with
MODEL 102E TOTAL REDUCED SULFUR ANALYZER
MODEL 501 TRS THERMAL CONVERTER
ADDENDUM TO MODEL 101E OPERATORS MANUAL
Page
Addendum to M101E Manual - P/N 04740 Rev A
TABLE OF CONTENTS
M102E/M501 TRS
05514 Rev A1
M102E/M501 TRS
LIST OF APPENDICES
8. INSTRUMENT MAINTENANCE
10. TROUBLESHOOTING & REPAIR
PREFACE
LIST OF FIGURES
LIST OF TABLES
M102E/M501 TRS
Page
PREFACE
1. PREFACE
corner of the display any time the instrument is in SETUP mode
M102E/M501 TRS
PREFACE
User Notes
1.1. Reference Numbering convention
M102E/M501 TRS
2.2. EPA Equivalency Designation
2. SPECIFICATIONS, APPROVALS AND WARRANTY
2.1. Specifications
2.1.1. M501-TRS Specifications
M102E/M501 TRS
2.3. CE Mark Compliance
SPECIFICATIONS, APPROVALS AND WARRANTY
User Notes
Never disconnect electronic circuit boards, wiring harnesses or
3. GETTING STARTED
3.1. Unpacking the M102E
3.2. Unpacking the M501-TRS
GETTING STARTED
3.2.1. M501-TRS Ventilation Clearance
the maximum operating temperature specification for the M102E 40C
M102E/M501 TRS
Figure 3-1 M102E Internal Layout
3.3. Internal Layouts
M102E/M501 TRS
GETTING STARTED
GETTING STARTED
3.4. Internal Pneumatic Flow of the M102E & the M501-TRS
Table 3-1 TRS - SO2 Switching Valve Operating Modes
M102E/M501 TRS
GETTING STARTED
3.5. Rear Panel Layout for the M102E & M501-TRS
Alarm Output
M102E/M501 TRS
Figure 3-6 Analog Output Connector
3.6. Initial Setup
3.6.1. Electrical Connections
3.6.1.1. M102E Analog Output Connections
M501-TRS PNEMATIC CONNECTERS
3.6.1.2. M501-TRS Alarm Output Connections
3.6.2. Pneumatic Connections
M102E PNEMATIC CONNECTERS
102E
MODEL
102E
MODEL
SPAN GAS
M102E/M501 TRS
GETTING STARTED
The exhaust from the instrument needs to be vented outside the
ZERO AIR
3.6.2.1. Connections with Internal Valve Options Installed
M102E/M501 TRS
GETTING STARTED
GETTING STARTED
MODEL
102E
M102E/M501 TRS
102E
MODEL
102E
MODEL
M102E/M501 TRS
3.7. Initial Operation
3.7.1. Startup / Warm Up of the M102E
3.7.2. Functional Check of the M102E
M102E/M501 TRS
High Alarm LED Low Alarm LED
3.7.3. Startup / Warm Up of the M501-TRS
Figure 3-12 M501-TRS Temperature Controller Startup
GETTING STARTED
3.8. Initial Calibration
User Notes
M102E/M501 TRS
Page
M102E/M501 TRS
4. OPTIONAL HARDWARE AND SOFTWARE
4.1. Rack Mount Kits Options 20a, 20b, 21, 22
4.2. Calibration Valves Options
Zero/Span Valve Operating States
M102E/M501 TRS
OPTIONAL HARDWARE AND SOFTWARE
M102E INSTRUMENT CHASSIS
Table 4-2 IZS Valve Operating States
M102E/M501 TRS
OPTIONAL HARDWARE AND SOFTWARE
M102E INSTRUMENT CHASSIS
User Notes
4.3. Additional Manuals
4.3.1. Printed Manuals P/N
4.3.2. Addendum on CD Part number
M102E/M501 TRS
5.1.1. M102E Analog Output Signals
5. M102E OPERATING INSTRUCTIONS
Figure 5-1 Analog Output Connector Key
M102E/M501 TRS
5.2. SETUP - DIAG Using the Diagnostics Functions
5.1.2. Setting the M102E Gas Measurement Mode
5.2.1. M102E Analog I/O Configuration
5.3.2. M102E Ethernet Host Name
5.3. SETUP - COMM Setting Up the M102E’s Communication Ports
5.2.2. M102E Test Channel Output
5.3.1. M102E ID Code
ZERO
5.4. Remote Operation of the Analyzer
5.4.1. Control Inputs
CONTROL IN
SPAN
5.4.2. Using the M102E with a Hessen Protocol Network
5 VDC Power Supply
5.4.2.1. M102E Hessen Protocol Gas ID List
M102E/M501 TRS
5.4.2.2. Setting Hessen Protocol Status Flags
Table 5-6 Default Hessen Status Bit Assignments
User Notes
OVEN TEMPERATURE WILL NOT REGULATE PROPERLY WITHOUT THE
6. M501-TRS OPERATING INSTRUCTIONS
6.1. Basic M501-TRS Controls
DO NOT OPERATE WITHOUT THE COVER OF THE M501TS CONVERTER INSTALLED
M501-TRS OPERATING INSTRUCTIONS
6.2. To Display The Current Temperature
Table 6-1 M501-TRS Temperature Controls and Definitions
M102E/M501 TRS
M501-TRS OPERATING INSTRUCTIONS
6.3. To Manually Adjust the Converter Oven Temperature
DO NOT SET THE TEMPERATURE HIGHER THAN 1050OC
M102E/M501 TRS
M102E/M501 TRS
6.4. Autotune the Temperature Controller
6.4.1. Initiating the Autotune Process
has reached a stable, constant temperature
M102E/M501 TRS
6.5. M501TRS Alarm Relay Adjustment
6.4.2. Aborting the Autotune Process
necessary to repeat the autotune procedure
Page
7.2. M501-TRS Calibration
7. CALIBRATION PROCEDURES
USER NOTES
7.1. M102E Calibration
Page
05514 Rev A1
8. INSTRUMENT MAINTENANCE
INSTRUMENT MAINTENANCE
M102E/M501 TRS
INSTRUMENT MAINTENANCE
8.1. Additional and Updated Maintenance Procedures
8.1.1.1. Predicting When the SO2 Scrubber Should Be Replaced
8.1.1. Maintaining the SO2 Scrubber
User Notes
8.1.1.2. Checking the Function of the SO2 Scrubber
8.1.1.3. Changing the SO2 Scrubber Material
INSTRUMENT MAINTENANCE
Page
9.1.2. SO2 Ultraviolet Fluorescence
9. THEORY OF OPERATION
9.1. Measurement Principle
9.1.1. TRS Conversion
M102E/M501 TRS
SO2 + hv214nm ⎯⎯Ia⎯→ SO2
SO2 * ⎯⎯→ SO2 + hv330nm
Ia = I0 1 − exp− axSO2
THEORY OF OPERATION
F = kSO2
M102E/M501 TRS
kSO2 * ⎯⎯F⎯→ SO2 + hv330nm
9.3.1. Sample gas Flow
9.2. The UV Light Path
9.3. Pneumatic Operation
9.2.1. UV Lamp Shutter & PMT Offset
SAMPLE CHAMBERUV Lamp
PMT HOUSING
9.4. Electronic Operation
9.4.1. Sensor Module
M102E/M501 TRS
9.4.1.1. Sample Chamber
9.4.1.2. Sample Chamber Heating Circuit
Sample Air Housing Outlet O-Ring O-Ring Seal Seal
P-I-D CONTROLLER
9.4.2.1. Thermal Switch
9.4.2. M501-TRS electronics
HEATER
THEORY OF OPERATION
9.4.2.2. Temperature Alarms and Alarm Output
User Notes
M102E/M501 TRS
10.1.1.1. M102E Warning Messages
10. TROUBLESHOOTING & REPAIR
10.1.1. Fault Diagnosis with Warning Messages
10.1.1.2. M501-TRS Error Codes
Table 10-2 Test Functions - Possible Causes for Out-Of-Range Values
10.1.2. Fault Diagnosis with Test Functions
TROUBLESHOOTING & REPAIR
M102E/M501 TRS
10.3.1. Excessive noise
10.2. M501-TRS Trouble shooting
10.3. Other Performance Problems
10.2.1. TRS Converter Not Heating
TROUBLESHOOTING & REPAIR
10.4. Subsystem Checkout
10.4.1. Checking the Efficiency of the M501-TRS SO2 Scrubber
10.4.2. Checking the Efficiency of the M501-TRS TRS Æ SO2 Converter
M102E/M501 TRS
10.5. Additional Repair Procedures
10.5.1. UV Lamp Adjustment and/or Replacement
TROUBLESHOOTING & REPAIR
Lamp Assembly
10.5.1.1. Adjusting the UV Lamp Peaking the Lamp
TROUBLESHOOTING & REPAIR
ALWAYS wear UV-Protective, Safety Glasses when working with the UV
M102E/M501 TRS
10.5.1.2. Replacing the UV Lamp
TROUBLESHOOTING & REPAIR
Figure 10-1 Shutter Assembly - Exploded View
M102E/M501 TRS
10.5.2. Replacing the UV filter/lens
TROUBLESHOOTING & REPAIR
Figure 10-2 Disassembling the Shutter Assembly
M102E/M501 TRS
10.5.3. Replacing the PMT, HVPS or TEC
TROUBLESHOOTING & REPAIR
Figure 10-3 PMT Assembly - Exploded View
05514 Rev A1
TROUBLESHOOTING & REPAIR
3. Remove the reaction cell assembly
M102E/M501 TRS
05514 Rev A1
10.5.4. M102E PMT Hardware Calibration FACTORY CAL
TROUBLESHOOTING & REPAIR
M102E/M501 TRS
Figure 10-4 Pre-Amplifier Board Layout
TROUBLESHOOTING & REPAIR
M102E/M501 TRS
6. Locate the Preamp board see Figure
Adjust the PMT until NORM PMT equals 1280 mV ± 10 mV
10.5.5. Replacing the TRS Converter Heating Tube
TROUBLESHOOTING & REPAIR
If a reporting range other than 500 ppb is used in this procedure
altered, except for temperature set point
10.6. Manually Programming the M501-TRS Temperature Controller
TROUBLESHOOTING & REPAIR
The ceramic bobbins at each end of the heater assembly are fragile
115V/60Hz with a set value of 1000C
10.6.1. Temperature Controller Primary Menu Parameters
TROUBLESHOOTING & REPAIR
M102E/M501 TRS
05514 Rev A1
TROUBLESHOOTING & REPAIR
Table 10-3 - Temperature Controller - Primary Parameter Settings
M102E/M501 TRS
M102E/M501 TRS
10.7. Technical Assistance
TROUBLESHOOTING & REPAIR
Table 10-4 - Temperature Controller - Primary Parameter Settings
05514 Rev A1
TROUBLESHOOTING & REPAIR
User Notes
M102E/M501 TRS
M102E/M501 TRS APPENDIX A - Version Specific Software Documentation
APPENDIX A - Version Specific Software Documentation
APPENDIX A-2 Model 102E Setup Variables Available Via Serial I/O
APPENDIX A-4 Model 102E Signal I/O Definitions
APPENDIX A-1 M102E Software Menu Trees, Revision A.2 SAMPLE
SETUP
ENTER SETUP PASS
APPENDIX A-1 M102E Software Menu Trees, Revision A.2
CLR 1,3
SAMPLE
TEST
MSG 1,2
SO2, 111, REPORTED
ACAL1
TR2, 112, REPORTED
DIAG
SAMPLE ENTER SETUP PASS
Figure A-4 Secondary Setup Menu DIAG
APPENDIX A-1 M102E Software Menu Trees, Revision A.2
05515 Rev A.2
APPENDIX A-2 Setup Variables For Serial I/O, Revision A.2
Deleted Setup Variables for M102E Software Revision A.2
Table A-2
Table A-4 Warning Messages deleted from M102 Software Revision A.2
setting of STABILFREQ and STABILSAMPLES
M102E/M501 TRS
APPENDIX A-3 Warnings and Test Functions, Revision A.2
05515 Rev A.2
APPENDIX A-4 M102E Signal I/O Definitions, Revision A.2
APPENDIX A-4 M102E Signal I/O Definitions, Revision A.2M102E/M501 TRS
Rear board primary MUX analog inputs
05515 Rev A.2
User Notes
M102E/M501 TRS
APPENDIX A-5 M102E iDAS Functions, Revision A.2
APPENDIX A-5 M102E iDAS Functions, Revision A.2
M102E/M501 TRS
A-10
05515 Rev A.2
M102E/M501 TRS
APPENDIX B - M102E Spare Parts List
APPENDIX B - M102E Spare Parts List
Table B-1 M102E Spare Parts List
Addendum to M101E Manual - P/N 04740 Rev A
APPENDIX B - M102E Spare Parts List
M102E/M501 TRS
05516 Rev A
INSTRUMENTS
Warranty/Repair Questionnaire Model 102E
M102E/M501 TRS
TELEDYNE
INSTRUMENTS
Warranty/Repair Questionnaire Model 102E
M102E/M501 TRS
TELEDYNE
USER NOTES
APPENDIX D - ELECTRONIC SCHEMATICS
APPENDIX D - ELECTRONIC SCHEMATICS
Table D-1 List of Included Electronic Schematics
05518 Rev A
APPENDIX D - ELECTRONIC SCHEMATICS
User Notes
M102E/M501 TRS