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G6600-90006 manual Operation and Maintenance Manual
Models:
G6600-90006
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Troubleshooting
Specs
Install
Schematic for 355 SCD
Tube Replacement for the SCD
Warranty
Maintenance
Solving Detector Problems
Set Up the Vacuum Pump
Burner Assembly Detail
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Agilent 355 Sulfur and 255 Nitrogen Chemiluminescence Detectors
Operation and Maintenance
Manual
Agilent Technologies
Page 2
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Contents
Operation and Maintenance Manual
Safety Notices
Warranty
Acknowledgements
Manual Part Number
WA R N I N G
English
Is not in use
Español
Français
Deutsch
Italiano
Veiligheidsvoorzieningen niet meer
Dutch
Following symbols are used on the equipment
Contents
Overview
Installation
Operation
Front Panel Controls and Initial Startup
Pump Maintenance
Maintenance
Index
Troubleshooting
Operation and Maintenance Manual
Introduction
Operation and Maintenance Manual
System Description
Technical Information 355 SCD
Specifications
Technical Information 255 NCD
Power requirements
Physical Specifications
Voltage
Sulfur Chemiluminescence Detector
Theory of Operation
Nitrogen Chemiluminescence Detector
Dual Plasma Burner with the 355 SCD
Dual Plasma Controller
Dual Plasma Burner
Description of Major Components
Cross-Section of the Dual Plasma Burner for the 355 SCD
Cross-Section of the Dual Plasma Burner for the 255 NCD
Chemiluminescence Reaction Cell and Photomultiplier Tube
Ozone Generator
355 SCD Left Side
355 SCD Right Side
255 NCD Left Side View
Vacuum Pump
Pressure Transducer
Oil Coalescing Filter
Chemical Trap
FID Adapter Optional
NCD Reaction Cell
NCD Photomultiplier Tube and Cooler
Schematic for 355 SCD
Schematic for 255 NCD, in Nitrogen Mode
Schematic for 255 NCD, in Nitrosamine Mode
Operation and Maintenance Manual
Installation
Overview
Selecting a Location
Power Requirements
Combustion Gas Requirements
Environmental Considerations
Two-stage pressure regulators
Venting Gases
Unpack and Inspect the Instrument
Required Installation Tools
Installing the Edwards RV5 Pump Oil-Sealed Vacuum Pump
Set Up the Vacuum Pump
WA R N I N G
Ard
RV5 Oil-Sealed Vacuum Pump and Associated Traps Front Side
RV5 Oil- Sealed Vacuum Pump and Associated Traps Top
Setting the Gas Ballast Position RV5
Installing the Welch Dry Piston Vacuum Pump
Operation Notes Welch Pump
Welch Dry Piston Pump
Operation and Maintenance Manual
SCD 230 V Unit Rear Panel Diagram
Connect the Power Cord
Install the Dry Compressed Air or O2 Supply
Install the Signal Output Cables
Additional information
Install the Dual Plasma Burner
Dual Plasma Controller Rear Panel
Install the Dual Plasma Controller
Capillary Columns
Install Column Connections
Packed Columns and Columns with an Outside Diameter 0.8 mm
Install the Transfer Line
Front Panel Controls and Initial Startup
Detector Front Panel Controls
Power Controls
Display Output Controls
Signal Controls
Dual Plasma Controller Front Panel
Dual Plasma Controller Controls
Vacuum Test
Initial Startup
Recorder Test
Initial Checkout
Detector Interface Setup
Ignition
Operation
Start-Up Procedure
Detector Stability and Response
Detector Operation
Column Bleed
Coking
Fluctuating Pressures
Contaminated Gases
Typical Operating Conditions
Typical Operating Conditions
Expected Detection Limits for Chromatographic Conditions
Detection Limits
Daily Shutdown
Instrument Shut-Down
Complete Shutdown
Special Operating Modes
Using the 255 NCD in Nitrosamine Mode
Operation and Maintenance Manual
Operation and Maintenance Manual
Maintenance
Operating Life of Components for Edwards RV5 Vacuum Pump
Pump Maintenance
Cleaning the Detector
Changing the Oil Mist Filter RV5
Equipment
Reaction Cell Cleaning
Reaction Cell, PMT Housing and PMT Socket
WA R N I N G
Flow Sensor Calibration
MDL
Detector Sensitivity
SCD
Proper Ferrule Orientation to the Large Ceramic Tube
Orientation of the Double Taper Ferrule
Tightening the Heater Swivel Nut
Operation and Maintenance Manual
NCD
Proper Ferrule Orientation to the Large Quartz Tube
Burner Assembly Detail
Tube Replacement for the SCD
Positioning the Upper Tube in the Union Fitting
100 Operation and Maintenance Manual
Operation and Maintenance Manual 101
Tube Replacement for the NCD
Operation and Maintenance Manual 103
NCD Tube Replacement Detail
Troubleshooting
Solving Detector Problems
Detector Fuse
Power Problems
Vacuum Pump Fuse
Dual Plasma Controller Fuses
Fuse Positions on the Power Supply Board
High Voltage Transformer
Ozone Generation Problems
Plugged Restrictor Lines
Response Problems
Temperature Reading Problems
Troubleshooting Detector Issues
Diagnosing General Problems
Detector gases
Troubleshooting Pump Issues
Troubleshooting Burner Issues
Index
Agilent Technologies, Inc
