Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F

7.6.12.1 NO Working Standard Traced to NIST NO Standard

First, use the NIST-traceable NO standard and the GPT calibration procedure to calibrate the NO, NOx, and NO2 responses of the analyzer. Also determine the efficiency of the Molycon. Refer to the calibration procedure described in Section 7.6.4.2.

Then, generate several NO concentrations by diluting the NO working standard. Use the nominal NO cylinder concentration, [NO]NOM, to calculate the diluted concentrations. Plot the analyzer NO response (in ppm) versus the nominal diluted NO concentration and determine the slope, SNOM. Calculate the NO concentration of the working standard [NO]STD from:

[NO]STD = [NO]NOM x SNOM

A procedure is presented in the TAD in Reference 2.

7.6.12.2Other Methods of Establishing Traceability

They are:

1.NO working standard traced to NIST NO2 standard

2.NO2 working standard traced to NIST NO2 standard

3.NO2 working standard traced to NIST NO2 standard

NOTE

For further information on calibration by GPT and NO2 permeation devices, refer to part 50 of Chapter 1, Title 40 CFR, Appendix F (revised December 1, 1976) and Reference 13 of that Appendix.

7.7 Calibration of Independent Ranges or Autoranging

There are additional considerations when AutoRange or Independent Ranges are selected. The M200AU uses one physical range of 0-2000 ppb to cover all EPA concentration ranges. The dynamic range of the internal hardware and computer software is sufficient to cover this entire range. Internally the range only scales parts of the 0-2000 ppb physical range to cover the voltage range selected for the analog outputs.

7.7.1 Zero Calibration with AutoRange or Independent Range

Having one physical range to cover all EPA concentration ranges simplifies zero calibration. No matter what AutoRange or Independent Range values are selected the values computed from a zero calibration are the same. Therefore no special precautions need to be taken when doing a zero calibration.

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Teledyne 200AU Calibration of Independent Ranges or Autoranging, Zero Calibration with AutoRange or Independent Range
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200AU specifications

The Teledyne 200AU is a cutting-edge analytical instrument designed primarily for trace and ultra-trace analysis of elements in various liquid samples. Renowned for its reliability and precision, this inductively coupled plasma mass spectrometer (ICP-MS) is widely utilized in environmental monitoring, food safety, clinical diagnostics, and geochemical research.

One of the distinguishing features of the Teledyne 200AU is its exceptional sensitivity, allowing for the detection of elements at concentrations as low as parts per trillion (ppt). This sensitivity is crucial for applications where even minute traces of contaminants can have significant implications. The instrument also boasts a wide dynamic range, accommodating high-concentration samples without compromising accuracy.

The Teledyne 200AU incorporates advanced technologies that enhance its analytical capabilities. At the core of its design is a robust ICP source, which ensures optimal ionization efficiency. The instrument also features a high-resolution quadrupole mass analyzer, which enables precise separation and identification of ions based on their mass-to-charge ratio. This feature is essential for distinguishing between isotopes and analyzing complex mixtures.

Another notable characteristic of the Teledyne 200AU is its user-friendly interface, which simplifies the operation and data management processes. The software is intuitive, offering sophisticated data processing algorithms that streamline analysis. Users can easily access real-time data visualization, facilitating timely decision-making based on analytical results.

The instrument is built with durability in mind, featuring a compact design that allows for easy integration into various laboratory environments. The Teledyne 200AU is also equipped with state-of-the-art safety features, including enhanced cooling systems and automated shutdown protocols to protect both the instrument and the user.

Moreover, the Teledyne 200AU supports a variety of sample introduction methods, including nebulization and laser ablation, providing flexibility to accommodate different types of samples and experimental needs. Its multi-element capability further enhances its versatility, allowing simultaneous detection of multiple elements in a single analysis.

In summary, the Teledyne 200AU stands out as a premier instrument in the field of mass spectrometry. Its combination of high sensitivity, advanced technology, user-friendly features, and robust design makes it an invaluable tool for scientists and researchers seeking precise elemental analysis across various disciplines.
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