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G6600-90006 manual Agilent Technologies, Inc
Models:
G6600-90006
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Troubleshooting
Specs
Install
Schematic for 355 SCD
Tube Replacement for the SCD
Warranty
Maintenance
Solving Detector Problems
Set Up the Vacuum Pump
Burner Assembly Detail
Page 118
Image 118
Agilent Technologies
© Agilent Technologies, Inc.
Printed in USA, June 2007
Page 117
Page 118
Image 118
Page 117
Contents
Operation and Maintenance Manual
Acknowledgements
Warranty
Safety Notices
Manual Part Number
English
WA R N I N G
Is not in use
Español
Français
Deutsch
Italiano
Dutch
Veiligheidsvoorzieningen niet meer
Following symbols are used on the equipment
Contents
Installation
Overview
Front Panel Controls and Initial Startup
Operation
Maintenance
Pump Maintenance
Troubleshooting
Index
Operation and Maintenance Manual
Introduction
Operation and Maintenance Manual
System Description
Technical Information 355 SCD
Specifications
Technical Information 255 NCD
Physical Specifications
Power requirements
Voltage
Sulfur Chemiluminescence Detector
Theory of Operation
Nitrogen Chemiluminescence Detector
Dual Plasma Controller
Dual Plasma Burner with the 355 SCD
Description of Major Components
Dual Plasma Burner
Cross-Section of the Dual Plasma Burner for the 355 SCD
Cross-Section of the Dual Plasma Burner for the 255 NCD
Ozone Generator
Chemiluminescence Reaction Cell and Photomultiplier Tube
355 SCD Left Side
355 SCD Right Side
255 NCD Left Side View
Pressure Transducer
Vacuum Pump
FID Adapter Optional
Chemical Trap
Oil Coalescing Filter
NCD Reaction Cell
NCD Photomultiplier Tube and Cooler
Schematic for 355 SCD
Schematic for 255 NCD, in Nitrogen Mode
Schematic for 255 NCD, in Nitrosamine Mode
Operation and Maintenance Manual
Installation
Overview
Power Requirements
Selecting a Location
Environmental Considerations
Combustion Gas Requirements
Two-stage pressure regulators
Venting Gases
Required Installation Tools
Unpack and Inspect the Instrument
Set Up the Vacuum Pump
Installing the Edwards RV5 Pump Oil-Sealed Vacuum Pump
WA R N I N G
Ard
RV5 Oil-Sealed Vacuum Pump and Associated Traps Front Side
RV5 Oil- Sealed Vacuum Pump and Associated Traps Top
Setting the Gas Ballast Position RV5
Installing the Welch Dry Piston Vacuum Pump
Operation Notes Welch Pump
Welch Dry Piston Pump
Operation and Maintenance Manual
Connect the Power Cord
SCD 230 V Unit Rear Panel Diagram
Install the Dry Compressed Air or O2 Supply
Install the Signal Output Cables
Install the Dual Plasma Burner
Additional information
Install the Dual Plasma Controller
Dual Plasma Controller Rear Panel
Capillary Columns
Install Column Connections
Packed Columns and Columns with an Outside Diameter 0.8 mm
Install the Transfer Line
Front Panel Controls and Initial Startup
Power Controls
Detector Front Panel Controls
Signal Controls
Display Output Controls
Dual Plasma Controller Controls
Dual Plasma Controller Front Panel
Initial Startup
Vacuum Test
Recorder Test
Detector Interface Setup
Initial Checkout
Ignition
Operation
Start-Up Procedure
Column Bleed
Detector Operation
Detector Stability and Response
Coking
Contaminated Gases
Fluctuating Pressures
Typical Operating Conditions
Typical Operating Conditions
Detection Limits
Expected Detection Limits for Chromatographic Conditions
Daily Shutdown
Instrument Shut-Down
Complete Shutdown
Using the 255 NCD in Nitrosamine Mode
Special Operating Modes
Operation and Maintenance Manual
Operation and Maintenance Manual
Maintenance
Pump Maintenance
Operating Life of Components for Edwards RV5 Vacuum Pump
Cleaning the Detector
Changing the Oil Mist Filter RV5
Reaction Cell Cleaning
Equipment
Reaction Cell, PMT Housing and PMT Socket
WA R N I N G
Flow Sensor Calibration
Detector Sensitivity
MDL
SCD
Proper Ferrule Orientation to the Large Ceramic Tube
Orientation of the Double Taper Ferrule
Tightening the Heater Swivel Nut
Operation and Maintenance Manual
NCD
Proper Ferrule Orientation to the Large Quartz Tube
Burner Assembly Detail
Tube Replacement for the SCD
Positioning the Upper Tube in the Union Fitting
100 Operation and Maintenance Manual
Operation and Maintenance Manual 101
Tube Replacement for the NCD
Operation and Maintenance Manual 103
NCD Tube Replacement Detail
Troubleshooting
Solving Detector Problems
Vacuum Pump Fuse
Power Problems
Detector Fuse
Dual Plasma Controller Fuses
Fuse Positions on the Power Supply Board
Ozone Generation Problems
High Voltage Transformer
Plugged Restrictor Lines
Response Problems
Temperature Reading Problems
Diagnosing General Problems
Troubleshooting Detector Issues
Detector gases
Troubleshooting Pump Issues
Troubleshooting Burner Issues
Index
Agilent Technologies, Inc
