MODEL 102E TOTAL REDUCED SULFUR ANALYZER, With

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Teledyne manual MODEL 102E TOTAL REDUCED SULFUR ANALYZER, MODEL 501 TRS THERMAL CONVERTER, with, P/N 04740 REV. A

Contents

MODEL 501 TRS THERMAL CONVERTER MODEL 102E TOTAL REDUCED SULFUR ANALYZERADDENDUM TO MODEL 101E OPERATORS MANUAL withPage M102E/M501 TRS TABLE OF CONTENTS05514 Rev A1 Addendum to M101E Manual - P/N 04740 Rev A 8. INSTRUMENT MAINTENANCE LIST OF APPENDICES10. TROUBLESHOOTING & REPAIR 9. THEORY OF OPERATION LIST OF TABLES LIST OF FIGURESPREFACE Page corner of the display any time the instrument is in SETUP mode 1. PREFACE 1.1. Reference Numbering convention User Notes 2.1. Specifications 2. SPECIFICATIONS, APPROVALS AND WARRANTY2.1.1. M501-TRS Specifications 2.2. EPA Equivalency Designation 2.3. CE Mark Compliance 3.1. Unpacking the M102E 3. GETTING STARTED3.2. Unpacking the M501-TRS Never disconnect electronic circuit boards, wiring harnesses or that the rack/enclosure itself is adequately ventilated 3.2.1. M501-TRS Ventilation Clearancethe maximum operating temperature specification for the M102E 40C Figure 3-1 M102E Internal Layout 3.3. Internal LayoutsFigure 3-2 M501-TRS Internal Layout Table 3-1 TRS - SO2 Switching Valve Operating Modes 3.4. Internal Pneumatic Flow of the M102E & the M501-TRSM102E INSTRUMENT CHASSIS M501 Alarm Output 3.5. Rear Panel Layout for the M102E & M501-TRSFigure 3-4 M102E Rear Panel Layout 5 Amp 3.6.1. Electrical Connections 3.6. Initial Setup3.6.1.1. M102E Analog Output Connections Figure 3-6 Analog Output Connector 3.6.2. Pneumatic Connections 3.6.1.2. M501-TRS Alarm Output ConnectionsM102E PNEMATIC CONNECTERS M501-TRS PNEMATIC CONNECTERS 102E MODEL SPAN GAS The exhaust from the instrument needs to be vented outside the ZERO AIR 3.6.2.1. Connections with Internal Valve Options Installed VENT Gas Dilution CalibratorVENT if input is pressurized Valve Option Option 3.7.1. Startup / Warm Up of the M102E 3.7. Initial Operation3.7.2. Functional Check of the M102E Possible Warning Messages at Start-Up 3.7.3. Startup / Warm Up of the M501-TRS High Alarm LED Low Alarm LEDProcess Variable Display area 3.8. Initial Calibration Page 4.1. Rack Mount Kits Options 20a, 20b, 21, 22 4. OPTIONAL HARDWARE AND SOFTWARE4.2. Calibration Valves Options OPTIONAL HARDWARE AND SOFTWARE Zero/Span Valve Operating States Table 4-2 IZS Valve Operating States M102E INSTRUMENT CHASSIS 4.3.1. Printed Manuals P/N 4.3. Additional Manuals4.3.2. Addendum on CD Part number 5. M102E OPERATING INSTRUCTIONS 5.1.1. M102E Analog Output SignalsFigure 5-1 Analog Output Connector Key M102E OPERATING INSTRUCTIONS 5.1.2. Setting the M102E Gas Measurement Mode 5.2. SETUP - DIAG Using the Diagnostics Functions5.2.1. M102E Analog I/O Configuration Table 5-1 M102E gas Measurement Modes 5.2.2. M102E Test Channel Output 5.3. SETUP - COMM Setting Up the M102E’s Communication Ports5.3.1. M102E ID Code 5.3.2. M102E Ethernet Host Name 5.4.1. Control Inputs 5.4. Remote Operation of the AnalyzerCONTROL IN ZERO 5 VDC Power Supply 5.4.2. Using the M102E with a Hessen Protocol Network5.4.2.1. M102E Hessen Protocol Gas ID List SPAN Table 5-6 Default Hessen Status Bit Assignments 5.4.2.2. Setting Hessen Protocol Status Flags 6.1. Basic M501-TRS Controls 6. M501-TRS OPERATING INSTRUCTIONSDO NOT OPERATE WITHOUT THE COVER OF THE M501TS CONVERTER INSTALLED Teledyne Instruments customer service Table 6-1 M501-TRS Temperature Controls and Definitions 6.2. To Display The Current Temperature DO NOT SET THE TEMPERATURE HIGHER THAN 1050OC 6.3. To Manually Adjust the Converter Oven Temperature 6.4.1. Initiating the Autotune Process 6.4. Autotune the Temperature Controllerhas reached a stable, constant temperature 6.4.2. Aborting the Autotune Process 6.5. M501TRS Alarm Relay Adjustmentnecessary to repeat the autotune procedure Page USER NOTES 7. CALIBRATION PROCEDURES7.1. M102E Calibration 7.2. M501-TRS CalibrationPage INSTRUMENT MAINTENANCE 8. INSTRUMENT MAINTENANCE 8.1.1.1. Predicting When the SO2 Scrubber Should Be Replaced 8.1. Additional and Updated Maintenance Procedures8.1.1. Maintaining the SO2 Scrubber 8.1.1.3. Changing the SO2 Scrubber Material 8.1.1.2. Checking the Function of the SO2 ScrubberPage 9.1. Measurement Principle 9. THEORY OF OPERATION9.1.1. TRS Conversion 9.1.2. SO2 Ultraviolet Fluorescence SO2 * ⎯⎯→ SO2 + hv330nm SO2 + hv214nm ⎯⎯Ia⎯→ SO2Ia = I0 1 − exp− axSO2 Figure 9-1 UV Absorption in the M102E Reaction Cell kSO2 * ⎯⎯F⎯→ SO2 + hv330nm F = kSO2Equation9-6 9.3. Pneumatic Operation 9.2. The UV Light Path9.2.1. UV Lamp Shutter & PMT Offset 9.3.1. Sample gas Flow 9.4. Electronic Operation PMT HOUSING9.4.1. Sensor Module SAMPLE CHAMBERUV Lamp 9.4.1.2. Sample Chamber Heating Circuit 9.4.1.1. Sample ChamberSample Air Housing Outlet O-Ring O-Ring Seal Seal Sample Air 9.4.2. M501-TRS electronics 9.4.2.1. Thermal SwitchHEATER P-I-D CONTROLLER 9.4.2.2. Temperature Alarms and Alarm Output 10.1.1. Fault Diagnosis with Warning Messages 10. TROUBLESHOOTING & REPAIR10.1.1.2. M501-TRS Error Codes 10.1.1.1. M102E Warning Messages Table 10-2 Test Functions - Possible Causes for Out-Of-Range Values 10.1.2. Fault Diagnosis with Test Functionsfunctioning 10.3. Other Performance Problems 10.2. M501-TRS Trouble shooting10.2.1. TRS Converter Not Heating 10.3.1. Excessive noise 10.4.1. Checking the Efficiency of the M501-TRS SO2 Scrubber 10.4. Subsystem Checkout10.4.2. Checking the Efficiency of the M501-TRS TRS Æ SO2 Converter 10.5.1. UV Lamp Adjustment and/or Replacement 10.5. Additional Repair Procedures ALWAYS wear UV-Protective, Safety Glasses when working with the UV 10.5.1.1. Adjusting the UV Lamp Peaking the LampLamp Assembly Always grasp the main body of the lamp Figure 10-1 Shutter Assembly - Exploded View 10.5.1.2. Replacing the UV Lamp Figure 10-2 Disassembling the Shutter Assembly 10.5.2. Replacing the UV filter/lens Figure 10-3 PMT Assembly - Exploded View 10.5.3. Replacing the PMT, HVPS or TEC 3. Remove the reaction cell assembly 10.5.4. M102E PMT Hardware Calibration FACTORY CAL Figure 10-4 Pre-Amplifier Board Layout 6. Locate the Preamp board see Figure If a reporting range other than 500 ppb is used in this procedure 10.5.5. Replacing the TRS Converter Heating TubeAdjust the PMT until NORM PMT equals 1280 mV ± 10 mV NORM PMT value of twice the ppb value of the span gas EXAMPLE The ceramic bobbins at each end of the heater assembly are fragile 10.6. Manually Programming the M501-TRS Temperature ControllerBe Careful element off 115V/60Hz with a set value of 1000C 10.6.1. Temperature Controller Primary Menu Parameters Table 10-3 - Temperature Controller - Primary Parameter Settings Table 10-4 - Temperature Controller - Primary Parameter Settings 10.7. Technical Assistance User Notes APPENDIX A-2 Model 102E Setup Variables Available Via Serial I/O APPENDIX A - Version Specific Software DocumentationAPPENDIX A-4 Model 102E Signal I/O Definitions M102E/M501 TRS APPENDIX A - Version Specific Software Documentation ENTER SETUP PASS SETUPAPPENDIX A-1 M102E Software Menu Trees, Revision A.2 APPENDIX A-1 M102E Software Menu Trees, Revision A.2 SAMPLE TEST SAMPLEMSG 1,2 CLR 1,3 SO2, 111, REPORTED ACAL1TR2, 112, REPORTED Figure A-4 Secondary Setup Menu DIAG SAMPLE ENTER SETUP PASSDIAG Deleted Setup Variables for M102E Software Revision A.2 APPENDIX A-2 Setup Variables For Serial I/O, Revision A.2Table A-2 MEASUREMODE APPENDIX A-3 Warnings and Test Functions, Revision A.2 setting of STABILFREQ and STABILSAMPLESTable A-4 Warning Messages deleted from M102 Software Revision A.2 Table A-6 Test Functions Deleted from M102 Software Revision A.2 APPENDIX A-4 M102E Signal I/O Definitions, Revision A.2M102E/M501 TRS APPENDIX A-4 M102E Signal I/O Definitions, Revision A.2Rear board primary MUX analog inputs Trigger Event APPENDIX A-5 M102E iDAS Functions, Revision A.2CTEMPW Function APPENDIX A-5 M102E iDAS Functions, Revision A.2 A-10 APPENDIX B - M102E Spare Parts List APPENDIX B - M102E Spare Parts ListTable B-1 M102E Spare Parts List M101E Manual - P/N 04740120 Rev A M102E/M501 TRS M102E/M501 TRS Warranty/Repair Questionnaire Model 102ETELEDYNE INSTRUMENTS M102E/M501 TRS APPENDIX D - ELECTRONIC SCHEMATICS APPENDIX D - ELECTRONIC SCHEMATICSTable D-1 List of Included Electronic Schematics Addendum to M101E Manual - P/N 04740 Rev A User Notes APPENDIX D - ELECTRONIC SCHEMATICSM102E/M501 TRS 05518 Rev A