Teledyne Trace Oxygen Analyzer operating instructions Operational Theory Model 3000TA-XL-EU

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2 Operational Theory

Model 3000TA-XL-EU

 

 

 

 

 

 

 

 

 

comes from outside the device as a constituent of the sample gas being analyzed. The Micro-Fuel Cell is therefore a hybrid between a battery and a true fuel cell. (All of the reactants are stored externally in a true fuel cell.)

2.2.2 Anatomy of a Micro-Fuel Cell

The Micro-Fuel Cell is a cylinder only 1¼ inches in diameter and 1¼ inches thick. It is made of an extremely inert plastic, which can be placed confidently in practically any environment or sample stream. It is effectively sealed, although one end is permeable to oxygen in the sample gas. The other end of the cell is a contact plate consisting of two concentric foil rings. The rings mate with spring-loaded contacts in the sensor block assembly and provide the electrical connection to the rest of the analyzer. Figure 2-1 illustrates the external features.

Figure 2-1: Micro-Fuel Cell

Refer to Figure 2-2, Cross Section of a Micro-Fuel Cell, which illus- trates the following internal description.

Figure 2-2. Cross Section of a Micro-Fuel Cell (not to scale)

At the top end of the cell is a diffusion membrane of Teflon, whose thickness is very accurately controlled. Beneath the diffusion membrane lies

2-2

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Contents Trace Oxygen Analyzer Teledyne Analytical InstrumentsModel 3000TA-XL-EU Copyright 1999 Teledyne Analytical InstrumentsIii Trace Oxygen Analyzer Specific Model InformationGround Protective Earth Teledyne Analytical InstrumentsTrace Oxygen Analyzer Table of Contents Introduction InstallationOperational Theory OperationMaintenance AppendixVii Trace Oxygen Analyzer AppendixCombustible GAS Usage Warning ViiiMain Features of the Analyzer OverviewTypical Applications Trace Oxygen Analyzer IntroductionModel Designations Introduction Model 3000TA-XL-EUFront Panel Operator Interface Model 3000TA-XL Front PanelIntroduction Model 3000TA-XL-EU Rear Panel Equipment Interface Analog OutputsRemote Probe RS-232 PortNetwork I/O Operational Theory Introduction Micro-Fuel Cell SensorTrace Oxygen Analyzer Operational Theory Principles of OperationOperational Theory Model 3000TA-XL-EU Anatomy of a Micro-Fuel CellElectrochemical Reactions + 2H 2O + 4e → 4OHCalibration Characteristics Effect of PressureCharacteristic Input/Output Curve for a Micro-Fuel Cell Sample SystemTOP Flow Diagram-Sample Under Pressure Standard Model Electronics and Signal Processing Electronic Component Location Inside the Model 3000TA-XLBlock Diagram of the Model 3000TA-XL Electronics Operational Theory Model 3000TA-XL-EU Unpacking the Analyzer Trace Oxygen Analyzer InstallationMounting the Analyzer Installation Model 3000TA-XL-EU Rear Panel ConnectionsGas Connections Rear Panel of the Model 3000TA-XL2.2 50-Pin Equipment Interface Connector PrimaryInputPowerElectrical Connections Equipment Interface Connector Pin Arrangement Pin FunctionPin Contact Remote Calibration Connections Range ID Relay Connections 2.3 RS-232 Port FET Series ResistanceCommand Description Parameter SettingInstalling the Micro-Fuel Cell Testing the SystemRemoving the Micro-Fuel Cell Trace Oxygen Analyzer Operation Auto Ranging onUsing the Data Entry and Function Buttons Operation Model 3000TA-XL-EUSystem Function Analyze SystemOperation Model 3000TA-XL-EU Setting up an Auto-Cal Password Protection Entering the Password Installing or Changing the Password System Self-Diagnostic Test LogoutVersion Screen Calibration of the Analyzer Span Gas CalibrationAir Calibration Zero CalAuto Mode Zeroing Manual Mode ZeroingCell Failure Auto Mode Spanning Operation Model 3000TA-XL-EU Span CalManual Mode Spanning Switching of Sample Streams Span FailureAlarms Function Special Notes on Hydrogen Gas StreamAL-1 AL-2 Choose Alarm Range Function Setting the Analog Output Ranges Fixed Range AnalysisSignal Output Analyze FunctionRange Voltage Current mA MEDRoutine Maintenance Cell ReplacementTrace Oxygen Analyzer Maintenance Storing and Handling Replacement CellsMaintenance Model 3000TA-XL-EU When to Replace a Cell Removing the Micro-Fuel CellRemoving the Micro-Fuel Cell Warranty Fuse Replacement Removing Fuse Block from HousingMaintenance Model 3000TA-XL-EU System Self Diagnostic TestMajor Internal Components Cleaning Rear-Panel ScrewsTroubleshooting SolutionSpecifications Operating Temperature 5-35 C AppendixRecommended 2-Year Spare Parts List Drawing List 19-inch Relay Rack Panel Mount3000XL Series Analyzers Conversions Page Material Safety Data Sheet Section IV Fire and Explosion Hazard Data Protective measures during cell replacement ExposureSection Viii Control Measures Read completely before beginning the procedure
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