Teledyne Model 300EU manual The A-Ref Valve Assembly, The Nafion→ Dryer, M300EU, Rev A1

Page 59
10.2.2. THE A-REF VALVE ASSEMBLY

M300EU

THEORY OF OPERATION

(Addendum to M300EU Manual - P/N 04145)

 

10.2.2. THE A-REF VALVE ASSEMBLY

The auto-reference valve assembly is located next to the optical bench, at the rear of the analyzer between the Nafiondryer and the outer wall of the instrument (see Figure 3-1). The following table describes the state of each valve during the analyzer’s various operational modes (see Figure 10-1).

Table 10-1:

Auto-Reference Valve Operating States

 

 

 

 

Mode

 

Valve State

VALVE PORT CONNECTIONS

SAMPLE

 

Gas stream from NafionDryer &

3 Æ 2

(Normal State)

 

SAMPLE inlet

A-REF DWELL

 

Gas stream from CO scrubber

1 Æ 2

A-REF MEASUREMENT

 

Gas stream from CO scrubber

1 Æ 2

SAMPLE DWELL

 

Gas stream from NafionDryer &

3 Æ 2

 

SAMPLE inlet

10.2.3. THE NAFIONDRYER.

Normal room air contains a certain amount of water vapor. While H2O is a very low-level interferent for IR absorption (in the same range as CO) it can cause enough interference to affect the high-resolution measurements of the M300EU.

To account for this the M300EU has a special dryer added to the gas stream. The dryer consists of a bundle of parallel tubes of Nafion®, a co-polymer similar to Teflon® that absorbs water very well but not other chemicals. The multiple tube design of this dryer creates a large reactive surface without causing a restriction in the higher gas flow rate required by the M300EU that a long single tube style dryer would.

Figure 10-3: Semi-Permeable Membrane Drying Process

05514 Rev A1

51

Image 59
Contents 9480 CARROLL PARK DRIVE SAN DIEGO, CALIFORNIA USA ADDENDUM TO M300E/EM MANUAL P/NMODEL 300EU CO ANALYZER WITH AUTO-REFERENCE TELEDYNE INSTRUMENTS ADVANCED POLLUTION INSTRUMENTATION DIVISION TAPIPage GENERAL SAFETY HAZARD SAFETY MESSAGESUSER NOTES M300EUAddendum to M300E/EM Manual P/N TABLE OF CONTENTS LIST OF TABLES LIST OF FIGURESAPPENDIX A-4 Model 300EU Signal I/O Definitions, Revision K.6 LIST OF APPENDICESAddendum to M300E/EM Manual P/N any time the instrument is in SETUP mode 1. INTRODUCTION1.1. REFERENCE NUMBERING CONVENTION 1.2. M300EU OVERVIEWAddendum to M300E/EM Manual P/N 05514 Rev A1 2. SPECIFICATIONS, APPROVALS AND WARRANTY2.1. SPECIFICATIONS M300EU Basic Unit Specifications05831 Rev 2.4. WARRANTY2.2. EPA EQUIVALENCY DESIGNATION 2.3. CE MARK COMPLIANCEOPTICAL BENCH 3. GETTING STARTED3.1. UNPACKING THE M300EU 3.2. M300EU ANALYZER LAYOUTFigure 3-2 M300EU Internal Gas Flow 3.3.1. POWER CONNECTION3.3. ELECTRICAL CONNECTIONS M300EUFigure 3-3 M300EU Analog Output Connector 3.3.2. ANALOG OUTPUT ConnectionsAnalog Output Data Type Default Settings Output # 3.3.3. CONNECTING THE STATUS OUTPUTSAnalog Output Pin Outs Table 3-3 Status Output Pin AssignmentsMESSAGE 3.4. INITIAL OPERATION OF THE M300EU3.4.1. STARTUP AND WARM UP OF THE M300EU 3.4.2. WARNING MESSAGESThe Test functions available from the front panel of the M300EU are 3.4.3. FUNCTIONAL CHECK3.5.2.1. Calibration Gases 3.5.2. BASIC CO CALIBRATION SETUP3.5. INITIAL CALIBRATION 3.5.1. PRE-CALIBRATION STABILIZATIONSTEP 3 - SET CO SPAN GAS CONCENTRATION 3.5.3. BASIC CO CALIBRATION PROCEDURESTEP 1 - SET LIMITS STEP 2 - DILUTION RATIO4. FREQENTLY ASKED QUESTIONS & GLOSSARY Addendum to M300E/EM Manual P/N 300E 5. OPTIONAL HARDWARE AND SOFTWAREOPTION DESCRIPTIONM300EU Internal Pneumatic Flow- Zero/Span Valves OPT 50A 5.1. CALIBRATION VALVE OPTIONS FOR THE M300EU5.1.1. ZERO SPAN VALVES OPT 50A TOLL-FREE FAX TEL E-MAIL api-sales@teledyne.comScrubber 5.1.2. ZERO SPAN VALVES WITH IZS OPT 51BSAMPLE CHAMBER 5.1.3. Zero Span Valves with IZS and Shutoff VALVE OPT 51B 6. M300EU OPERATING INSTRUCTIONS reference gas path 6.2. OPERATING MODESM300EU Operating Modes sample gas stream is being routed through the CO scrubber of the autoAUTO-REF RANGE = 50.000 PPM 6.2.1. AUTO-REFERENCE MODE AREFSETUP Mode FieldParameter 6.2.2. TEST FUNCTIONSUnits Table 6-2 Test Functions DefinedANALOG OUT 6.3. SETUP Æ RNGE ANALOG OUTPUT REPORTING RANGE CONFIGURATION6.3.1. PHYSICAL RANGE VERSUS ANALOG OUTPUT REPORTING RANGES 6.3.2. ANALOG OUTPUT RANGES FOR CO CONCENTRATIONAUTO DEFAULT SETTINGSSNGL DUALThis is the default reporting range mode for the analyzer To set the ranges press following keystroke sequence M300EU OPERATING INSTRUCTIONS Consult your local regulations for the STP used by your agency 6.3.6. SETUP Æ RNGE Æ UNIT SETTING THE REPORTING RANGE UNIT TYPEweight/volume units CO ppb x 1.25 = CO ug/m3 CO ppm x 1.25= CO mg/m3 Pressure STP6.4.1. ADJUSTING THE A-REF MODE CYCLE TIME To manually start an auto-reference measurement cycle, press 6.4.2. FORCING AN AUTO-REFERENCE MEASUREMENT05514 Rev A1 DESCRIPTION 6.5. SETUP Æ MORE Æ VARS INTERNAL VARIABLES VARSTable 6-3 Test Functions Defined VARIABLEDIAG AIO 6.6. SETUP Æ MORE Æ DIAG USING THE DIAGNOSTICS FUNCTIONSDIAG I/O DIAG AOUTDIAG - Analog I/O Functions 6.7. ANALOG OUTPUT CONFIGURATION6.7.1. ANALOG I/O CONFIGURATION THE ANALOG I/O CONFIGURATION SUBMENU4. Choose a Test Channel parameter to be output on the channel 6.13.5.8 SETTING DATA UPDATE RATE FOR AN ANALOG OUTPUT ANALOG OUTPUT SIGNAL TYPE AND RANGE SELECTIONTURNING THE ANALOG OUTPUT OVER-RANGE FEATURE ON/OFF 6.13.5.7 SETTING THE REPORTING RANGE SCALE FOR AN ANALOG OUTPUTAUTOMATIC ANALOG OUTPUT CALIBRATION 6.7.2. CALIBRATION OF THE ANALOG OUTPUTSMANUAL CALIBRATION OF ANALOG OUTPUT CONFIGURED FOR VOLTAGE RANGES ENABLING OR DISABLING THE AUTO-CAL FOR AN INDIVIDUAL ANALOG OUTPUTZERO 6.7.3. SELECTING A TEST CHANNEL FUNCTION FOR OUTPUT A4Test Channels Functions Available on the M300EU’s Analog Output TEST CHANNELTable 6-7 M300EU Hessen GAS ID List 6.7.4. HESSEN PROTOCOLDefault Hessen Status Bit Assignments STEP3 - ZERO/SPAN CALIBRATION 7. CALIBRATION PROCEDURESmanual for troubleshooting tips MANUAL CALIBRATION REQUIRED EQUIPMENT, SUPPLIES AND EXPENDABLESMANUAL CALIBRATION CHECKS WITH ZERO/SPAN VALVES 7.9.1 SECTION O2 SENSOR CALIBRATION PROCEDURE7.9.2 CO2 SENSOR CALIBRATION PROCEDURE MANUAL CALIBRATION WITH ZERO/SPAN VALVES8. EPA PROTOCOL CALIBRATION Addendum to M300E/EM Manual P/N 9.1. PERFOMING AN AUTO-REFERENCE MEASUREMENT AFTER MAINTENANCE 9. INSTRUMENT MAINTENANCEAddendum to M300E/EM Manual P/N MR RATIO Table 9-1 M300EU Test Function RecordSTABILITY CO MEASAddendum to M300E/EM Manual P/N Figure 10-1 M300EU Gas flow during Auto-Reference Measurements 10. THEORY OF OPERATION10.1. MEASUREMENT METHOD 10.1.1. AUTO-REFERENCE RATIOThis includes calibration gases such as zero air and span gas 10.2. PNEUMATIC OPERATION10.2.1. THE A-REF CARBON MONOXIDE SCRUBBER Figure 10-2 Auto-Reference Measurement CycleFigure 10-3 Semi-Permeable Membrane Drying Process 10.2.2. THE A-REF VALVE ASSEMBLY10.2.3. THE NAFION→ DRYER Auto-Reference Valve Operating StatesThe dryer consists of a bundle of 0.030 O.D. Nafion→ tubes housed within a single large tube shell. Sample gas flows within the Nafion tubes while water vapor absorbs into the tubular membrane walls and is removed. Moisture permeating the tubing is carried away by a dry purge gas within the shell that flows countercurrent to the sample gas Aout 10.3. ELECTRONIC OPERATION10.3.1. OVERVIEW Figure 10-4 M300EU Electronic Overview Block DiagramFigure 10-5 M300EU Heating Control Block Diagram 10.3.2. THE RELAY PCA10.3.2.1. Temperature Control of the Convection Oven Figure 10-6 M300EU Oven Heater Configuration Jumpers 10.3.2.2. Oven Heaters AC Power Configuration115 VAC Configuration 230 VAC Configuration10.3.3.2. Sensor Inputs 10.3.3. MOTHERBOARD10.3.2.3. Status LED’s 10.3.3.1. A to D ConversionFigure 10-8 M300EU Distribution Block Diagram 10.3.4. POWER DISTRIBUTIONRELAY PCA Page PROCEDURES 11. TROUBLESHOOTING & REPAIR11.1. GENERAL NOTES MAINTENANCE PERSONNEL ONLYTable continued on next page 11.2. FAULT DIAGNOSIS WITH WARNING MESSAGESWarning Messages - Indicated Failures Sample flow rate is Warning Messages - Indicated Failures contINDICATED FAILURES 11.2.1. FAULT DIAGNOSIS WITH TEST FUNCTIONSTable 11-2 Test Functions - Indicated Failures table continuedValues outside range indicate Test Functions - Indicated FailuresVoltage displayed should change. If not 11.2.2. RELAY BOARD STATUS LED’SFaulty Connectors/Wiring Table 11-3 Relay Board Status LED Failure Indications11.4.1. Unexplained DRIFT 11.3. GAS FLOW PROBLEMS11.4. OTHER PERFORMANCE PROBLEMS 11.5.2.1. A/D Functions 11.5. SUBSYSTEM CHECHOUT11.5.1. RELAY BOARD 11.5.2. MOTHERBOARD11.6. TECHNICAL ASSISTANCE Addendum to M300E/EM Manual P/N M300EU Addendum to M300E/EM Manual APPENDIX A - Version Specific Software DocumentationAPPENDIX A-2 M300EU Setup Variables Available Via Serial I/O APPENDIX A-4 M300EU Signal I/O DefinitionsMSG1 CLR1TEST1 Figure A-2 Primary Setup Menu Except iDAS Figure A-3 Primary Setup Menu Æ iDAS Submenu Figure A-4 Secondary Setup Menu Æ COMM and VARS Submenus Figure A-5 Secondary Setup Menu Æ Hessen Protocol Submenu Press ENTR ENTER PASSWORDAuto Cal feature is OFF or the range is set for Figure A-6 DIAG MenuTable continues APPENDIX A-2 Setup Variables For Serial I/O, Revision K.6APPENDIX A-2 Setup Variables For Serial I/O, Revision K.6 CO2FILTPCT STDO2CELLTEMP A-10O2FILTPCT A-11 APPENDIX A-3 Warnings and Test Functions, Revision K.6NAME MESSAGE TEXTThese gases not applicable to the M300EU Table A-5A-12 These gases not applicable to the M300EUNumber Signal NameBit or Channel DescriptionA-14 APPENDIX A-5 M300EU iDAS Parameters Revision K.6OVTMPW Internal box temperature #2/oven warning O2OFST A-15CO2OFS O2SLPEA-16 APPENDIX A-6 Terminal Command Designators, Revision K.605925 Rev A APPENDIX B - M300EU SPARE PARTS & EXPENDABLESAPPENDIX B - M300EU SPARE PARTS & EXPENDABLES European standard ENM300EU Addendum to M300E/EM Manual