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Teledyne 200AU 7.6.5 Dynamic Multipoint Calibration Procedure

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Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F

7-16

5. Verify that the residence time (tR) in the reaction chamber is <2 min using Equation 7-5:

min58.0

min/

cm

5.29min/

cm

282

cm

180

= t 33

3

R=

+

6. Verify the dynamic parameter specification (PR) of the calibrator reaction chamber using

Equation 7-6:

ppm75.2

min/

cm

4.29min/

cm

282

cm

180

min/

cm

4.29min/

cm

282

min/

cm

4.29

ppm5.50= P 33

3

33

3

R=

+

×

+

×

7. Calculate the diluent air flow (FD) required at the mixing chamber, using Equation 7-7:

FD = 3300 cm3/min - 282 cm3/min –29.4 cm3/min = 2988.6 cm3/min

7.6.5 Dynamic Multipoint Calibration Procedure

The procedure for calibration of chemiluminescent NOx analyzers by GPT is specified in the

Federal Register.1 This section applies the general procedure to the specific case of the

M200AU.

Calibration must be performed with a calibrator that meets all conditions specified in Subsection

2.3.2 (Q.A. Handbook). Flow settings used in the GPT calibration for NO2 must be determined

as illustrated in Section 7.6.4, this manual.

The user should be sure that all flow meters are calibrated under the conditions of use against a

reliable standard. All volumetric flow rates should be corrected to 25oC (78oF) and 760 mm

(29.92 in.) Hg. Calibrations of flow meters are discussed in TAD.2

Gas Phase Titration (GPT) requires the use of the NO channel of the analyzer to determine the

amount of NO2 generated by titration. Therefore it is necessary to calibrate and determine the

linearity of the NO channel before proceeding with the NO2 calibration. It is also necessary to

calibrate the NOx channel. This can be done simultaneously with the NO calibration. During the

calibration the M200AU should be operating in its normal sampling mode, and the test

atmosphere should pass through all filters, scrubbers, conditioners, and other components used

during normal ambient sampling and as much of the ambient air inlet system as is practicable.

All operational adjustments to the M200AU should be completed prior to the calibration. The

following software features must be set into the desired state before calibration.

Contents

Main INSTRUCTION MANUAL MODEL 200AU NITROGEN OXIDES ANALYZER SAFETY MESSAGES TABLE OF CONTENTS 3 SPECIFICATIONS, AGENCY APPROVALS, WARRANTY ........................3-1 4 THE M200AU NOX ANALYZER................................................................... 4-1 6 OPTIONAL HARDWARE AND SOFTWARE............................................... 6-1 7 CALIBRATION & ZERO/SPAN CHECKS ................................................... 7-1 9 TROUBLESHOOTING, ADJUSTMENTS .................................................... 9-1 Page LIST OF FIGURES Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F viii LIST OF TABLES Page Page 1 HOW TO USE THIS MANUAL Page 2 GETTING STARTED 2.1 Unpacking 2.2 Electrical and Pneumatic Connections Page Page Page Page 2.3 Initial Operation Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 2-7 Step 1 - Enter the expected NOx and NO span gas concentrations: Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 2-9 Step 3 - Review the quality of the calibration: Calibration Quality Check Procedure Step 4 - The M200AU is now ready to measure sample gas. Page Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 2-12 Table 2-1: Final Test and Calibration Values (table continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 2-13 Table 2-1: Final Test and Calibration Values (Continued) PROM # Serial # Date Technician Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 3-1 3 SPECIFICATIONS, AGENCY APPROVALS, WARRANTY 3.1 Specifications 3.2 EPA Equivalency Designation 3.3 Warranty Page 4 THE M200AU NOX ANALYZER 4.1 Principle of Operation Page 4.2 Operation Summary 4.2.1 Sensor Module, Reaction Cell, Detector 4.2.2 Pneumatic Sensor Board 4.2.3 Computer Hardware and Software 4.2.4 V/F Board 4.2.5 Front Panel Page 4.2.6 Power Supply Module 4.2.7 Pump, Valves, Pneumatic System 4.2.8 Ozone Generator 4.2.9 Molybdenum Converter Ozone Scrubber 5 SOFTWARE FEATURES 5.1 Index To Front Panel Menus Page Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-4 5.1.1 Sample Menu Table 5-1: Sample Menu Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-5 Table 5-2: Sample Menu Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-6 5.1.2 Set-Up Menu (table continued) Table 5-3: Setup Menu Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-7 Table 5-3: Setup Menu (Continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-8 Table 5-4: Setup Menu Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-9 Table 5-5: Setup Menu 5.2 Sample Mode 5.2.1 Test Functions Page Page 5.2.2 CAL, CALS, CALZ, Calibration Functions Page Page 5.3 Set-Up Mode 5.3.1 Configuration Information (CFG) 5.3.2 Automatic Calibration (AutoCal) 5.3.3 Data Acquisition System (DAS) Page Page 5.3.4 Range Menu Page 5.3.5 Password Enable 5.3.6 Time of Day Clock 5.3.7 Diagnostic Mode 5.3.8 Communications Menu 5.3.9 Variables Menu (VARS) 5.3.10 M200AU Operating Modes 5.4 Status Output 5.5 RS-232 Interface 5.5.1 Setting Up the RS-232 Interface Page Page 5.5.2 Command Summary Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-29 Table 5-13: RS-232 Command Summary Page Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 5-32 5.5.3 TEST Commands and Messages Table 5-16: RS-232 Test Messages 5.5.4 WARNING Commands and Messages 5.5.5 CALIBRATION Commands and Messages Page 5.5.6 DIAGNOSTIC Commands and Messages 5.5.7 DAS Commands and Message Page 5.5.8 Internal Variables Page 6 OPTIONAL HARDWARE AND SOFTWARE 6.1 Rack Mount Options 6.2 Zero/Span Valves 6.3 Autocal - Setup Zero/Span Valves Page 6.4 4-20 mA, Current Loop Output 6.5 NOy Converter 7 CALIBRATION & ZERO/SPAN CHECKS Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 7-2 Table 7-1: Types of Zero/Span Check and Calibration Page 7.1 Manual Zero/Span Check or Cal with Zero/Span Gas in the Sample Port Page 7.2 Manual Zero/Span Check or Calibration with Zero/Span Valves Option 7.3 Automatic Zero/Span Check 7.4 Dynamic Zero/Span Calibration 7.5 Use of Zero/Span Valves with Remote Contact Closure 7.6 EPA Protocol Calibration 7.6.1 Calibration of Equipment Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 7-11 Table 7-10: Activity Matrix for Calibration Procedure 7.6.2 Calibration Gas and Zero Air Sources 7.6.3 Data Recording Device 7.6.4 Gas Phase Titration (GPT) System Page [] Page 7.6.5 Dynamic Multipoint Calibration Procedure Page Page Page Page Page Page 7.6.6 Moly Converter Efficiency Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 7-24 Table 7-14: Automatic Calculation of Converter Efficiency 7.6.7 Calibration Frequency 7.6.8 Other Quality Assurance Procedures Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 7-26 Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 7-28 Table 7-16: Activity Matrix for Data Quality 7.6.10 ZERO and SPAN Checks 7.6.11 Recommended Standards for Establishing Traceability 7.6.12 Certification Procedures of Working Standards 7.7 Calibration of Independent Ranges or Autoranging 7.7.1 Zero Calibration with AutoRange or Independent Range 7.7.2 Span Calibration with AutoRange or Independent Range 7.8 Calibration Quality Page 7.9 References Page 8 MAINTENANCE 8.1 Maintenance Schedule Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 8-2 Table 8-2: Preventative Maintenance Calendar 8.2 Replacing the Sample Particulate Filter Page 8.3 Sample Pump Maintenance Page 8.4 Cleaning the Reaction Cell Page 8.5 Replacing the Molybdenum Converter Page 8.6 Pneumatic Line Inspection Page Page Page 8.7 Leak Check Procedure 8.8 Light Leak Check Procedure 8.9 Prom Replacement Procedure Page Page 9 TROUBLESHOOTING, ADJUSTMENTS Page Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-4 Table 9-1: Test Functions (table continued) Test Function Factory Set-Up Comment Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-5 Table 9-1: Test Functions (Continued) (table continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-6 Table 9-1: Test Functions (Continued) (table continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-7 Table 9-1: Test Functions (Continued) 9.1.2 Fault Diagnosis with WARNING Messages Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-9 Table 9-2: Front Panel Warning Messages (table continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-10 Table 9-2: Front Panel Warning Messages (Continued) 9.1.3 Fault Diagnosis using DIAGNOSTIC Mode Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-12 Table 9-3: Summary of Diagnostic Modes Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-13 9.1.3.1 Signal I/O Diagnostic Table 9-4: Diagnostic Mode - Signal I/O (table continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-14 Table 9-4: Diagnostic Mode - Signal I/O (Continued) (table continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-15 Table 9-4: Diagnostic Mode - Signal I/O (Continued) (table continued) Page Page Page 9.1.4 M200AU Internal Variables Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-20 Table 9-5: Model 200AU Variables Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9.1.5 Test Channel Analog Output (table continued) Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-22 Table 9-6: Test Channel Readings (Continued) 9.1.6 Factory Calibration Procedure Page Page 9.2 Performance Problems 9.2.1 AC Power Check 9.2.2 Flow Check 9.2.3 No Response to Sample Gas 9.2.4 Negative Output 9.2.5 Excessive Noise 9.2.6 Unstable Span 9.2.7 Unstable Zero 9.2.8 Inability to Span 9.2.9 Inability to Zero 9.2.10 Non-Linear Response 9.2.11 Slow Response 9.2.12 Analog Output Doesn't Agree with Display Concentration 9.3.1 Computer, Display, Keyboard 9.3 Subsystem Troubleshooting and Adjustments Page Page Page 9.3.2 RS-232 Communications Page Page 9.3.3 Voltage/Frequency (V/F) Board Page Page Page Page Page 9.3.4 Status/Temp Board Page 9.3.5 Power Supply Module Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 9-48 Table 9-9: Power Supply Module Subassemblies Page Page Page 9.3.6 Ozone Generator Page Page 9.3.7 Flow/Pressure Sensor Page Page Page Page 9.3.8 NOx Sensor Module Page Page Page 9.3.9 Z/S Valves 9.3.10 Pneumatic System Page 10 M200AU SPARE PARTS LIST Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F 10-2 Table 10-1: Teledyne API M200AU Spare Parts List (Continued) Page Page Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F APPENDIX A ELECTRICAL SCHEMATICS Table A-1: Electrical Schematics (table continued) A-1