Agilent Technologies G6600-90006 manual Initial Startup, Vacuum Test

Models: G6600-90006

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Controller Status

Illuminate to reflect current status. The Power LED

Lights

indicates power is on; the Heater LED indicates

 

temperature set point has been obtained; the Valves

 

LED indicates the solenoid valves open; and the

 

Fault LED indicates a drop in pressure or excessive

 

temperature (see Chapter 7, “Troubleshooting” for

 

details).

Initial Startup

Vacuum Test

With the 1/8" Valco cap on the black PFA transfer line still in place and the air supply to the ozone generator off, set the internal air regulator to 0 psi (fully counterclockwise), and power on the SCD or NCD by plugging the power cord into the house power supply. The SCD and NCD will power up in STANDBY mode, with the pump and the ozone generator OFF. For this test, the desired mode is power ON, vacuum pump ON, ozone generator OFF, display range in the low sensitivity mode and PRESSURE signal displayed. Press the following controls in the order shown in order to start the vacuum pump and to view the reaction cell pressure.

Press until green ON LED is lit

Press until red LED is lit

Press to display reaction cell pressure in torr

After the pressure has stabilized (~5 minutes), record the pressure below. Typical pressure in the reaction cell should be 1-2 torr with the oil-sealed pump, or 5-8 torr for the oil-free pump.

Operation and Maintenance Manual

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Page 67
Image 67
Agilent Technologies G6600-90006 manual Initial Startup, Vacuum Test