Teledyne M5000B operating instructions TeledyneAnalyticalInstruments4-7

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Operations/Analysis Unit 4

chemical background has changed. In some cases, TAI is not able to duplicate the background your sample for purposesofopticallybalancingtheanalyzerbeforeshipment. In these cases, it is necessary for you to screen for an approximate balance, and to then electronically adjust R3 for precise balance. To do so:

1.Reset R3 to its midpoint.

2.Re-screen the filter wheel, as necessary, to obtain a measuring voltage within 10% of the reference voltage. Every time a screen is added or removed from a filter, the analyzer must be turned off, and the filter wheel removed from the analyzer. When the filter wheel is replaced in the analyzer, its rotational position is not critical, but the white backing must face in the direction of the position sensor. The filter wheel must also be securely tightened, so that no slippage or vibration can occur. See Figure 5-1.

NOTE: Refer to Figure 5-1 when installing filter screens. Screens should be installed in the filter disk cup, under the filter holder. Also, if a bal- ance ring is used, it should be placed over the screen.

c.After screening to bring the measuring voltage to within 10% of the reference voltage, adjust R3 as in step a above to make the measuring peak voltage read the same as the reference peak voltage.

5.Turn the NORM/ZERO switch to ZERO. The analysis section meter should be made to read zero by adjusting the coarse ZERO control on the analysis section power module.

6.Check the control module SPAN setting to make sure it agrees with the calibration results obtained by TAI (see Specific Application Data in the Appendix).

7.Adjust the ZERO control on the control module to give a zero reading on the control module meter.

8.Add span fluid (see Span Fluid, above) to the sample cell. Make certain that all of the zero fluid is displaced.

9.Adjust the control module SPAN control to obtain the correct meter reading with reference to the concentration of span fluid. For example, if the sample contains 100% of whatever the

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Contents Teledyne Analytical Instruments Photometric AnalyzerCopyright 1999 Teledyne Analytical Instruments Model 5000BIii Table of ContentsModel 5000B Teledyne Analytical Instruments Part I Control Unit Part IInstallation Ii PartOperation Maintenance Model 5000B Photometric Analyzer Iv PartOverview Typical ApplicationsPhotometric Analyzer Part I Control Unit Introduction Model 5000B Other NIR Absorbers that can be measured consult factory Introduction Model 5000B Main Features of the Analyzer 1 UP/DOWN Switch ESCAPE/ENTER SwitchOperator Interface Model 5000B Controls, Indicators, and Connectors Control Section Interface Panel Model 5000B Interface Panel Introduction Model 5000B Unpacking the Control/Analysis Unit InstallationPart 115VAC Primary Input Power ConnectionsAnalog Output Connections ExamplesRange Voltage Current mA Alarm RelaysTypes of Relay Contacts The connectors are Part I RS-232 Sig RS-232 Pin Purpose RS-232 SignalsTesting the System Command DescriptionParameter Setting Part Photometric Analyzer Operation /Control Unit OperationOperation/Control Unit Hierarchy of System Functions and Subfunctions System Function Setting up an AUTO-CALSelect More and press the Enter Key Entering the Password PasswordProtectionInstalling or Changing the Password Logging Out System Self-Diagnostic Test CheckingLinearitywithALGORITHM Model ScreenSetting 90% Response time seconds Digital Filter SetupFilter or Solenoid Setup Calibration/Hold Timer Setup Hold/Track SetupAnalog 4 to 20 mA Output Calibration Calbrt hold 3 min Sample hold 1 minModel Use UP/DOWN arrow to Adjust 4 ma 250Auto Mode Zeroing Show NegativeZero Cal Manual Mode Zeroing Sccm Cell FailureAuto Mode Spanning Manual Mode SpanningSpan Cal Offset Function How to access the offset functionZero off 0.0 ppm ENT to begin Zero Select zero mode Auto Select zero mode MANAlarms Function AL1 1ØØØ ppm HI DftN FsN LtchN Manual Select/Define Range Screen Range Select FunctionAuto Screen Precautions 2illustratestheseschemesgraphically Analyze Function Set Range Screen Algorithm Application More Curve Algorithm Screen Auto Mode Linearization Part I Control Unit/Analysis Unit Maintenance Fuse ReplacementAnalog System Self Diagnostic TestMaintenance Model 5000B Photometric Analyzer PowerCell detector PreampPart Part II Analysis Unit Part IIRoutine Maintenance Part II Analysis Unit Appendix Iv Part Operations/Analysis Unit Explosion-ProofVersionControlModule Control FunctionsAnalyzers not equipped with Auto Zero Control SettingsStart-p PreliminaryInspectionPre-Start-upElectricalCheckout Power On ObservationsTeledyneAnalyticalInstruments4-5 Procedure CalibrationStandardizationFluids TeledyneAnalyticalInstruments4-7 Operations/Analysis Unit TeledyneAnalyticalInstruments4-9 Operations/Analysis Unit TeledyneAnalyticalInstruments4-11 Operations/Analysis Unit TeledyneAnalyticalInstruments4-13 Ppm simulated water using Sample Span ZeroAttachment 5000B/5020 NIR Analyzer Operations/Analysis Unit Operational Theory Contd Source Module Sample cell OpticalSystemAnalyzerSystem-BlockDiagram Power Module Block Diagram Detectorcompartment Automatic operation and routine operational duties Routine MaintenancePart II Maintenance/Analysis Unit System Visual Check and Response ProcedureDaily Suggested Preventive Maintenance ScheduleEquipment Required Oscilloscope Display of the I to E Converter Output Part II Maintenance/Analysis Unit Inverting Amplifier Setup of the Logarithmic AmplifierInterface Board Terminals Strip Battery-Powered Oscilloscope Synchronization PointPart Part II Maintenance/Analysis Unit Part Specifications Operating Temperature 0-50oCPhotometric Analyzer, 5000B Appendix Appendix Models 5000B Other Features QtyP/NDescription Recommended 2-Year Spare Parts ListDrawing List, 5000B Appendix Models 5000B Teledyne Analytical Instruments