Appendix C

pH Troubleshooting

Symptom

Possible Cause

Solution

 

 

 

 

 

 

Inspect the cable and connector of the faulty electrode for evidence of

 

 

 

a crushed or broken cable jacket or brittleness of the cable due to

Meter continuously

Open circuit in either

 

exposure to heat. Discard the electrode if damage is present.

Manipulate meter/electrode connections to check for intermittent

reads pH 14 or drifts

glass or reference

 

continuity. Replace if faulty.

above 14.

electrode.

 

Inspect the bulb, making sure it is filled with solution. If not, shake

 

 

 

 

 

down (like a clinical thermometer) to displace air in the pH bulb. Retest.

 

 

Inspect the bulb for signs of coating.

 

 

 

 

 

Interface is wired

Check interface wiring.

Temperature is

wrong.

 

 

constant or incorrect.

Thermistor is open.

Check interface wiring. Check for open at electrode RTD wire. Disconnect

 

to make measurement. (Should read approximately 100–110 ohms.)

 

 

 

 

 

 

 

 

Ensure that solutions are fresh and labeled properly.

 

 

Confirm that electrode and buffer temperatures have stabilized.

Electrode won’t

Gain or offset error.

Confirm that the wetting cap is removed.

calibrate.

Check bulb for cracks or other damage.

 

 

 

Confirm that interface wires are connected properly.

 

 

Check interface connections for corrosion.

 

 

 

 

 

 

Inspect the pH bulb for coating or clogging. If present, clean

 

 

 

thoroughly.

 

 

Keep the electrode wet at all times. If it dries out, the impedance will

 

 

 

increase dramatically. To restore performance, soak in 0.1 N HCI

 

 

 

(Cat. No. 1481253) for 30 minutes and rinse well with distilled water.

 

 

Chemical degradation of pH glass can occur rapidly in a high

 

Very high impedance

 

temperature or high pH environment, yielding sluggish response. Low

 

in either glass or

 

temperature environments can double the impedance for every 8 °C

 

reference electrode.

 

drop below 25°C.

Slow response and/or

 

A high impedance electrode is extremely sensitive to electrical noise,

 

 

e.g., oscillating electrical fields generated by motors, generators or

erratic readings.

 

 

discharges from electrical thermostats. A free-hanging cable swinging

 

 

 

due to air currents will also generate erratic signals.

 

 

Manipulate electrode cable and connections to check for intermittent

 

 

 

continuity. Replace as necessary.

 

 

 

 

 

 

Check to see if the ground wire is connected properly at the pre-amp

 

Ground loop problem.

 

junction box.

 

Check for continuity between the stainless steel lug on the electrode

 

 

 

 

 

and the ground wire at the interface.

 

 

 

 

 

Temperature is

See “Temperature” symptom in this table.

 

incorrect.

 

 

 

 

 

 

 

Cracked glass bulb.

If the electrode gives readings between 5.8 and 6.2 pH in all solutions,

 

inspect the glass bulb. If damaged, discard.

 

 

 

 

 

 

 

If a constant reading of 7.0 pH or 0.0 mV is obtained, inspect the cable. If

No response to pH

Short Circuit.

no visible damage exists, remove the connector and test for a short circuit.

change.

 

Replace if faulty.

 

 

 

 

High impedance

Inspect the connector for moisture or corrosion. If wet, rinse well with

 

distilled water and dry thoroughly. Determine the cause of wetness and

 

bridge.

 

correct it.

 

 

 

 

 

 

 

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Troubleshooting and Error Messages

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Hach 900 MAX manual Appendix C PH Troubleshooting, Symptom Possible Cause Solution

900 MAX specifications

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