Teledyne M5000B operating instructions Attachment 5000B/5020 NIR Analyzer

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4 Operations/Analysis Unit

ATTACHMENT 5000B/5020 NIR ANALYZER

Quote "Exceptions" and "LIQUID PHASE Conditions" for this application.

1Response Time is proportional to sample system design for take-off distance, process pressure, line size, sequencing and bypass, by-pass analyzer flow design, dead-volumes/tee's, sample cell volume and instrument electronics.

2Maximum cell operation pressure to be 175 psig, based upon standard Sapphire window cell design. Higher pressures available.

3The sample flow through the analyzer should be regulated to within ± 5% of its recommended absolute nominal set point flow value (typically 20-60ccm). This will avoid any pressure drops across any orifices or poor temperature control of the sample.

4The temperature of the sample from the take-off thorough the sample cell must be non-freezing, non- crystallizing, non-coating as provided by customer.

5The sample temperature should not vary at the inlet more than ± 15 OC of the calibration temperature, nor exceed the design operating specifications typically5-45 OC. Assume sample below 45 C and requires no cooling.

6Any background components later found to be present and not specified in the original application feasibility may void the instrument performance should they interfere. particulates assumed none.

7If compounds are found present, such as moisture, acid gases or corrosive solvents, etc., the sample system materials may be compromised for corrosion resistance integrity. We assume that the sample will not polymerize, clog or react in any 1/4" sample line, filter or sample cell when transporting through the sample systems for all inlet ambient or sample pressures and temperatures from takeoff or derived from sample conditioning. Special materials may be required for stability, corrosion protection, coalesc- ing, filtering, hazardous protection or due to heating or cooling.

8We recommend when ambient temperatures exceed outside a 1-50 OC range that the instrument and sample system be conditioned appropriately for heating/ cooling without condensation, crystallizing, coating, polymerization, etc.

9Should the general purpose or explosion proof instrument be supplied on a back-panel or as a bulk- mount housing, the customer must install to protect the instrument to meet harsh ambient conditions for dust, water, snow, wind, corrosion, etc.

10Teledyne is not responsible for applying a general purpose instrument in a hazardous area or where a flammable or toxic gas or liquid is brought to an analyzer above its lower explosive limit and the area has been classified as general purpose and safe.

11The internal calibration features using optical filters are optimized and used when the sample can be flushed (backflushed usually) out of the sample cell using dry nitrogen or air to a reproducible back- ground zero. The zero offset and/or span flag is introduced and set-up to simulate the on-line calibration only after the customer has calibrated the analyzer on the representative process fluid. Thereafter, no calibration fluids are needed to check analyzer.

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Contents Photometric Analyzer Teledyne Analytical InstrumentsModel 5000B Copyright 1999 Teledyne Analytical InstrumentsTable of Contents IiiModel 5000B Teledyne Analytical Instruments Part I Part I Control UnitInstallation Ii PartOperation Maintenance Iv Part Model 5000B Photometric AnalyzerOverview Typical ApplicationsPhotometric Analyzer Part I Control Unit Introduction Model 5000B Other NIR Absorbers that can be measured consult factory Introduction Model 5000B Main Features of the Analyzer 1 UP/DOWN Switch ESCAPE/ENTER SwitchOperator Interface Model 5000B Controls, Indicators, and Connectors Control Section Interface Panel Model 5000B Interface Panel Introduction Model 5000B Installation Unpacking the Control/Analysis UnitPart Primary Input Power Connections 115VACExamples Analog Output ConnectionsAlarm Relays Range Voltage Current mATypes of Relay Contacts The connectors are Part I RS-232 Signals RS-232 Sig RS-232 Pin PurposeTesting the System Command DescriptionParameter Setting Part Operation Photometric Analyzer Operation /Control UnitOperation/Control Unit Hierarchy of System Functions and Subfunctions Setting up an AUTO-CAL System FunctionSelect More and press the Enter Key PasswordProtection Entering the PasswordInstalling or Changing the Password Logging Out System Self-Diagnostic Test Model Screen CheckingLinearitywithALGORITHMDigital Filter Setup Setting 90% Response time secondsFilter or Solenoid Setup Hold/Track Setup Calibration/Hold Timer SetupCalbrt hold 3 min Sample hold 1 min Analog 4 to 20 mA Output CalibrationUse UP/DOWN arrow to Adjust 4 ma 250 ModelAuto Mode Zeroing Show NegativeZero Cal Manual Mode Zeroing Cell Failure SccmAuto Mode Spanning Manual Mode SpanningSpan Cal How to access the offset function Offset FunctionSelect zero mode Auto Select zero mode MAN Zero off 0.0 ppm ENT to begin ZeroAlarms Function AL1 1ØØØ ppm HI DftN FsN LtchN Range Select Function Manual Select/Define Range ScreenAuto Screen Precautions 2illustratestheseschemesgraphically Analyze Function Set Range Screen Algorithm Application More Curve Algorithm Screen Auto Mode Linearization Fuse Replacement Part I Control Unit/Analysis Unit MaintenanceSystem Self Diagnostic Test Maintenance Model 5000B Photometric AnalyzerPower AnalogPreamp Cell detectorPart Part II Part II Analysis UnitRoutine Maintenance Part II Analysis Unit Appendix Iv Part Operations/Analysis Unit Control Functions Explosion-ProofVersionControlModuleControl Settings Start-pPreliminaryInspection Analyzers not equipped with Auto ZeroPower On Observations Pre-Start-upElectricalCheckoutTeledyneAnalyticalInstruments4-5 Procedure CalibrationStandardizationFluids TeledyneAnalyticalInstruments4-7 Operations/Analysis Unit TeledyneAnalyticalInstruments4-9 Operations/Analysis Unit TeledyneAnalyticalInstruments4-11 Operations/Analysis Unit TeledyneAnalyticalInstruments4-13 Ppm simulated water using Span Zero SampleAttachment 5000B/5020 NIR Analyzer Operations/Analysis Unit Operational Theory Contd Source Module OpticalSystem Sample cellAnalyzerSystem-BlockDiagram Power Module Block Diagram Detectorcompartment Routine Maintenance Part II Maintenance/Analysis UnitSystem Visual Check and Response Procedure Automatic operation and routine operational dutiesSuggested Preventive Maintenance Schedule DailyEquipment Required Oscilloscope Display of the I to E Converter Output Part II Maintenance/Analysis Unit Setup of the Logarithmic Amplifier Inverting AmplifierBattery-Powered Oscilloscope Synchronization Point Interface Board Terminals StripPart Part II Maintenance/Analysis Unit Part Specifications Operating Temperature 0-50oCPhotometric Analyzer, 5000B Appendix Appendix Models 5000B Other Features Recommended 2-Year Spare Parts List QtyP/NDescriptionDrawing List, 5000B Appendix Models 5000B Teledyne Analytical Instruments