Teledyne API Model 200AU NOX Analyzer Instruction Manual, 02293, Rev. F

Table 7-8: Z/S Valves Modes with Remote Contact Closure

Ext Zero CC

Ext Span CC

Operation

Contact Open

Contact Open

State when in SAMPLE mode, normal monitoring.

 

 

 

Contact Open

Contact Closed

Span check or calibrate*

Contact Closed

Contact Open

Zero check or calibrate*

*Calibrate only if Dynamic Calibration is enabled.

7.6EPA Protocol Calibration

If the M200AU is to be used for EPA compliance monitoring, it must be calibrated in accordance with the instructions in this section.

In order to insure that high quality, accurate measurements are obtained at all times, the M200AU must be calibrated prior to use. A quality assurance program centered on this aspect and including attention to the built-in warning features of the M200AU, periodic inspection, regular zero/span checks and routine maintenance is paramount to achieving this.

In order to have a better understanding of the factors involved in assuring continuous and reliable information from the M200AU, it is strongly recommended that Publication No. PB 273- 518 Quality Assurance Handbook for Air Pollution Measurement Systems (abbreviated, Q.A. Handbook) be purchased from the NTIS (phone 703-487-4650). Special attention should be paid to Section 2.3 which deals with chemiluminescent based NO2 analyzers and upon which most of this section is based. Specific regulations regarding the use and operation of ambient oxides of nitrogen analyzers can be found in 40 CFR 50 and 40 CFR 58. Both publications are available from the U.S. Government Printing Office (phone 202-783-3238).

7.6.1 Calibration of Equipment

In general, calibration is the process of adjusting the gain and offset of the M200AU against some recognized standard. The reliability and usefulness of all data derived from any analyzer depends primarily upon its state of calibration. In this section the term dynamic calibration is used to express a multipoint check against known standards and involves introducing gas samples of known concentration into the instrument in order to adjust the instrument to a predetermined sensitivity and to produce a calibration relationship. This relationship is derived from the instrumental response to successive samples of different known concentrations. As a minimum, three reference points and a zero point are recommended to define this relationship. The true values of the calibration gas must be traceable to NIST-SRM's (Section 2.0.7, Q.A. Handbook).

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Teledyne 200AU EPA Protocol Calibration, Calibration of Equipment, Z/S Valves Modes with Remote Contact Closure

200AU specifications

The Teledyne 200AU is a cutting-edge analytical instrument designed primarily for trace and ultra-trace analysis of elements in various liquid samples. Renowned for its reliability and precision, this inductively coupled plasma mass spectrometer (ICP-MS) is widely utilized in environmental monitoring, food safety, clinical diagnostics, and geochemical research.

One of the distinguishing features of the Teledyne 200AU is its exceptional sensitivity, allowing for the detection of elements at concentrations as low as parts per trillion (ppt). This sensitivity is crucial for applications where even minute traces of contaminants can have significant implications. The instrument also boasts a wide dynamic range, accommodating high-concentration samples without compromising accuracy.

The Teledyne 200AU incorporates advanced technologies that enhance its analytical capabilities. At the core of its design is a robust ICP source, which ensures optimal ionization efficiency. The instrument also features a high-resolution quadrupole mass analyzer, which enables precise separation and identification of ions based on their mass-to-charge ratio. This feature is essential for distinguishing between isotopes and analyzing complex mixtures.

Another notable characteristic of the Teledyne 200AU is its user-friendly interface, which simplifies the operation and data management processes. The software is intuitive, offering sophisticated data processing algorithms that streamline analysis. Users can easily access real-time data visualization, facilitating timely decision-making based on analytical results.

The instrument is built with durability in mind, featuring a compact design that allows for easy integration into various laboratory environments. The Teledyne 200AU is also equipped with state-of-the-art safety features, including enhanced cooling systems and automated shutdown protocols to protect both the instrument and the user.

Moreover, the Teledyne 200AU supports a variety of sample introduction methods, including nebulization and laser ablation, providing flexibility to accommodate different types of samples and experimental needs. Its multi-element capability further enhances its versatility, allowing simultaneous detection of multiple elements in a single analysis.

In summary, the Teledyne 200AU stands out as a premier instrument in the field of mass spectrometry. Its combination of high sensitivity, advanced technology, user-friendly features, and robust design makes it an invaluable tool for scientists and researchers seeking precise elemental analysis across various disciplines.