Teledyne M5000B operating instructions Cell Failure, Sccm

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3 Operation/Control Unit

Model 5000B

 

 

 

 

 

 

 

 

 

####.## % SO2 Zero adj:2048 C—Zero

The analyzer goes through C–Zero, F–Zero, and S–Zero. During C– Zero and F–Zero, use the DÑ keys to adjust displayed Zero adj: value as close as possible to zero. Then, press Enter.

S–Zero starts. During S–Zero, the Microcontroller takes control as in Auto Mode Zeroing, above. It calculates the differences between successive samplings and displays the rate of change as Slope= a value in parts per million per second (ppm/s).

####.## % SO2 Slope=#.### S—Zero

Generally, you have a good zero when Slope is less than 0.05 ppm/s for about 30 seconds.

Once zero settling completes, the information is stored in the analyzer’s memory, and the instrument automatically returns to the Analyze mode.

3.4.1.3 Cell Failure

Detector failure in the 5000BF is usually associated with inability to zero the instrument with a reasonable voltage differential between the refer- ence and measure voltages. If this should ever happen, the 5000BF system alarm trips, and the LCD displays a failure message.

Detector cannot be balanced

Check your zero fluid

Before optical balancing:

a.Check your zero fluid to make sure it is within specifications.

b.Check for leaks downstream from the Sample Cell, where con- tamination may be leaking into the system.

c.Check flowmeter to ensure that the flow is no more than 200

SCCM

d.Check temperature controller board.

e.Check fluid temperature.

f.Check the Sample Cell for dirty windows.

If none of the above, proceed to perform an optical balance as described in section 5.

3-18 Part I

Teledyne Analytical Instruments

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Contents Photometric Analyzer Teledyne Analytical InstrumentsModel 5000B Copyright 1999 Teledyne Analytical InstrumentsTable of Contents IiiModel 5000B Teledyne Analytical Instruments Part I Part I Control UnitIi Part InstallationOperation Maintenance Iv Part Model 5000B Photometric AnalyzerTypical Applications OverviewPhotometric Analyzer Part I Control Unit Introduction Model 5000B Other NIR Absorbers that can be measured consult factory Introduction Model 5000B Main Features of the Analyzer ESCAPE/ENTER Switch 1 UP/DOWN SwitchOperator Interface Model 5000B Controls, Indicators, and Connectors Control Section Interface Panel Model 5000B Interface Panel Introduction Model 5000B Installation Unpacking the Control/Analysis UnitPart Primary Input Power Connections 115VACExamples Analog Output ConnectionsAlarm Relays Range Voltage Current mATypes of Relay Contacts The connectors are Part I RS-232 Signals RS-232 Sig RS-232 Pin PurposeCommand Description Testing the SystemParameter Setting Part Operation Photometric Analyzer Operation /Control UnitOperation/Control Unit Hierarchy of System Functions and Subfunctions Setting up an AUTO-CAL System FunctionSelect More and press the Enter Key PasswordProtection Entering the PasswordInstalling or Changing the Password Logging Out System Self-Diagnostic Test Model Screen CheckingLinearitywithALGORITHMDigital Filter Setup Setting 90% Response time secondsFilter or Solenoid Setup Hold/Track Setup Calibration/Hold Timer SetupCalbrt hold 3 min Sample hold 1 min Analog 4 to 20 mA Output CalibrationUse UP/DOWN arrow to Adjust 4 ma 250 ModelShow Negative Auto Mode ZeroingZero Cal Manual Mode Zeroing Cell Failure SccmManual Mode Spanning Auto Mode SpanningSpan Cal How to access the offset function Offset FunctionSelect zero mode Auto Select zero mode MAN Zero off 0.0 ppm ENT to begin ZeroAlarms Function AL1 1ØØØ ppm HI DftN FsN LtchN Range Select Function Manual Select/Define Range ScreenAuto Screen Precautions 2illustratestheseschemesgraphically Analyze Function Set Range Screen Algorithm Application More Curve Algorithm Screen Auto Mode Linearization Fuse Replacement Part I Control Unit/Analysis Unit MaintenancePower System Self Diagnostic TestMaintenance Model 5000B Photometric Analyzer AnalogPreamp Cell detectorPart Part II Part II Analysis UnitRoutine Maintenance Part II Analysis Unit Appendix Iv Part Operations/Analysis Unit Control Functions Explosion-ProofVersionControlModulePreliminaryInspection Control SettingsStart-p Analyzers not equipped with Auto ZeroPower On Observations Pre-Start-upElectricalCheckoutTeledyneAnalyticalInstruments4-5 Calibration ProcedureStandardizationFluids TeledyneAnalyticalInstruments4-7 Operations/Analysis Unit TeledyneAnalyticalInstruments4-9 Operations/Analysis Unit TeledyneAnalyticalInstruments4-11 Operations/Analysis Unit TeledyneAnalyticalInstruments4-13 Ppm simulated water using Span Zero SampleAttachment 5000B/5020 NIR Analyzer Operations/Analysis Unit Operational Theory Contd Source Module OpticalSystem Sample cellAnalyzerSystem-BlockDiagram Power Module Block Diagram Detectorcompartment System Visual Check and Response Procedure Routine MaintenancePart II Maintenance/Analysis Unit Automatic operation and routine operational dutiesSuggested Preventive Maintenance Schedule DailyEquipment Required Oscilloscope Display of the I to E Converter Output Part II Maintenance/Analysis Unit Setup of the Logarithmic Amplifier Inverting AmplifierBattery-Powered Oscilloscope Synchronization Point Interface Board Terminals StripPart Part II Maintenance/Analysis Unit Part Operating Temperature 0-50oC SpecificationsPhotometric Analyzer, 5000B Appendix Appendix Models 5000B Other Features Recommended 2-Year Spare Parts List QtyP/NDescriptionDrawing List, 5000B Appendix Models 5000B Teledyne Analytical Instruments