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Agilent Technologies G6600-90006 manual Operation and Maintenance Manual

Models: G6600-90006

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Troubleshooting Specs Install Schematic for 355 SCD Signal Controls Warranty Maintenance Solving Detector Problems Set Up the Vacuum Pump Burner Assembly Detail

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16	Operation and Maintenance Manual

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Agilent Technologies G6600-90006 manual Operation and Maintenance Manual

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Contents

Operation and Maintenance Manual Warranty Safety NoticesAcknowledgements Manual Part Number English WA R N I N G Is not in use Español Français Deutsch Italiano Dutch Veiligheidsvoorzieningen niet meer Following symbols are used on the equipment Contents Installation Overview Front Panel Controls and Initial Startup Operation Maintenance Pump Maintenance Troubleshooting Index Operation and Maintenance Manual Introduction Operation and Maintenance Manual System Description Technical Information 355 SCD SpecificationsTechnical Information 255 NCD Physical Specifications Power requirements Voltage Sulfur Chemiluminescence Detector Theory of OperationNitrogen Chemiluminescence Detector Dual Plasma Controller Dual Plasma Burner with the 355 SCD Description of Major Components Dual Plasma Burner Cross-Section of the Dual Plasma Burner for the 355 SCD Cross-Section of the Dual Plasma Burner for the 255 NCD Ozone Generator Chemiluminescence Reaction Cell and Photomultiplier Tube 355 SCD Left Side 355 SCD Right Side 255 NCD Left Side View Pressure Transducer Vacuum Pump Chemical Trap Oil Coalescing FilterFID Adapter Optional NCD Reaction Cell NCD Photomultiplier Tube and Cooler Schematic for 355 SCD Schematic for 255 NCD, in Nitrogen Mode Schematic for 255 NCD, in Nitrosamine Mode Operation and Maintenance Manual Installation Overview Power Requirements Selecting a Location Environmental Considerations Combustion Gas Requirements Two-stage pressure regulators Venting Gases Required Installation Tools Unpack and Inspect the Instrument Set Up the Vacuum Pump Installing the Edwards RV5 Pump Oil-Sealed Vacuum Pump WA R N I N G Ard RV5 Oil-Sealed Vacuum Pump and Associated Traps Front Side RV5 Oil- Sealed Vacuum Pump and Associated Traps Top Setting the Gas Ballast Position RV5 Installing the Welch Dry Piston Vacuum Pump Operation Notes Welch Pump Welch Dry Piston Pump Operation and Maintenance Manual Connect the Power Cord SCD 230 V Unit Rear Panel Diagram Install the Dry Compressed Air or O2 Supply Install the Signal Output Cables Install the Dual Plasma Burner Additional information Install the Dual Plasma Controller Dual Plasma Controller Rear Panel Capillary Columns Install Column ConnectionsPacked Columns and Columns with an Outside Diameter 0.8 mm Install the Transfer Line Front Panel Controls and Initial Startup Power Controls Detector Front Panel Controls Signal Controls Display Output Controls Dual Plasma Controller Controls Dual Plasma Controller Front Panel Initial Startup Vacuum Test Recorder Test Detector Interface Setup Initial Checkout Ignition Operation Start-Up Procedure Detector Operation Detector Stability and ResponseColumn Bleed Coking Contaminated Gases Fluctuating Pressures Typical Operating Conditions Typical Operating Conditions Detection Limits Expected Detection Limits for Chromatographic Conditions Daily Shutdown Instrument Shut-DownComplete Shutdown Using the 255 NCD in Nitrosamine Mode Special Operating Modes Operation and Maintenance Manual Operation and Maintenance Manual Maintenance Pump Maintenance Operating Life of Components for Edwards RV5 Vacuum Pump Cleaning the Detector Changing the Oil Mist Filter RV5 Reaction Cell Cleaning Equipment Reaction Cell, PMT Housing and PMT Socket WA R N I N G Flow Sensor Calibration Detector Sensitivity MDL SCD Proper Ferrule Orientation to the Large Ceramic Tube Orientation of the Double Taper Ferrule Tightening the Heater Swivel Nut Operation and Maintenance Manual NCD Proper Ferrule Orientation to the Large Quartz Tube Burner Assembly Detail Tube Replacement for the SCD Positioning the Upper Tube in the Union Fitting 100 Operation and Maintenance Manual Operation and Maintenance Manual 101 Tube Replacement for the NCD Operation and Maintenance Manual 103 NCD Tube Replacement Detail Troubleshooting Solving Detector Problems Power Problems Detector FuseVacuum Pump Fuse Dual Plasma Controller Fuses Fuse Positions on the Power Supply Board Ozone Generation Problems High Voltage Transformer Plugged Restrictor Lines Response Problems Temperature Reading Problems Diagnosing General Problems Troubleshooting Detector Issues Detector gases Troubleshooting Pump Issues Troubleshooting Burner Issues Index Agilent Technologies, Inc

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