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Agilent Technologies 1100 Series manual

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Agilent 1100 Series

Quaternary Pump

Reference Manual

Contents

Main Agilent Technologies Hewlett-Packard-Strasse 8 76337 Waldbronn Germany Warrant y ! WARNI NG Page In This Book Page Page Page Page Page Page Page Page Page Site Requirements Power Consideration Power Cords Bench Space Environment Page Unpacking the Quaternary Pump Damaged Packaging Delivery Checklist Page Page Optimizing the Stack Configuration Page Installing the Quaternary Pump Page Page Flow Connections of the Quaternary Pump Page Page Priming and Purging the System Page Page Page Hints for Successful Use of the Quaternary Pump Page Solvent Information Prevent Blocking of Solvent Filters Operational Hints for the Vacuum Degasser Operational Hints for the Vacuum Degasser Operational Hints for the Multi Channel Gradient Valve (MCGV) When to use the Continuous Seal Wash Option When to Use Alternative Seals Optimize the Compressibility Compensation Setting Page Page Page Troubleshooting and Test Functions Status Indicators Error Messages Pressure Test Leak Test Page Power Supply Indicator Pump Status Indicator Error Messages Page Shut-Down Remote Timeout Synchronization Lost Leak Leak Sensor Open Leak Sensor Short Compensation Sensor Open Compensation Sensor Short Fan Failed Open Cover Restart Without Cover Zero Solvent Counter Pressure Above Upper Limit Pressure Below Lower Limit Pressure Signal Missing Missing Pressure Reading Pump Configuration Valv e Fus e Inlet-Valve Fuse Valve Failed Motor-Drive Power Encoder Missing Inlet-Valve Missing Page Temperature Limit Exceeded Servo Restart Failed Pump Head Missing Index Limit Index Adjustment Index Missing Stroke Length Initialization Failed Wait Ti meout Pressure Test Description Positioning the blank nut Running the Pressure Test Running the test from the ChemStation Running the test from the Control Module Page Evaluating the Results If the pressure test fails: Potential Causes of Pressure Test Failure Leak Test Description Page Running the Leak Test Running the test from the ChemStation Running the test from the Control Module Page Evaluating the Results No Pressure increase at Ramp 1 Pressure limit not reached but plateaus horizontal or positive All plateaus negative First plateau positive, second and third plateau negative First plateau negative, second plateau positive Ramp 3 does not reach limit Third plateau negative (pressure drop > 2 bar/min) Page Page Repairing the Pump Simple Repairs Exchanging Internal Parts Cleaning the Quaternary Pump Using the ESD Strap Using the ESD Strap Overview Simple Repair Procedures Exchanging the Active Inlet Valve Cartridge or the Active Inlet Valve Removing the Active Inlet Valve Exchanging the Valve Cartridge Replacing the Active Inlet Valve Page Exchanging the Outlet Ball Valve Page Exchanging the Purge Valve Frit or the Purge Valve Page Removing and Disassembling the Pump Head Assembly Page Exchanging the Pump Seals and Seal Wear-in Procedure Seal Wear-in Procedure Page Exchanging the Plungers Installing the Continuous Seal Wash Option Page Page Exchanging the Wash Seals Page Reassembling the Pump Head Assembly Page Exchanging the Multi-Channel Gradient Valv e (MC GV) Page Page Exchanging the optional Interface Board Exchanging Internal Parts Removing the Top Cover and Foam Page Page Exchanging the Low Pressure Pump Main Board (LPM Board) Page Page Entering the Type Command Entering the Serial Number Page Replacing the Quaternary Pumps Firmware Exchanging the Damper Page Page Exchanging the Fan Page Exchanging the Pump Drive Page Page Page Exchanging the Power Supply Page Page Page Page Exchanging the Leak Sensor Page Exchanging the Status Light Pipe Assembling the Main Cover Replacing the Top Cover and Foam Page Page Page Overview of Main Assemblies Overview of Main Assemblies Table 9 Repair Parts - Pump Housing and Main Assemblies (Fron t View) Page Control Module (B-version) Solvent Cabinet Bottle Head Assembly Hydraulic Path Cover Parts Sheet Metal Kit Foam Parts Power and Status Light Pipes Leak Parts Pump Head Assembly Page Pump Head Assembly with Seal Wash Option Page Outlet Ball Valve Assembly Purge Valve Assembly Active Inlet Valve Assembly Accessory Kit G1311-68705 Seal Wash Option Kit 01018-68722 Cable Overview Page Analog Cables Page Remote Cables Remote Cables Agilent 1100 to 3392/3 Integrators Agilent 1100 to 3394 Integrators NOTE START and STOP are connected via diodes to pin 3 of the 3394 connector. Page Remote Cables Agilent 1100 to 3396 Series III / 3395B Integrators Agilent 1100 to HP 1050, HP 1046A or Agilent 35900 A/D Converters Page BCD Cables BCD Cables Agilent 1100 to 3396 Integrators Agilent 1100 to General Purpose Auxiliary Cable CAN Cable External Contact Cable RS-232 Cable Kit RS-232 Cable Kit Instrument PC Page Page Page Introduction to the Quaternary Pump Overview How does the Pump Work? Page How Does Compressibility Compensation Work? How Does Variable Stroke Volume Work? Electrical Connections Page Instrument Layout Early Maintenance Feedback (EMF) EMF Counters Using the EMF Counters The Electronics The Low-Pressure Pump Main Board (LPM) Page Page Page Firmware Description Resident System Main System Firmware Updates Optional Interface Boards BCD Board LAN Board Agilent 1100 Series Interfaces Analog Signal Output GPIB Interface CAN Interface APG Remote Interface RS-232C Page Instrument PC Setting the 8-bit Configuration Switch GPIB Default Addresses Communication Settings for RS-232C Communication Page Forced Cold-Start Settings Stay Resident Settings Page The Main Power Supply Assembly Page Page Page Major keys on the Agilent 1100 Control Module Screens available from the Analysis screen Page Page Page Page Page Page Page Page Page Page Page Page Page Page Page Page Page Diagnostics and Tests Page Page Performance Specifications Page Page Warranty Statement All Chemical Analysis Products Limitation of Warranty Limitation of Remedies and Liability Responsibilities of the Customer Responsibilities of Agilent Technologies Safety Information General Operation Safety Symbols ! Page Lithium Batteries Information weggooien maar inleveren als KCA. Radio Interference Sound Emission Manufacturers Declaration Solvent Information Flow Cell Solvents Page Page Page Page Page Page sa In This Book

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