Emerson 51-DO-03, DO-04 Process readings are erratic, Readings drift, Oxygen readings are too low

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MODEL DO-03/04

SECTION 10.0

 

TROUBLESHOOTING

10.4.6 Process readings are erratic.

A.Readings are often erratic when a new sensor or a rebuilt sensor is first placed in service. The current usual- ly stabilizes after a few hours.

B.Is the sample flow within the recommended range? High sample flow may cause erratic readings. Refer to the sensor instruction manual for recommended flow rates.

C.Gas bubbles impinging on the membrane may cause erratic readings. Orienting the sensor at an angle away from vertical may reduce the noise.

D.The holes between the membrane and electrolyte reservoir might be plugged. Refer to Section 10.4.2.

E.Verify that wiring is correct. Pay particular attention to shield and ground connections.

F.Is the membrane in good condition and is the sensor filled with electrolyte solution? Replace the fill solution and electrolyte. Refer to Section 9.2 for details.

10.4.7 Readings drift.

A.Is the sample temperature changing? Membrane permeability is a function of temperature. The time constant for response to a temperature change is about 5 minutes. Therefore, the reading may drift for a while after a sudden temperature change.

B.Is the membrane clean? For the sensor to work properly oxygen must diffuse freely through the membrane. A coating on the membrane will interfere with the passage of oxygen, resulting in slow response.

C.Is the sensor in direct sunlight? If the sensor is in direct sunlight during air calibration, readings will drift as the sensor warms up. Because the temperature reading lags the true temperature of the membrane, calibrating the sensor in direct sunlight may introduce an error.

D.Is the sample flow within the recommended range? Gradual loss of sample flow will cause downward drift.

E.Is the sensor new or has it been recently serviced? New or rebuilt sensors may require several hours to sta- bilize.

10.4.8 Sensor does not respond to changes in oxygen level.

A.If readings are being compared with a portable laboratory instrument, verify that the laboratory instrument is working.

B.Is the membrane clean? Clean the membrane and replace it if necessary. Also, increase the frequency and duration of the air blast. Check that the holes at the base of the cathode stem are open. Use a straightened paper clip to clear blockages. Replace the electrolyte solution.

C.Replace the sensor.

10.4.9 Oxygen readings are too low.

A.Low readings can be caused by zeroing the sensor before the residual current has reached a stable minimum value. Residual current is the current the sensor generates even when no oxygen is in the sample. Because the residual current is subtracted from subsequent measured currents, zeroing before the current is a mini- mum can lead to low results.

Example: the true residual (zero) current for a 499ADO sensor is 0.05 μA, and the sensitivity based on cali- bration in water-saturated air is 2.35 μA/ppm. Assume the measured current is 2.00 μA. The true concentra- tion is (2.00 - 0.05)/2.35 or 0.83 ppm. If the sensor was zeroed prematurely when the current was 0.2 μA, the

measured concentration will be (2.00 - 0.2)/2.35 or 0.77 ppm. The error is 7.2%. Suppose the measured cur- rent is 5.00 μA. The true concentration is 2.11 ppm, and the measured concentration is 2.05 ppm. The error is now 3.3%. The absolute difference between the readings remains the same, 0.06 ppm.

B.Sensor response depends on flow. If the flow is too low, readings will be low and flow sensitive. Move the sen- sor to an area in the aeration basin where the flow or agitation is greater.

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Contents Dissolved Oxygen Measurement System with Air Blast Cleaner Model DO-03/04Essential Instructions Page Model DO-03/04 Measuring System Section Title10.0 List of Tables11.0 Section Title List of FiguresIii Section Specifications Features and BenefitsPower Repeatability ±0.05 ppm 25CRFI/EMI EN-61326 Output Accuracy ± 0.05 mAMaximum distance between compressor and sensor Maximum continuous pressure 50 psig 446 kPa absMaterials of Construction Analyzer dimensions Enclosure dimensions Description Power required selection9240048-00 Tag, stainless steel, specify marking Section Installation InstallationUnpacking and Inspection Model or part number DescriptionInstalling the handrail mounting assembly Installing the air compressor enclosureAssembling the pipe and pipe clamp Attaching the pipe boom to the handrail mounting assembly Installing the sensor in the washer head assemblyAssembling the washer head and pipe boom Attaching the air compressor enclosure to the handrail Installing the sensor in the washer head assembly POWER, ALARM, and Output Wiring Section WiringGeneral 454EPH02 Section Section Wiring the Oxygen Sensor Sensor WiringGeneral Alarm Status Section Display and OperationDisplay KEY Functions and ControlSection Software Configuration Menu Tree for the 54eA AnalyzerOn following Main Menu Calibrate See Diagnostic Variable see Program Settings List Choices Factory Settings SetpointsChoices Factory Settings Configure Choices Factory Settings Alarm setpoints Alarm 1 setpointAlarm 2 setpoint Alarm 3 setpointMA 0.00 ppm 20 mA 20.00 ppm Output 1 12.00 mA Ranging the OutputsSimulated tests Test alarm 1 OpenTest output Outputs Alarms DisplayMeasure Oxygen Meas units ppmTemp units C Output 1 mA Output 2 mA Display contrast Timeout OnLanguage English Display left Display right Out Output 1 control OutputsOutput Measurement Output 1 Control Output 1 SetupRange 4-20 mA Dampen 0 sec Hold Last Value Configure Alarm 1 controlAlarm 1 setup Alarm 2 control Changing Alarm ParametersAlarm 1 control Alarm 1 setupAlarm Low Activate ProcessAlarm Fault Feed limit DisableTimeout 3600 sec Alarm 4 setupAlarm 4 setup Feed limit timer Interval timerTimer Disable Timer Time activated Interval 24.0 hr Interval timer setupTemperature Compensation and Temperature Units Temp comp AutoTemp units C Temp comp Manual Temp units C60 Hz Noise ReductionBar units mm Hg Bar meas AutoBarometric Pressure Main sensor cal Salinity 0.0 o/ooNoise rejection Main sensor cal Security SecurityCondition Definitions Analyzer Mode PriorityAction Definitions Section Calibration Temperature IntroductionAdjust temp + 025.1 C Temperature CalibrationSection Calibration Dissolved Oxygen Sensor Current as a Function Dissolved Oxygen ConcentrationSensor must be in zero solution Zeroing the SensorStabilizing . . . Wait Calibrating the Sensor in AIRSection Calibrate 8.32 ppm Calibrating the Sensor Against a Standard InstrumentZero main sensor Adjust temperature Calibrate main sensorStandardize Calibrating Barometric PressureSection Calibration Current Outputs Trimming the OutputsSection Maintenance Replacement PartsCleaning the membrane Replacing electrolyte solution and membraneSection Power Fuse Spare PartsReplacement Parts Location Part Number Description AIR Blast Sensor WasherSection Troubleshooting Troubleshooting When a Fault Message is ShowingFault message Explanation See Section Overview Temperature error low or high High input current Check sensor zero Sense line openProblem See Section Troubleshooting When no Fault Message is Showing OxygenZero current is too high Zero reading Is unstable Possible error warning during in-process calibrationBarometric pressure reading is too high or too low Process readings are erratic Readings driftSensor does not respond to changes in oxygen level Oxygen readings are too lowTroubleshooting not Related to Measurement Problems Problem ActionSimulating Inputs Dissolved Oxygen Sensor Polarizing Voltage Resistance Expected currentSimulating Temperature Simulating temperatureSection Return of Material GeneralReturn of Materials Request Sensor or Circuit Board onlyWarranty Specifications subject to change without notice