Emerson DO-03 Zero reading Is unstable, Possible error warning during in-process calibration

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MODEL DO-03/04

SECTION 10.0

 

TROUBLESHOOTING

10.4.2 Zero reading Is unstable.

A.Is the sensor properly wired to the analyzer? See Section 3.3. Verify that all wiring connections are tight.

B.Readings are often erratic when a new or rebuilt sensor is first placed in service. Readings usually stabilize after an hour.

C.Is the space between the membrane and cathode filled with electrolyte solution and is the flow path between the electrolyte reservoir and the membrane clear? Often the flow of electrolyte can be started by simply hold- ing the sensor with the membrane end pointing down and sharply shaking the sensor a few times as though shaking down a clinical thermometer. If shaking does not work, perform the checks below. Refer to the sensor instruction manuals for additional information.

Verify that the holes at the base of the cathode stem are open (use a straightened paperclip to clear the holes). Also verify that air bubbles are not blocking the holes. Fill the reservoir and establish electrolyte flow to the cathode. Refer to the sensor instruction manual for the detailed procedure.

10.4.3 Sensor can be calibrated, but current in air is too high or too low

A.Is the sensor properly wired to the analyzer? See Section 3.3. Verify that all connections are tight.

B.Is the membrane dry? The membrane must be dry during air calibration. A droplet of water on the membrane during air calibration will lower the sensor current and cause an inaccurate calibration.

C.If the sensor current in air is very low and the sensor is new, either the electrolyte flow has stopped or the mem- brane is torn or loose. For instructions on how to restart electrolyte flow see Section 10.4.2. To replace a torn membrane, refer to Section 9.2.

D.Is the temperature low? Sensor current is a strong function of temperature. The sensor current decreases about 3% for every °C drop in temperature.

E.Is the membrane fouled or coated? Slime, oil, and solids inhibit diffusion of oxygen through the membrane, reducing the sensor current. Clean the membrane by rinsing it with a stream of water from a wash bottle or by gently wiping the membrane with a soft tissue. Also, increase the air blast cleaning frequency and duration. If cleaning the membrane and increasing the air blast frequency do not improve the sensor response, replace the membrane and electrolyte solution. If necessary, polish the cathode. See Section 9.2 for more information.

10.4.4 Possible error warning during in-process calibration

This error warning appears if the current process reading and the reading it is being changed to, ie, the reading from the standard instrument, are appreciably different.

A.Is the standard instrument properly zeroed and calibrated?

B.Are the standard and process sensor measuring the same sample? Place the sensors as close together as possible.

C.Is the process sensor working properly? Check the response of the process sensor in air and in sodium sul- fite solution.

10.4.5 Barometric pressure reading is too high or too low.

A.Is the pressure inside the enclosure equal to ambient pressure? The pressure sensor is inside the analyzer enclosure. When cable glands are in place and the front panel is tightly closed, the enclosure is moderately airtight. Therefore, as the air trapped in the enclosure heats or cools, the pressure inside the enclosure may be different from ambient. Open the front door to equalize the pressure.

B.If equalizing the pressure does not solve the problem, the pressure sensor is out of calibration. Calibrate the sensor against the local barometric pressure. Be sure to use the actual barometric pressure. Pressure, some- times called altimeter, from a local airport or pressure from a weather forecasting service is usually corrected to sea level. It is not the actual barometric pressure.

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Contents Model DO-03/04 Dissolved Oxygen Measurement System with Air Blast CleanerEssential Instructions Page Section Title Model DO-03/04 Measuring SystemList of Tables 10.011.0 List of Figures Section TitleIii Features and Benefits Section SpecificationsOutput Accuracy ± 0.05 mA PowerRepeatability ±0.05 ppm 25C RFI/EMI EN-61326Maximum continuous pressure 50 psig 446 kPa abs Maximum distance between compressor and sensorMaterials of Construction Analyzer dimensions Enclosure dimensions Power required selection Description9240048-00 Tag, stainless steel, specify marking Model or part number Description Section InstallationInstallation Unpacking and InspectionInstalling the air compressor enclosure Installing the handrail mounting assemblyAssembling the pipe and pipe clamp Installing the sensor in the washer head assembly Attaching the pipe boom to the handrail mounting assemblyAssembling the washer head and pipe boom Attaching the air compressor enclosure to the handrail Installing the sensor in the washer head assembly Section Wiring POWER, ALARM, and Output WiringGeneral 454EPH02 Section Section Sensor Wiring Wiring the Oxygen SensorGeneral KEY Functions and Control Alarm StatusSection Display and Operation DisplayMenu Tree for the 54eA Analyzer Section Software ConfigurationOn following Main Menu Calibrate See Diagnostic Variable see Choices Factory Settings Setpoints Program Settings ListChoices Factory Settings Configure Choices Factory Settings Alarm 3 setpoint Alarm setpointsAlarm 1 setpoint Alarm 2 setpointRanging the Outputs MA 0.00 ppm 20 mA 20.00 ppm Output 1 12.00 mATest alarm 1 Open Simulated testsTest output Meas units ppm Outputs AlarmsDisplay Measure OxygenDisplay contrast Timeout On Temp units C Output 1 mA Output 2 mALanguage English Display left Display right Out Outputs Output 1 controlOutput Measurement Output 1 Setup Output 1 ControlRange 4-20 mA Dampen 0 sec Hold Last Value Changing Alarm Parameters ConfigureAlarm 1 control Alarm 1 setup Alarm 2 controlActivate Process Alarm 1 controlAlarm 1 setup Alarm LowAlarm 4 setup Alarm FaultFeed limit Disable Timeout 3600 secInterval timer setup Alarm 4 setup Feed limit timerInterval timer Timer Disable Timer Time activated Interval 24.0 hrTemp comp Manual Temp units C Temperature Compensation and Temperature UnitsTemp comp Auto Temp units CNoise Reduction 60 HzBar meas Auto Bar units mm HgBarometric Pressure Salinity 0.0 o/oo Main sensor calSecurity Noise rejection Main sensor cal SecurityAnalyzer Mode Priority Condition DefinitionsAction Definitions Introduction Section Calibration TemperatureTemperature Calibration Adjust temp + 025.1 CSensor Current as a Function Dissolved Oxygen Concentration Section Calibration Dissolved OxygenZeroing the Sensor Sensor must be in zero solutionCalibrating the Sensor in AIR Stabilizing . . . WaitSection Calibrating the Sensor Against a Standard Instrument Calibrate 8.32 ppmCalibrating Barometric Pressure Zero main sensor Adjust temperatureCalibrate main sensor StandardizeTrimming the Outputs Section Calibration Current OutputsReplacing electrolyte solution and membrane Section MaintenanceReplacement Parts Cleaning the membraneSection Spare Parts Power FuseAIR Blast Sensor Washer Replacement Parts Location Part Number DescriptionOverview Section TroubleshootingTroubleshooting When a Fault Message is Showing Fault message Explanation See SectionSense line open Temperature error low or highHigh input current Check sensor zeroTroubleshooting When no Fault Message is Showing Oxygen Problem See SectionZero current is too high Possible error warning during in-process calibration Zero reading Is unstableBarometric pressure reading is too high or too low Oxygen readings are too low Process readings are erraticReadings drift Sensor does not respond to changes in oxygen levelSensor Polarizing Voltage Resistance Expected current Troubleshooting not Related to Measurement ProblemsProblem Action Simulating Inputs Dissolved OxygenSimulating temperature Simulating TemperatureGeneral Section Return of MaterialSensor or Circuit Board only Return of Materials RequestWarranty Specifications subject to change without notice