Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F

Table 9-1: Test Functions (Continued)

Test Function

Factory Set-Up

Comment

OZONE FL

80 cc/min ± 10

This is the Ozone flow. It is measured by a solid state flow meter,

 

 

and thus is a true indication of flow.

 

 

If you suspect there is no ozone being generated, disconnect the

 

 

tube at the reaction cell and rub the end of the tube on your

 

 

fingertips, then sniff your fingers. The odor of ozone should be

 

 

readily apparent.

 

 

 

PMT

0-5000 mV

This is the instantaneous output of the PMT. During normal

 

 

operation the value varies widely as the M200AU switches from

 

 

NO to NOx to Pre-reactor modes. Changes in reading will be

 

 

synchronized with valve switching. The PMT voltage values will

 

 

be relatively constant when:

 

 

1.

Electric test - variation in the 2000 mV signal observed will be

 

 

 

sampling errors of the V/F board and preamp noise. See Section

 

 

 

9.1.3.2.

 

 

2.

Optic test - variation in the 2000 mV signal will be PMT dark

 

 

 

current, preamp, HVPS plus item 1 above. See Section 9.1.3.3.

 

 

3.

Sampling zero gas - signal from 1, 2 plus signal from ozone

 

 

 

generator air

 

 

4.

Sampling pure NO span gas - signal will be 1, 2, 3, above plus

 

 

 

signal from chemiluminescent reaction. Slight pulsations will

 

 

 

be noticed as the M200AU switches from NO to NOx. This is

 

 

 

due to differences in flowrates in each channel. These

 

 

 

differences are taken out in the calibration process resulting in

 

 

 

slightly different slopes for the NO and NOx channels. Large

 

 

 

pulsations when switching to the NOx channel is indicative of a

 

 

 

bad moly converter.

 

 

When sampling zero gas the PMT reading should be less than 150

 

 

mV and relatively constant.

 

 

High or noisy readings could be due to:

 

 

1.

Excessive background light which is caused by a possible

 

 

 

contaminated reaction cell.

 

 

2.

Humidity (undried ambient air) in the ozone generator feed air.

 

 

3.

PMT recently exposed to room light. It takes 24-48 hours for

 

 

 

the PMT to adapt to dim light.

 

 

4.

Light leak in reaction cell.

 

 

5.

Improper slopes

 

 

 

NORM PMT

0-5000 mV

The Normalized PMT reading is to be used as the PMT reading

 

 

during the FACTORY CALIBRATION procedure. In addition to

 

 

the raw mV reading from the PMT this reading is adjusted using

 

 

certain other factors to produce an accurate reading for the Factory

 

 

Calibration procedure.

 

 

 

 

(table continued)

 

 

 

9-5

Page 141
Image 141
Teledyne 200AU instruction manual Ozone FL

200AU specifications

The Teledyne 200AU is a cutting-edge analytical instrument designed primarily for trace and ultra-trace analysis of elements in various liquid samples. Renowned for its reliability and precision, this inductively coupled plasma mass spectrometer (ICP-MS) is widely utilized in environmental monitoring, food safety, clinical diagnostics, and geochemical research.

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