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Agilent Technologies G6600-90006 manual Operation and Maintenance Manual

Models: G6600-90006

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Troubleshooting Specs Install Schematic for 355 SCD Signal Controls Warranty Maintenance Solving Detector Problems Set Up the Vacuum Pump Burner Assembly Detail

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Agilent 355 Sulfur and 255 Nitrogen Chemiluminescence Detectors

Operation and Maintenance

Manual

Agilent Technologies

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Agilent Technologies G6600-90006 manual Operation and Maintenance Manual

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Contents

Operation and Maintenance Manual Safety Notices WarrantyAcknowledgements Manual Part Number WA R N I N G English Is not in use Español Français Deutsch Italiano Veiligheidsvoorzieningen niet meer Dutch Following symbols are used on the equipment Contents Overview Installation Operation Front Panel Controls and Initial Startup Pump Maintenance Maintenance Index Troubleshooting Operation and Maintenance Manual Introduction Operation and Maintenance Manual System Description Technical Information 355 SCD SpecificationsTechnical Information 255 NCD Power requirements Physical Specifications Voltage Sulfur Chemiluminescence Detector Theory of OperationNitrogen Chemiluminescence Detector Dual Plasma Burner with the 355 SCD Dual Plasma Controller Dual Plasma Burner Description of Major Components Cross-Section of the Dual Plasma Burner for the 355 SCD Cross-Section of the Dual Plasma Burner for the 255 NCD Chemiluminescence Reaction Cell and Photomultiplier Tube Ozone Generator 355 SCD Left Side 355 SCD Right Side 255 NCD Left Side View Vacuum Pump Pressure Transducer Oil Coalescing Filter Chemical TrapFID Adapter Optional NCD Reaction Cell NCD Photomultiplier Tube and Cooler Schematic for 355 SCD Schematic for 255 NCD, in Nitrogen Mode Schematic for 255 NCD, in Nitrosamine Mode Operation and Maintenance Manual Installation Overview Selecting a Location Power Requirements Combustion Gas Requirements Environmental Considerations Two-stage pressure regulators Venting Gases Unpack and Inspect the Instrument Required Installation Tools Installing the Edwards RV5 Pump Oil-Sealed Vacuum Pump Set Up the Vacuum Pump WA R N I N G Ard RV5 Oil-Sealed Vacuum Pump and Associated Traps Front Side RV5 Oil- Sealed Vacuum Pump and Associated Traps Top Setting the Gas Ballast Position RV5 Installing the Welch Dry Piston Vacuum Pump Operation Notes Welch Pump Welch Dry Piston Pump Operation and Maintenance Manual SCD 230 V Unit Rear Panel Diagram Connect the Power Cord Install the Dry Compressed Air or O2 Supply Install the Signal Output Cables Additional information Install the Dual Plasma Burner Dual Plasma Controller Rear Panel Install the Dual Plasma Controller Capillary Columns Install Column ConnectionsPacked Columns and Columns with an Outside Diameter 0.8 mm Install the Transfer Line Front Panel Controls and Initial Startup Detector Front Panel Controls Power Controls Display Output Controls Signal Controls Dual Plasma Controller Front Panel Dual Plasma Controller Controls Vacuum Test Initial Startup Recorder Test Initial Checkout Detector Interface Setup Ignition Operation Start-Up Procedure Detector Stability and Response Detector OperationColumn Bleed Coking Fluctuating Pressures Contaminated Gases Typical Operating Conditions Typical Operating Conditions Expected Detection Limits for Chromatographic Conditions Detection Limits Daily Shutdown Instrument Shut-DownComplete Shutdown Special Operating Modes Using the 255 NCD in Nitrosamine Mode Operation and Maintenance Manual Operation and Maintenance Manual Maintenance Operating Life of Components for Edwards RV5 Vacuum Pump Pump Maintenance Cleaning the Detector Changing the Oil Mist Filter RV5 Equipment Reaction Cell Cleaning Reaction Cell, PMT Housing and PMT Socket WA R N I N G Flow Sensor Calibration MDL Detector Sensitivity SCD Proper Ferrule Orientation to the Large Ceramic Tube Orientation of the Double Taper Ferrule Tightening the Heater Swivel Nut Operation and Maintenance Manual NCD Proper Ferrule Orientation to the Large Quartz Tube Burner Assembly Detail Tube Replacement for the SCD Positioning the Upper Tube in the Union Fitting 100 Operation and Maintenance Manual Operation and Maintenance Manual 101 Tube Replacement for the NCD Operation and Maintenance Manual 103 NCD Tube Replacement Detail Troubleshooting Solving Detector Problems Detector Fuse Power ProblemsVacuum Pump Fuse Dual Plasma Controller Fuses Fuse Positions on the Power Supply Board High Voltage Transformer Ozone Generation Problems Plugged Restrictor Lines Response Problems Temperature Reading Problems Troubleshooting Detector Issues Diagnosing General Problems Detector gases Troubleshooting Pump Issues Troubleshooting Burner Issues Index Agilent Technologies, Inc

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