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Agilent Technologies manual Agilent 1100 Series Quaternary Pump

Models: 1100 Series

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Agilent 1100 Series Quaternary Pump

Reference Manual

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Agilent Technologies manual Agilent 1100 Series Quaternary Pump

Contents

Reference Manual Warranty Agilent 1100 Series Quaternary Pump This Book Status Indicators Installing the PumpError Messages Leak Test Pressure TestOverview of Main Assemblies Exchanging Internal Parts 127Introduction to the Quaternary Pump Cable Overview 181Control Module Screens for the Quaternary Pump Contents Contents Installing the Pump Power Consideration Power CordsSite Requirements Environment Bench SpacePhysical Specifications Type Comments Damaged Packaging Delivery ChecklistQuaternary Pump Checklist Description Quantity Unpacking the Quaternary PumpAccessory Kit Contents Quaternary Pump Accessory Kit Contents-Vacuum Degasser Recommended Stack Configuration Front View Optimizing the Stack ConfigurationStack containing the autosampler Installing the Quaternary Pump PreparationsParts required Rear of Quaternary Pump Front panel is turned off Settings, see Setting the 8-bit Configuration Switch onRemoving the Front Cover Flow Connections of the Quaternary PumpTwo wrenches 1/4-5/16 inch for capillary connections Toxic or hazardous solvents are usedFlow Connections of the Quaternary Pump Mcgv Priming and Purging the System Priming with the Pump Activity Solvent Comments Optimizing Performance Hints for Successful Use of the Quaternary Pump Procedure on Solvent Information Cleaning the Solvent Filters Prevent Blocking of Solvent FiltersChecking the Solvent Filters Operational Hints for the Vacuum Degasser Operational Hints for the Vacuum DegasserOperational Hints for the Multi Channel Gradient Valve Mcgv When to use the Continuous Seal Wash Option When to Use Alternative Seals Optimize the Compressibility Compensation SettingSolvent pure Compressibility 10-6/bar Optimize the Compressibility Compensation Setting Troubleshooting and Test Functions Troubleshooting and Test Functions Location of Status Indicators Status IndicatorsPump Status Indicator Power Supply IndicatorError Messages Timeout Shut-Down Remote Timeout Synchronization Lost Leak Leak sensor in the quaternary pump has failed open circuit Leak Sensor OpenLeak sensor in the quaternary pump has failed short circuit Leak Sensor ShortCompensation Sensor Open Compensation Sensor Short Fan Failed Open Cover Replace the top cover and foam Restart Without CoverZero Solvent Counter Pressure Above Upper Limit Pressure Below Lower Limit Pressure Signal Missing Missing Pressure Reading Pump Configuration Valve Fuse Inlet-Valve Fuse Valve 0 Failed valve a Valve FailedMotor-Drive Power Encoder Missing Inlet-Valve Missing Temperature Out of Range Temperature Limit Exceeded Position for restarting Servo Restart FailedBroken plunger Pump Head MissingIndex Limit Index Adjustment Index Missing Stroke Length Initialization Failed Wait Timeout Description Pressure TestPressure Test Positioning the blank nutInside the flow path definitely will cause the test to fail Running the Pressure TestRunning the test from the ChemStation Running the test from the Control ModuleRunning the Pressure Test If the pressure test fails Evaluating the ResultsPotential Causes of Pressure Test Failure Potential Cause Pump Corrective ActionPotential Cause Autosampler Leak Test Half of the ramp Start the test and follow the instructions Tools required ¼ inch wrench Parts and materialsRunning the Leak Test Leak Test Pressure Profile No Pressure increase at Ramp Potential Cause Corrective ActionPotential Cause First plateau positive, second and third plateau negative All plateaus negativeFirst plateau negative, second plateau positive Ramp 3 does not reach limitThird plateau negative pressure drop 2 bar/min Evaluating the Results Repairing the Pump Exchanging Internal Parts Simple RepairsCleaning the Quaternary Pump Using the ESD Strap Using the ESD StrapOverview Overview of Repair ProceduresSimple Repair Procedures Typical Frequency Simple Repair ProceduresExchanging the Valve Cartridge Exchanging the Active Inlet ValveCartridge or the Active Inlet Valve Removing the Active Inlet ValveReplacing the Active Inlet Valve 105 Exchanging the Outlet Ball Valve 107 Purge Valve Exchanging the Purge Valve Frit orExchanged Head Assembly Removing and Disassembling the PumpDamage the pump drive 111 Tools required Exchanging the Pump Seals and Seal Wear-in ProcedureWhen required For the seal wear-in procedureSeal Wear-in Procedure Will definetely damage the normal phase application seals0905-1420 Exchanging the Pump Seals and Seal Wear-in Procedure Parts Exchanging the PlungersInstalling the Continuous Seal Wash Option 117 Lifetime of the seals 119 Exchanging the Wash SealsExchanging the Wash Seals Mm hexagonal key Pump head grease Reassembling the Pump Head AssemblyReassembling the Pump Head Assembly Procedure Exchanging the Multi-Channel GradientValve Mcgv 124 125 Exchanging the optional Interface Board Exchanging Internal Parts Remove the solvent cabinet from the quaternary pump Removing the Top Cover and Foam129 130 Exchanging the Low Pressure Pump Main Board LPM Board LPM Board ConnectorsMcgv Connector DescriptionWA R NI N G T E Entering the Type Command using the Control Module Entering the Type CommandEntering the Type Command using the ChemStation Entering the Serial Number using the Control ModuleEntering the Serial Number Entering the Serial Number using the ChemStation Replacing the Quaternary Pump’s Firmware Exchanging the Damper Disconnect the two damper capillaries Reconnect the two damper capillaries Fan and arrow on the bottom foam Exchanging the Fan142 Part required Exchanging the Pump Drive144 Reinstall the pump head and fix with the two screws Tubings and cables Preparation for this procedure Exchanging the Power Supply148 149 150 Exchanging the Power Supply Exchanging the Leak Sensor 153 Part required Exchanging the Status Light PipeAssembling the Main Cover Cover kit contains all parts, but it is not assembledMay not be able to remove the side from the top part Procedure Located in its correct place Replacing the Top Cover and FoamTools required Screwdriver Pozidriv #1 Location of foam in the light switch 158 Parts and Materials Overview of Main Assemblies Overview of Main Assemblies Repair Parts Pump Housing and Main Assemblies Front ViewRepair Parts Pump Housing and Main Assemblies Rear View Control Module B-version Solvent Cabinet Solvent Cabinet Parts Description Part NumberSolvent Cabinet Parts Bottle Head Assembly Bottle-Head Assembly Parts Description Part NumberBottle-Head Assembly Parts Hydraulic Path Hydraulic Path Description Part NumberHydraulic Flow Path of the Quaternary Pump Cover Parts Cover Parts Description Part NumberCover Parts Sheet Metal Kit Sheet Metal Kit Description Part NumberSheet Metal Kit Foam Parts Foam Parts DescriptionFoam Parts Power and Status Light Pipes Power and Status Light Pipes Description Part NumberPower and Status Light Pipes Leak Parts Leak Parts Description Part NumberLeak Parts Pump Head Assembly Description Part Number Pump Head Assembly173 Pump Head Assembly with Seal Wash Option 175 Outlet Ball Valve Assembly Outlet Ball Valve Assembly Description Part NumberOutlet Ball Valve Assembly Purge Valve Assembly Purge-Valve Assembly Description Part NumberPurge-Valve Assembly Active Inlet Valve Assembly Description Part Number Active Inlet Valve AssemblyTools and Accessories Description Part Number Accessory Kit G1311-68705Seal Wash Option Description Part Number Seal Wash Option KitCables Overview Type Description Part Number Cable OverviewContacts CablesAuxiliary ExternalAnalog Cables Agilent 1100 to 3390/2/3 IntegratorsAgilent 1100 to 3394/6 Integrators Agilent 1100 to General Purpose Agilent 1100 to BNC ConnectorAgilent 1100 to 3390 Integrators Remote CablesAgilent 1100 to 3394 Integrators Agilent 1100 to 3392/3 IntegratorsAgilent 1100 to 3396 Series II / 3395A Integrators Agilent 1100 to 3396A IntegratorsAgilent 1100 to 3396 Series III / 3395B Integrators TTL Connector Pin Active 01046-60202 AgilentBCD Cables Agilent 1100 to 3396 Integrators Auxiliary Cable Can CableAgilent 1100 Series Degasser to general purposes Connector Pin G1103-61611 Color External Contact CableAgilent 1100 Series Interface Board to general purposes Agilent 1100 module to PC RS-232 Cable Kit 34398A RS-232 Cable KitRecommended Cables LAN Cables196 Introduction to the Quaternary Pump Overview of the Quaternary Pump Introduction to the Quaternary Pump199 How does the Pump Work? 201 Quaternary Pump Details How Does Compressibility Compensation Work?How Does Variable Stroke Volume Work? Electrical Connections 205 Instrument Layout Seal Wear Counters Early Maintenance Feedback EMFEMF Counters Pump LiquimeterSetting the EMF Limits Using the EMF CountersLow pressure pump main board LPM, see ElectronicsLow-Pressure Pump Main Board LPM Electronic Fuses Onboard BatteryBlock Diagram Signal Explanations Fan Drive212 Interconnection Diagram Low Pressure Main Board LPM Firmware Description Resident SystemMain System Firmware Updates Optional Interface Boards BCD Board2110-0004 LAN Boards Agilent Order Number Supported networks LAN BoardAgilent 1100 Series Interfaces Agilent 1100 Series InterfacesRegulations, see Cable Overview on Analog Signal OutputGpib Interface Can InterfaceRS-232C APG Remote InterfacePin Signal Description APG Remote Signal DistributionRS-232C Connection Table Pin Direction FunctionRS-232 Cable Bit Configuration Switch Setting the 8-bit Configuration SwitchModule Address Binary Address Gpib Default AddressesCommunication Settings for RS-232C Communication Default Addresses for Agilent Series 1100 ModulesBaudrate Settings Forced cold start has been completed Forced Cold-Start SettingsStay Resident Settings Parity SettingsStay Resident Settings Main Power Supply MPS Block Diagram Main Power Supply AssemblyMain Power Supply Specifications 230 Control Module Screens for the Quaternary Pump Menu Major keys on the Agilent 1100 Control ModuleInformation/help EnterScreens available from the Analysis screen Setup View Pump ON/OFF Settings Screens available from the Analysis screen Fillings to their current state Analog -Status Screens available from the Analysis screen 241 System screen Screens available from the System screenSystem Screens available from the Records screen Counters after exchanging parts that are subject to wear Screens available from the Records screen 247 Maintenance logbook Screens available from the Records screen Schematics Tests screen Diagnostics and TestsPressure Test Specifications Type Specification Performance Specifications255 256 Warranty Statement Limitation of WarrantyAll Chemical Analysis Products Responsibilities of the Customer Limitation of Remedies and LiabilityDays Onsite Responsibilities of Agilent TechnologiesSafety Information GeneralOperation Safety Symbols Safety SymbolsSymbol Description WA R NI N G CA U T IO N Lithium Batteries Information Radio Interference Sound EmissionManufacturer’s Declaration Solvents Flow CellAgilent Technologies on Internet Index 268 269 270 Page This Book