Teledyne 7300A manual Ndir Analyzer

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Infrared Gas Analyzer

Introduction 1

 

 

 

 

 

 

 

 

 

being measured. There is a direct correlation between absorption and the concentration of the component of interest in the liquid mixture.

1.5 NDIR Analyzer

The Model 7300A contains an optical system consisting of an infrared (IR) source, sample cell, and detectors. In front of the thermopile detectors are four interference-type filters. These filters are designated the reference and measuring filters. The sample flows continuously through the sample cell, absorbing energy at various wavelengths throughout the IR spectrum. The wavelengths and intensities of absorption peaks throughout the spectrum are characteristic of the specific compounds that are present in the sample.

In any photometric analysis, there is always the analysis of the compo- nent of interest, and other components (background) which are not of mea- suring interest. Both the “component of interest” and the background compo- nent may have complex IR absorption spectra.

The quantitative measurement of a compound using the 7300A is based on the Beer-Lambert Law, where the intensity of a beam of monochromatic radiation transmitted through a sample decreases exponentially as the con- centration of the absorbing sample increases. The use of two filters and detectors allows cancellation of energy changes due to turbidity, dirty sample cell windows, aging of the source and sudden temperature changes.

The center pass band of the measuring filter is selected to transmit energy in a narrow region (band pass) where the component of interest absorbs strongly by comparison with the background components.The center pass band of the reference filter is generally selected to transmit energy in a band pass region where the background absorption of IR energy is equiva- lent to that seen by the measuring filter, and also to be in a region where the component of interest has minimal absorption of energy. The IR radiation passes through the sample and filters and strikes the detectors, which convert the radiation into electrical signals, and are then amplified. Signal processing involves comparing the measuring and reference signals in order to give a readout representing the “component of interest” concentration in the sample.

Teledyne Analytical Instruments

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Contents Teledyne Analytical Instruments Model 7300ACopyright 2000 Teledyne Analytical Instruments Model 7300AApplication Impurity of Interest Infrared Gas Analyzer Technician Record SheetModel 7300A Teledyne Analytical Instruments Model 7300A Model 7300A Infrared Gas Analyzer Table of Contents IntroductionInstallation Operation Electrical/Control Unit Modes/Functioning Table of ContentsStart-up and Theory of Operation Appendix MaintenanceInfrared Gas Analyzer Introduction OverviewTypical Gas Applications Introduction Model 7300A Main Features of the AnalyzerGeneral Ndir Analyzer Introduction Model 7300A Teledyne Analytical Instruments Unpacking the Analyzer/Inspection Installing and Connecting the AnalyzerInfrared Gas Analyzer Installation Calibration Gases Installation Model 7300AElectrical Power Connections User ConnectionsVenting the System Infrared Gas Analyzer Installation Pipe ConnectionsElectrical Connections Rear Panel Sample Delivery SystemAnalog Outputs Installation Model 7300A Primary Input PowerFuse Installation 3 50-Pin Equipment Interface ConnectorOutput V dc Output mA dc Pin FunctionExamples Range Voltage Current mA Application Alarm RelaysDigital Remote Cal Inputs Pin ContactRemote Calibration Connections Network I/O Remote Valve ConnectorRange ID Relays FET Series Resistance 4 RS-232 PortGas Requirements Command DescriptionParameter Setting Calibration Testing the SystemCalibration Calibration Fluids Infrared Gas Analyzer Installation Installation Model 7300A Teledyne Analytical Instruments Infrared Gas Analyzer Start-up and Operation PreliminaryNdir Analyzer Startup Initial Set-up and ZeroingStart-up and Theory of Operation Model 7300A Operational CalibrationAnalyzer Theory of operation GeneralBlock Diagram of the Model 7300A Electronics Circuit Description Digital Signal Processing & Electronics Linearizer Linearizer Output Linearizer Input Teledyne Analytical Instruments Page Infrared Gas Analyzer Operation IntroductionMode/Function Selection Using the ControlsAnalysis Mode Operation Model 7300ASetup Mode Setup Mode Escape Data EntryEnter Enter Setting up an AUTO-CALEntering the Password Infrared Gas Analyzer Operation Password ProtectionAAA Installing or Changing the PasswordLogging Out System Self-Diagnostic TestChecking Linearity with Algorithm Model ScreenTroubleshooting information Digital Filter Setup Zero Offset Adjustment CAL-OUT Function Adjst output to 4ma ENT to OK Zero Cal Zero and Span FunctionsAuto Mode Zeroing Cell Failure Manual Mode ZeroingSpan Cal Auto Mode SpanningManual Mode Spanning Installation Alarms FunctionPress enter again to set the alarm setpoints Manual Select/Define Range Screen Range Select FunctionAuto Screen Precautions Illustrates these schemes graphically Analyze FunctionSet Application Screen ProgrammingOFFST/INVRT ENT Checking the linearization Curve Algorithm ScreenManual Mode Linearization Auto Mode Linearization Offset OUTPUT/Reversal Output Output Signal Reversal Special Function SetupPolarity Reversal Output Signal OffsetGain Preset Infrared Gas Analyzer Maintenance MaintenanceFilter Routine MaintenanceMaintenance Model 7300A Ndir Analyzer Measurement Cell System Self Diagnostic TestPreamp PowerMajor Internal Components AnalogCell Assembly Troubleshooting General Trouble Shooting Chart Maintenance Model 7300A Infrared Gas Analyzer Maintenance Maintenance Model 7300A Teledyne Analytical Instruments Infrared Gas Analyzer Appendix Appendix Model 7300A SpecificationsDrawing List Qty Description Recommended 2-Year Spare Parts ListAttachment 7300A Infrared Gas Analyzer Appendix