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Teledyne 200AU 7.7 Calibration of Independent Ranges or Autoranging

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Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F

7-32

7.6.12.1 NO Working Standard Traced to NIST NO Standard

First, use the NIST-traceable NO standard and the GPT calibration procedure to calibrate the

NO, NOx, and NO2 responses of the analyzer. Also determine the efficiency of the Molycon.

Refer to the calibration procedure described in Section 7.6.4.2.

Then, generate several NO concentrations by diluting the NO working standard. Use the nominal

NO cylinder concentration, [NO]NOM, to calculate the diluted concentrations. Plot the analyzer

NO response (in ppm) versus the nominal diluted NO concentration and determine the slope,

SNOM. Calculate the NO concentration of the working standard [NO]STD from:

[NO]STD = [NO]NOM x SNOM

A procedure is presented in the TAD in Reference 2.

7.6.12.2 Other Methods of Establishing Traceability

They are:

1. NO working standard traced to NIST NO2 standard

2. NO2 working standard traced to NIST NO2 standard

3. NO2 working standard traced to NIST NO2 standard

NOTE

For further information on calibration by GPT and NO2 permeation

devices, refer to part 50 of Chapter 1, Title 40 CFR, Appendix F

(revised December 1, 1976) and Reference 13 of that Appendix.

7.7 Calibration of Independent Ranges or Autoranging

There are additional considerations when AutoRange or Independent Ranges are selected. The

M200AU uses one physical range of 0-2000 ppb to cover all EPA concentration ranges. The

dynamic range of the internal hardware and computer software is sufficient to cover this entire

range. Internally the range only scales parts of the 0-2000 ppb physical range to cover the

voltage range selected for the analog outputs.

7.7.1 Zero Calibration with AutoRange or Independent Range

Having one physical range to cover all EPA concentration ranges simplifies zero calibration. No

matter what AutoRange or Independent Range values are selected the values computed from a

zero calibration are the same. Therefore no special precautions need to be taken when doing a

zero calibration.

Contents

Main INSTRUCTION MANUAL MODEL 200AU NITROGEN OXIDES ANALYZER SAFETY MESSAGES TABLE OF CONTENTS 3 SPECIFICATIONS, AGENCY APPROVALS, WARRANTY ........................3-1 4 THE M200AU NOX ANALYZER................................................................... 4-1 6 OPTIONAL HARDWARE AND SOFTWARE............................................... 6-1 7 CALIBRATION & ZERO/SPAN CHECKS ................................................... 7-1 9 TROUBLESHOOTING, ADJUSTMENTS .................................................... 9-1 Page LIST OF FIGURES Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F viii LIST OF TABLES Page Page 1 HOW TO USE THIS MANUAL Page 2 GETTING STARTED 2.1 Unpacking 2.2 Electrical and Pneumatic Connections Page Page Page Page 2.3 Initial Operation Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 2-7 Step 1 - Enter the expected NOx and NO span gas concentrations: Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 2-9 Step 3 - Review the quality of the calibration: Calibration Quality Check Procedure Step 4 - The M200AU is now ready to measure sample gas. Page Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 2-12 Table 2-1: Final Test and Calibration Values (table continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 2-13 Table 2-1: Final Test and Calibration Values (Continued) PROM # Serial # Date Technician Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 3-1 3 SPECIFICATIONS, AGENCY APPROVALS, WARRANTY 3.1 Specifications 3.2 EPA Equivalency Designation 3.3 Warranty Page 4 THE M200AU NOX ANALYZER 4.1 Principle of Operation Page 4.2 Operation Summary 4.2.1 Sensor Module, Reaction Cell, Detector 4.2.2 Pneumatic Sensor Board 4.2.3 Computer Hardware and Software 4.2.4 V/F Board 4.2.5 Front Panel Page 4.2.6 Power Supply Module 4.2.7 Pump, Valves, Pneumatic System 4.2.8 Ozone Generator 4.2.9 Molybdenum Converter Ozone Scrubber 5 SOFTWARE FEATURES 5.1 Index To Front Panel Menus Page Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-4 5.1.1 Sample Menu Table 5-1: Sample Menu Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-5 Table 5-2: Sample Menu Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-6 5.1.2 Set-Up Menu (table continued) Table 5-3: Setup Menu Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-7 Table 5-3: Setup Menu (Continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-8 Table 5-4: Setup Menu Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-9 Table 5-5: Setup Menu 5.2 Sample Mode 5.2.1 Test Functions Page Page 5.2.2 CAL, CALS, CALZ, Calibration Functions Page Page 5.3 Set-Up Mode 5.3.1 Configuration Information (CFG) 5.3.2 Automatic Calibration (AutoCal) 5.3.3 Data Acquisition System (DAS) Page Page 5.3.4 Range Menu Page 5.3.5 Password Enable 5.3.6 Time of Day Clock 5.3.7 Diagnostic Mode 5.3.8 Communications Menu 5.3.9 Variables Menu (VARS) 5.3.10 M200AU Operating Modes 5.4 Status Output 5.5 RS-232 Interface 5.5.1 Setting Up the RS-232 Interface Page Page 5.5.2 Command Summary Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-29 Table 5-13: RS-232 Command Summary Page Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-32 5.5.3 TEST Commands and Messages Table 5-16: RS-232 Test Messages 5.5.4 WARNING Commands and Messages 5.5.5 CALIBRATION Commands and Messages Page 5.5.6 DIAGNOSTIC Commands and Messages 5.5.7 DAS Commands and Message Page 5.5.8 Internal Variables Page 6 OPTIONAL HARDWARE AND SOFTWARE 6.1 Rack Mount Options 6.2 Zero/Span Valves 6.3 Autocal - Setup Zero/Span Valves Page 6.4 4-20 mA, Current Loop Output 6.5 NOy Converter 7 CALIBRATION & ZERO/SPAN CHECKS Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 7-2 Table 7-1: Types of Zero/Span Check and Calibration Page 7.1 Manual Zero/Span Check or Cal with Zero/Span Gas in the Sample Port Page 7.2 Manual Zero/Span Check or Calibration with Zero/Span Valves Option 7.3 Automatic Zero/Span Check 7.4 Dynamic Zero/Span Calibration 7.5 Use of Zero/Span Valves with Remote Contact Closure 7.6 EPA Protocol Calibration 7.6.1 Calibration of Equipment Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 7-11 Table 7-10: Activity Matrix for Calibration Procedure 7.6.2 Calibration Gas and Zero Air Sources 7.6.3 Data Recording Device 7.6.4 Gas Phase Titration (GPT) System Page [] Page 7.6.5 Dynamic Multipoint Calibration Procedure Page Page Page Page Page Page 7.6.6 Moly Converter Efficiency Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 7-24 Table 7-14: Automatic Calculation of Converter Efficiency 7.6.7 Calibration Frequency 7.6.8 Other Quality Assurance Procedures Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 7-26 Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 7-28 Table 7-16: Activity Matrix for Data Quality 7.6.10 ZERO and SPAN Checks 7.6.11 Recommended Standards for Establishing Traceability 7.6.12 Certification Procedures of Working Standards 7.7 Calibration of Independent Ranges or Autoranging 7.7.1 Zero Calibration with AutoRange or Independent Range 7.7.2 Span Calibration with AutoRange or Independent Range 7.8 Calibration Quality Page 7.9 References Page 8 MAINTENANCE 8.1 Maintenance Schedule Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 8-2 Table 8-2: Preventative Maintenance Calendar 8.2 Replacing the Sample Particulate Filter Page 8.3 Sample Pump Maintenance Page 8.4 Cleaning the Reaction Cell Page 8.5 Replacing the Molybdenum Converter Page 8.6 Pneumatic Line Inspection Page Page Page 8.7 Leak Check Procedure 8.8 Light Leak Check Procedure 8.9 Prom Replacement Procedure Page Page 9 TROUBLESHOOTING, ADJUSTMENTS Page Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-4 Table 9-1: Test Functions (table continued) Test Function Factory Set-Up Comment Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-5 Table 9-1: Test Functions (Continued) (table continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-6 Table 9-1: Test Functions (Continued) (table continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-7 Table 9-1: Test Functions (Continued) 9.1.2 Fault Diagnosis with WARNING Messages Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-9 Table 9-2: Front Panel Warning Messages (table continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-10 Table 9-2: Front Panel Warning Messages (Continued) 9.1.3 Fault Diagnosis using DIAGNOSTIC Mode Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-12 Table 9-3: Summary of Diagnostic Modes Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-13 9.1.3.1 Signal I/O Diagnostic Table 9-4: Diagnostic Mode - Signal I/O (table continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-14 Table 9-4: Diagnostic Mode - Signal I/O (Continued) (table continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-15 Table 9-4: Diagnostic Mode - Signal I/O (Continued) (table continued) Page Page Page 9.1.4 M200AU Internal Variables Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-20 Table 9-5: Model 200AU Variables Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9.1.5 Test Channel Analog Output (table continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-22 Table 9-6: Test Channel Readings (Continued) 9.1.6 Factory Calibration Procedure Page Page 9.2 Performance Problems 9.2.1 AC Power Check 9.2.2 Flow Check 9.2.3 No Response to Sample Gas 9.2.4 Negative Output 9.2.5 Excessive Noise 9.2.6 Unstable Span 9.2.7 Unstable Zero 9.2.8 Inability to Span 9.2.9 Inability to Zero 9.2.10 Non-Linear Response 9.2.11 Slow Response 9.2.12 Analog Output Doesn't Agree with Display Concentration 9.3.1 Computer, Display, Keyboard 9.3 Subsystem Troubleshooting and Adjustments Page Page Page 9.3.2 RS-232 Communications Page Page 9.3.3 Voltage/Frequency (V/F) Board Page Page Page Page Page 9.3.4 Status/Temp Board Page 9.3.5 Power Supply Module Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-48 Table 9-9: Power Supply Module Subassemblies Page Page Page 9.3.6 Ozone Generator Page Page 9.3.7 Flow/Pressure Sensor Page Page Page Page 9.3.8 NOx Sensor Module Page Page Page 9.3.9 Z/S Valves 9.3.10 Pneumatic System Page 10 M200AU SPARE PARTS LIST Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 10-2 Table 10-1: Teledyne API M200AU Spare Parts List (Continued) Page Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F APPENDIX A ELECTRICAL SCHEMATICS Table A-1: Electrical Schematics (table continued) A-1