Teledyne M5000B operating instructions Operations/Analysis Unit

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4 Operations/Analysis Unit

instrument is set up to analyze, then the SPAN control must be adjusted for a full scale reading, i. e., 200 ppm water in EDC.

10.Re-checktheZEROsettingwithzerofluid.

11.If desired, the linearity of the analyzer can be checked with a fluid intermediateinconcentrationbetweenthezeroandthespanfluid.

12.The analyzer is now calibrated. It is often desirable to check calibration (fine tune) on a dynamic sample from your process, double checking the 5020 analyzer response with laboratory analyzed grab samples. This is desirable where there is a possibility that your sample stream may have some background materials not in the makeup of the calibration fluid.

13.From time to time, re-check the zero setting. If it is found that there is no zero drift, re-checking the zero setting may become unnecessary or may be performed only on an occasional basis.

14.Some optical filters used in some applications will be so temperature sensitive that screening must be performed with the filters near the operating temperature.

DIRECTIONS FOR USING TELEDYNE CALIBRATION OPTIONS

FOR ON-LINE PROCESS PHOTOMETRIC ANALYZERS

IGeneral

These calibration options consists of procedures for calibrating analyzers on-line. These techniques are offered when process conditions (high pressures, temperatures, sample phase changes) are extremely difficult to deal with and calibration standards are impossible, difficult to obtain, are too expensive to use due to volume consumption into the system, are unstable, or are difficult to introduce into the analyzer or sample system because of toxicity, pressure, etc. Also many times the sample stream composition is difficult to match with a calibration fluid.

In one case an optical absorbing filter(s) is inserted into the light path of the analyzer. The absorber is actuated by a switch(s) located on the readout panel of the control unit. The option functions by pre- senting a calibrated and reproducible absorbance or fluid into the light path of the analyzer.

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A Business Unit of Teledyne Electronic Technologies

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Contents Photometric Analyzer Teledyne Analytical InstrumentsModel 5000B Copyright 1999 Teledyne Analytical InstrumentsTable of Contents IiiModel 5000B Teledyne Analytical Instruments Part I Part I Control UnitIi Part InstallationOperation Maintenance Iv Part Model 5000B Photometric AnalyzerTypical Applications OverviewPhotometric Analyzer Part I Control Unit Introduction Model 5000B Other NIR Absorbers that can be measured consult factory Introduction Model 5000B Main Features of the Analyzer ESCAPE/ENTER Switch 1 UP/DOWN SwitchOperator Interface Model 5000B Controls, Indicators, and Connectors Control Section Interface Panel Model 5000B Interface Panel Introduction Model 5000B Installation Unpacking the Control/Analysis UnitPart Primary Input Power Connections 115VACExamples Analog Output ConnectionsAlarm Relays Range Voltage Current mATypes of Relay Contacts The connectors are Part I RS-232 Signals RS-232 Sig RS-232 Pin PurposeCommand Description Testing the SystemParameter Setting Part Operation Photometric Analyzer Operation /Control UnitOperation/Control Unit Hierarchy of System Functions and Subfunctions Setting up an AUTO-CAL System FunctionSelect More and press the Enter Key PasswordProtection Entering the PasswordInstalling or Changing the Password Logging Out System Self-Diagnostic Test Model Screen CheckingLinearitywithALGORITHMDigital Filter Setup Setting 90% Response time secondsFilter or Solenoid Setup Hold/Track Setup Calibration/Hold Timer SetupCalbrt hold 3 min Sample hold 1 min Analog 4 to 20 mA Output CalibrationUse UP/DOWN arrow to Adjust 4 ma 250 ModelShow Negative Auto Mode ZeroingZero Cal Manual Mode Zeroing Cell Failure SccmManual Mode Spanning Auto Mode SpanningSpan Cal How to access the offset function Offset FunctionSelect zero mode Auto Select zero mode MAN Zero off 0.0 ppm ENT to begin ZeroAlarms Function AL1 1ØØØ ppm HI DftN FsN LtchN Range Select Function Manual Select/Define Range ScreenAuto Screen Precautions 2illustratestheseschemesgraphically Analyze Function Set Range Screen Algorithm Application More Curve Algorithm Screen Auto Mode Linearization Fuse Replacement Part I Control Unit/Analysis Unit MaintenanceSystem Self Diagnostic Test Maintenance Model 5000B Photometric AnalyzerPower AnalogPreamp Cell detectorPart Part II Part II Analysis UnitRoutine Maintenance Part II Analysis Unit Appendix Iv Part Operations/Analysis Unit Control Functions Explosion-ProofVersionControlModuleControl Settings Start-pPreliminaryInspection Analyzers not equipped with Auto ZeroPower On Observations Pre-Start-upElectricalCheckoutTeledyneAnalyticalInstruments4-5 Calibration ProcedureStandardizationFluids TeledyneAnalyticalInstruments4-7 Operations/Analysis Unit TeledyneAnalyticalInstruments4-9 Operations/Analysis Unit TeledyneAnalyticalInstruments4-11 Operations/Analysis Unit TeledyneAnalyticalInstruments4-13 Ppm simulated water using Span Zero SampleAttachment 5000B/5020 NIR Analyzer Operations/Analysis Unit Operational Theory Contd Source Module OpticalSystem Sample cellAnalyzerSystem-BlockDiagram Power Module Block Diagram Detectorcompartment Routine Maintenance Part II Maintenance/Analysis UnitSystem Visual Check and Response Procedure Automatic operation and routine operational dutiesSuggested Preventive Maintenance Schedule DailyEquipment Required Oscilloscope Display of the I to E Converter Output Part II Maintenance/Analysis Unit Setup of the Logarithmic Amplifier Inverting AmplifierBattery-Powered Oscilloscope Synchronization Point Interface Board Terminals StripPart Part II Maintenance/Analysis Unit Part Operating Temperature 0-50oC SpecificationsPhotometric Analyzer, 5000B Appendix Appendix Models 5000B Other Features Recommended 2-Year Spare Parts List QtyP/NDescriptionDrawing List, 5000B Appendix Models 5000B Teledyne Analytical Instruments