Teledyne 3000PA operating instructions Series Analyzers

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Percent Oxygen Analyzer

Appendix

 

 

 

 

 

 

 

 

 

A-53000 SERIES ANALYZERS

APPLICATION NOTES ON RESTRICTORS,

PRESSURES, AND FLOW RECOMMENDATIONS

3000 series analyzers require reasonably regulated sample pressures. While the 3000 analyzers are not sensitive to variations of incoming pressure (provided they are properly vented to atmospheric pressure) The pressure must be maintained as to provide a useable flow rate trough the analyzer. Any line attached to sample vent should be 1/4 or larger in diameter.

FLOW RATE RECOMMENDATIONS:

A usable flow rate for a 3000 series analyzer is one which can be measured on the flowmeter. This is basically .2 - 2.4 SLPM . The optimum flow rate is 1 SLPM (mid scale). Note: response time is dependent on flow rate, a low flow rate will result in slow response to O2 changes in the sample stream. The span flow rate should be the approximately same as the sample flow rate.

CELL PRESSURE CONCERNS:

The sensors used in 3000 series analyzers are optimized to function at atmospheric pressure. At pressures other than atmospheric the diffusion rate of O2 will be different than optimum value. Higher pressures will produce faster O2 diffusion rates resulting in higher O2 reading and shorter cell life. To use a 3000 series analyzer at a cell pressure other than atmospheric, the analyzer must be calibrated with a known calibration gas at the new cell pressure to adjust for the different diffusion rate. Cell pressures below 2/3 atmospheric are not recommended because as they tend to cause excessive internal expansion which may result in seal failure.

For operation at cell pressures other than atmospheric care must be taken not to change the sample pressure rapidly or cell damage may occur. For cell pressures above atmospheric, caution must be exercised to avoid over pressuring the cell holder. ( percent analyzers will require some type of cell retainer to prevent the cell from being pushed out by the pressure .) For operation at pressures below atmospheric pressure a suffix C ( clamped) cell is required.

RESTRICTION DEVICES:

For proper operation, all 3000 series analyzers require a flow restriction device. This device is typically a restrictor or a valve. This restriction device serves two functions in the sample path. The first function is to limit the flow rate of the sample through the analyzer. A restrictor is chosen to operate over a range of pressures and provide a useable flow rate over that range.

The second function that the restriction device provides is a pressure drop. This device is selected to provide the only significant pressure drop in the sample path.

Teledyne Analytical Instruments

A-5

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Contents Model 3000PA Teledyne Analytical Instruments Model 3000PAInstrument Serial Number Includes the following options IiiPercent Oxygen Analyzer Specific Model Information Installation Model 3000PA Table of Contents IntroductionOperationalTheory OperationAppendix MaintenancePercent Oxygen Analyzer Combustible GAS Usage Warning Overview Main Features of the AnalyzerTypical Applications Percent Oxygen Analyzer IntroductionIntroduction Model 3000PA Model DesignationsModel 3000PA Front Panel Front Panel Operator InterfaceIntroduction Model 3000PA Analog Outputs Recognizing Difference Between LCDRear Panel Equipment Interface Remote Probe RS-232 PortNetwork OptionalMicro-Fuel Cell Sensor Operational Theory IntroductionPercent Oxygen Analyzer Operational Theory Principles of OperationAnatomy of a Micro-Fuel Cell Operational Theory Model 3000PA+ 2H O + 4e → 4OH Electrochemical ReactionsEffect of Pressure Calibration CharacteristicsClass A-5 Cell Micro-Fuel Cell ClassClass A-3 Cell Sample System Hydrogen and/or Helium ServiceClass B-1 Cell Class B-3 CellPiping Layout and Flow Diagram for Standard Model Span Zero Sample Electronics and Signal ProcessingBlock Diagram of the Model 3000P Electronics Operational Theory Model 3000PA Mounting the Analyzer Percent Oxygen Analyzer InstallationUnpacking the Analyzer Rear Panel Connections Installation Model 3000PARear Panel of the Model 3000PA Gas ConnectionsElectrical Connections Percent Oxygen Analyzer Installation Teledyne Analytical Instruments Percent Oxygen Analyzer Installation Command Description Remote Probe Connector Parameter SettingTesting the System Installing the Micro-Fuel CellAuto Ranging on Percent Oxygen Analyzer OperationOperation Model 3000PA Using the Data Entry and Function ButtonsHierarchy of Functions and Subfunctions System FunctionSetting the Display Password Protection Percent Oxygen Analyzer Operation Setting up an Auto-CalEntering the Password Installing or Changing the Password Logout Version Screen Cell Failure Span FunctionsSpan Cal Auto Mode SpanningManual Mode Spanning Alarms FunctionInstallation AL-1 AL-2 Choose Alarm Range Function Setting the Analog Output RangesFixed Range Analysis Operation Model 3000PA Autoranging AnalysisAnalyze Function Signal OutputVoltage Signal Current Signal Output V dc Output mA dc Range Voltage Current mA Cell Replacement Routine MaintenancePercent Oxygen Analyzer Maintenance Storing and Handling Replacement CellsWhen to Replace a Cell Maintenance Model 3000PRemoving the Micro-Fuel Cell IndexRemoving or Installing a Micro-Fuel Cell Cell Warranty System Self Diagnostic Test Fuse ReplacementMajor Internal Components PowerAnalog PreampRear-Panel Screws CleaningPossible Cause TroubleshootingSolution Maintenance Model 3000P Teledyne Analytical Instruments Percent Oxygen Analyzer Appendix Model 3000PA SpecificationsAppendix Model 3000PA Qty Part Number Description Recommended 2-Year Spare Parts List19-inch Relay Rack Panel Mount Drawing ListSeries Analyzers Calibration GAS Conversions Zero Cal ZeroSettlingMan ENT To Begin