODE AREFSETUP Mode FieldParameter 6.2.2. TEST FUNCTIONSUnits Table 6-2 Test Functions DefinedANALOG OUT 6.3. SETUP Æ RNGE ANALOG OUTPUT REPORTING RANGE CONFIGURATION6.3.1. PHYSICAL RANGE VERSUS ANALOG OUTPUT REPORTING RANGES 6.3.2. ANALOG OUTPUT RANGES FOR CO CONCENTRATIONAUTO DEFAULT SETTINGSSNGL DUALThis is the default reporting range mode for the analyzer To set the ranges press following keystroke sequence M300EU OPERATING INSTRUCTIONS Consult your local regulations for the STP used by your agency 6.3.6. SETUP Æ RNGE Æ UNIT SETTING THE REPORTING RANGE UNIT TYPEweight/volume units CO ppb x 1.25 = CO ug/m3 CO ppm x 1.25= CO mg/m3 Pressure STP6.4.1. ADJUSTING THE A-REF MODE CYCLE TIME To manually start an auto-reference measurement cycle, press 6.4.2. FORCING AN AUTO-REFERENCE MEASUREMENT05514 Rev A1 DESCRIPTION 6.5. SETUP Æ MORE Æ VARS INTERNAL VARIABLES VARSTable 6-3 Test Functions Defined VARIABLEDIAG AIO 6.6. SETUP Æ MORE Æ DIAG USING THE DIAGNOSTICS FUNCTIONSDIAG I/O DIAG AOUTDIAG - Analog I/O Functions 6.7. ANALOG OUTPUT CONFIGURATION6.7.1. ANALOG I/O CONFIGURATION THE ANALOG I/O CONFIGURATION SUBMENU4. Choose a Test Channel parameter to be output on the channel 6.13.5.8 SETTING DATA UPDATE RATE FOR AN ANALOG OUTPUT ANALOG OUTPUT SIGNAL TYPE AND RANGE SELECTIONTURNING THE ANALOG OUTPUT OVER-RANGE FEATURE ON/OFF 6.13.5.7 SETTING THE REPORTING RANGE SCALE FOR AN ANALOG OUTPUTAUTOMATIC ANALOG OUTPUT CALIBRATION 6.7.2. CALIBRATION OF THE ANALOG OUTPUTSMANUAL CALIBRATION OF ANALOG OUTPUT CONFIGURED FOR VOLTAGE RANGES ENABLING OR DISABLING THE AUTO-CAL FOR AN INDIVIDUAL ANALOG OUTPUTZERO 6.7.3. SELECTING A TEST CHANNEL FUNCTION FOR OUTPUT A4Test Channels Functions Available on the M300EU’s Analog Output TEST CHANNELTable 6-7 M300EU Hessen GAS ID List 6.7.4. HESSEN PROTOCOLDefault Hessen Status Bit Assignments STEP3 - ZERO/SPAN CALIBRATION 7. CALIBRATION PROCEDURESmanual for troubleshooting tips MANUAL CALIBRATION REQUIRED EQUIPMENT, SUPPLIES AND EXPENDABLESMANUAL CALIBRATION CHECKS WITH ZERO/SPAN VALVES 7.9.1 SECTION O2 SENSOR CALIBRATION PROCEDURE7.9.2 CO2 SENSOR CALIBRATION PROCEDURE MANUAL CALIBRATION WITH ZERO/SPAN VALVES8. EPA PROTOCOL CALIBRATION Addendum to M300E/EM Manual P/N 9.1. PERFOMING AN AUTO-REFERENCE MEASUREMENT AFTER MAINTENANCE 9. INSTRUMENT MAINTENANCEAddendum to M300E/EM Manual P/N MR RATIO Table 9-1 M300EU Test Function RecordSTABILITY CO MEASAddendum to M300E/EM Manual P/N Figure 10-1 M300EU Gas flow during Auto-Reference Measurements 10. THEORY OF OPERATION10.1. MEASUREMENT METHOD 10.1.1. AUTO-REFERENCE RATIOThis includes calibration gases such as zero air and span gas 10.2. PNEUMATIC OPERATION10.2.1. THE A-REF CARBON MONOXIDE SCRUBBER Figure 10-2 Auto-Reference Measurement CycleFigure 10-3 Semi-Permeable Membrane Drying Process 10.2.2. THE A-REF VALVE ASSEMBLY10.2.3. THE NAFION→ DRYER Auto-Reference Valve Operating StatesThe dryer consists of a bundle of 0.030 O.D. Nafion→ tubes housed within a single large tube shell. Sample gas flows within the Nafion tubes while water vapor absorbs into the tubular membrane walls and is removed. Moisture permeating the tubing is carried away by a dry purge gas within the shell that flows countercurrent to the sample gas Aout 10.3. ELECTRONIC OPERATION10.3.1. OVERVIEW Figure 10-4 M300EU Electronic Overview Block Diagram10.3.2.1. Temperature Control of the Convection Oven 10.3.2. THE RELAY PCAFigure 10-5 M300EU Heating Control Block Diagram Figure 10-6 M300EU Oven Heater Configuration Jumpers 10.3.2.2. Oven Heaters AC Power Configuration115 VAC Configuration 230 VAC Configuration10.3.3.2. Sensor Inputs 10.3.3. MOTHERBOARD10.3.2.3. Status LED’s 10.3.3.1. A to D ConversionRELAY PCA 10.3.4. POWER DISTRIBUTIONFigure 10-8 M300EU Distribution Block Diagram Page PROCEDURES 11. TROUBLESHOOTING & REPAIR11.1. GENERAL NOTES MAINTENANCE PERSONNEL ONLYWarning Messages - Indicated Failures 11.2. FAULT DIAGNOSIS WITH WARNING MESSAGESTable continued on next page Sample flow rate is Warning Messages - Indicated Failures contINDICATED FAILURES 11.2.1. FAULT DIAGNOSIS WITH TEST FUNCTIONSTable 11-2 Test Functions - Indicated Failures table continuedValues outside range indicate Test Functions - Indicated FailuresVoltage displayed should change. If not 11.2.2. RELAY BOARD STATUS LED’SFaulty Connectors/Wiring Table 11-3 Relay Board Status LED Failure Indications11.4. OTHER PERFORMANCE PROBLEMS 11.3. GAS FLOW PROBLEMS11.4.1. Unexplained DRIFT 11.5.2.1. A/D Functions 11.5. SUBSYSTEM CHECHOUT11.5.1. RELAY BOARD 11.5.2. MOTHERBOARD11.6. TECHNICAL ASSISTANCE Addendum to M300E/EM Manual P/N M300EU Addendum to M300E/EM Manual APPENDIX A - Version Specific Software DocumentationAPPENDIX A-2 M300EU Setup Variables Available Via Serial I/O APPENDIX A-4 M300EU Signal I/O DefinitionsTEST1 CLR1MSG1 Figure A-2 Primary Setup Menu Except iDAS Figure A-3 Primary Setup Menu Æ iDAS Submenu Figure A-4 Secondary Setup Menu Æ COMM and VARS Submenus Figure A-5 Secondary Setup Menu Æ Hessen Protocol Submenu Press ENTR ENTER PASSWORDAuto Cal feature is OFF or the range is set for Figure A-6 DIAG MenuAPPENDIX A-2 Setup Variables For Serial I/O, Revision K.6 APPENDIX A-2 Setup Variables For Serial I/O, Revision K.6Table continues CO2FILTPCT O2FILTPCT A-10STDO2CELLTEMP A-11 APPENDIX A-3 Warnings and Test Functions, Revision K.6NAME MESSAGE TEXTThese gases not applicable to the M300EU Table A-5A-12 These gases not applicable to the M300EUNumber Signal NameBit or Channel DescriptionOVTMPW Internal box temperature #2/oven warning APPENDIX A-5 M300EU iDAS Parameters Revision K.6A-14 O2OFST A-15CO2OFS O2SLPEA-16 APPENDIX A-6 Terminal Command Designators, Revision K.605925 Rev A APPENDIX B - M300EU SPARE PARTS & EXPENDABLESAPPENDIX B - M300EU SPARE PARTS & EXPENDABLES European standard ENM300EU Addendum to M300E/EM Manual