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Gilson 402 manual Chemical Compatibility, Appendix B, Materials in Contact with Liquids

Models: 402

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Chemical Compatibility

Chemical Compatibility		Appendix B

Chemical Compatibility

Chemical Compatibility

Materials in Contact with Liquids

In the 402 Dilutor Dispenser flow-path, several materials are in contact with liquids:

FEP	Inlet tubing, Transfer tubing
PTFE/Ekonol	Piston nose of the syringes (except 25 mL)
PTFE	Piston nose of the 25 mL syringe
Borosilicate glass	Syringe
Ceramic	Valve
PEEK	Valve, Tee junction

Compatibility

The syringe assemblies and the tubings are compatible with a wide range of liquids:

Acetic acid (glacial)		Ethyl acetate
Acetone		Ethylene glycol
Acetonitrile		Hexane
Ammonium hydroxide		Hydrochloric acid - 37%
Benzene		Isooctane
Benzyl alcohol		Methanol
Boric acid		Nitric acid - 50%
Butanol		Propanol
Carbon tetrachloride		Sodium hydroxide - 30%
Chlorobenzene		Sodium hypochlorite -10%
Chloroform		Sulfuric acid - 96%
Cyclohexane		Toluene
Cyclohexanone		Trichloroethane
Dichloroethane		Trichloroethylene
Dichlorobenzene		Tetrahydrofuran
Diethyl ether		Toluene
Dimethylformamide		Xylene
Ethanol
Ethanol

Appendix B-2

Image 108

Gilson 402 manual Chemical Compatibility, Appendix B, Materials in Contact with Liquids

Contents

402 Dilutor Dispenser User’s Guide Page 402 Dilutor Dispenser User’s Guide LT801310/C - 2003 Gilson SAS All rights reservedNovember Page Table of Contents Safety3 Installation 1 IntroductionMaintenance Operation - Standard UseOperation - Advanced Use Table of Contents-27 Troubleshooting AppendicesIndex 402 Dual Syringe with Tee Junction ConfigPage Safety Safety-1Safety Introduction1 Notational Conventions IntroductionNotational Conventions Overview OverviewIntroduction checking protocol for the hydraulic specifica- tions IQ/OQ procedures IntroductionOverview Good Laboratory Practice GLP is facilitated by the followingUnpacking UnpackingIntroduction Warranty WarrantyIntroduction Customer Service Customer ServiceIntroduction Introduction Description2 Single-syringeModel Description2Front Panel Rear PanelDual-syringe Model DescriptionDual-syringe Model Front PanelKeypad and Probe KeypadProbe Keypad and ProbeHydraulic Components ValveTee Junction SyringesDescription2 Hydraulic ComponentsThere are seven syringe sizes available for the Installation3 Installation Assembling the ProbeFor Standard Use Adapter Kit for Disposable TipsInstallation Assembling the Probe2 Special adapters for the probe 1 D200 tips, pack of Connecting the Tubing Connecting the TubingSingle-syringe Model Valve Inlet TubingConnecting the Dual-syringe ModelTubing Valve Waste TubingInstallation Connecting the Tubing1 mL, 5 mL, and 10 mL are available as additional accessories Installing the Fuses Electrical ConnectionsSector Block Voltage SelectorConnecting the Power Cord Connecting the KeypadConnecting the Probe InstallationSyringes Assembling a SyringeFitting a Syringe InstallationUpgrading to Dual-syringe Model Upgrading to Dual-syringe ModelInstallation Installation Removing the Cover Connecting the Flat CableUpgrading to Dual-syringe Model Inserting the Module Installation3 Secure the module in place at the top using the two screws provided Upgrading to Dual-syringe ModelOperation - Standard Use Fit the Fuses and Connect the Power Essential StepsOperation - Standard Use Standard PartsSwitch-on Initialization Screen Initialization Screen Homing ScreenStart-up Screen Operation - Standard UseConfiguration Conf VolumesConfiguration Screen Tubing Volume Screen Air Gap Volume Screen Operation - Standard UseConfiguration Screen SyringesFlow Rates Operation - Standard UseOther Items Resv Flow Screen Prime Flow Screen Beeper Screen Autorefill ScreenOperation - Standard Use Essential StepsConfiguration Screen Syringe Screen Counter Screen Fit the SyringesCreating a Method Edit IntroductionIn-run Prompts Method ExampleStart-up Screen Task Selection Screen Entering the MethodPress ESC, Dispense Screen 7 appears Dispense Screen Dispense Screen Dispense Screen Dispense Screen 4aDispense Screen 4b Dispense Screen Dispense Screen Dispense Screen Task Selection Screen Rinse Screen Task Edit Screen Save ScreenPrime the 402 Man Pressing EndPressing STOP Manipulation Screen Initialization Screen Abort ScreenRunning a Method Run Run Screen Run Screen Abort ScreenOperation - Standard Use Essential StepsIn Run Screen In Run Screen 2a In Run Screen 2b Operation - Standard UseEssential Steps Method ExampleIn Run Screen 3b In Run Screen 4b In Run Screen 5b In Run Screen 6b Abort ScreenOperation - Standard Use Essential StepsOperation - Standard Use Essential StepsOperation - Advanced Use Correct Use of a Operation - Advanced UseCorrect Use of the Liquids should be separated by an air gap to minimize contaminationLeft-hand Syringe Aspirating from Reservoir Left-hand Syringe Dispensing from ReservoirOperation - Advanced Use Correct Use of theAspirating Large Volumes via the Probe Aspirating Small Volumes via the ProbeRight-hand Syringe Dispensing to ProbeSoftware SoftwareOperation - Advanced Use Entering the Configuration CONF Tubing Volume ScreenVolumes Configuration ScreenSyringe Screen Change SizeOperation - Advanced Use SoftwareSyringe Correction Screen Air Flow Screen Resv Flow Screen Prime Flow ScreenCorrection Factor Operation - Advanced Usereturn to the Configuration Screen Creating a Method EDITCounters press Count, the Syringe Counter Screen appearsSaving a Method File Manipulations FILEDelete a File Syringe Correction Screen Save Screen File Menu ScreenCopy a File File DirectoryLock or Unlock a File New File ScreenDirect Manipulations MAN PrimeLocked File Screen Action Screen Initialization Screen Abort Screen Operation - Advanced UseMeasure Measure Screen Flow Rate ScreenOperation - Advanced Use SoftwareProcedure TitrateMeasurement Screen Operation - Advanced UseTasks - Detailed Descriptions Titrate Screen Titrate Screen Titrate Screen Titrate ScreenOperation - Advanced Use SoftwareKeys ParametersOperation - Advanced Use SoftwareChaining Tasks Operation - Advanced UseSoftware ParameterDilute ScreensDilute Normal Typical Task EntryENTER NextREAG Dilute SeriallyOperation - Advanced Use SoftwareTypical Task Entry ScreensDilute Unknown Typical Task EntryOperation - Advanced Use SoftwareRun Procedure Operation - Advanced UseSoftware Dispense Operation - Advanced UseSoftware Operation - Advanced Use SoftwareTypical Task Entry Pipette Operation - Advanced UseSoftware Key to pressRinse ExtraOperation - Advanced Use SoftwareLink What it DoesExample Operation - Advanced UseConfiguration Prefabricated MethodsKey to Press Edit More Link File # 7 ENTER Next File # 8 ENTERRunning a Method RUN Operation - Advanced UseSoftware In-run PromptsWhen you have finished, or wish to change programs, press STOP, to instantly halt the program. Alterna- tively, you can bring the 402 to a halt by switching off the power, in which case you must ensure that the probe end of transfer-tubing is in a suitable waste container before switching on again Operation - Advanced UseSoftware Pressing STOPIn Configuration Additional InformationFlow Rates Additional InformationFlow Rates - Dual-syringe Model Operation - Advanced UseAdditional Information ExampleOperation - Advanced Use Syringe Correction Function Use of Disposable TipsAir Mode Additional InformationLiquid Mode Operation - Advanced UseAdditional Information Maintenance6 The only maintenance operations necessary for the 402 DD areCleaning the exterior of the instrument Cleaning of the valve, Tee, syringe assemblies and the tubingsCleaning MaintenanceCleaning the Exterior Cleaning the ValveCleaning the Tee Junction MaintenanceCleaning 1 Pull the axle away from the valve main bodyCleaning the Syringe Assembly MaintenanceCleaning 1 Dismount the Syringe assembly from the instrumentAutoclaving Autoclaving the TubingAutoclaving MaintenanceChanging the Syringe Piston Assembly Chaning the Syringe Piston AssemblyReplacing the Piston MaintenanceChanging the Piston Syringes and Piston Noses Changing the 100 and 250 µL Piston NosesChanging the Piston Syringes and Piston Noses MaintenanceNoses Changing the PistonMaintenance PistonChanging the 500 µL Piston Noses Changing the Syringe Piston and Piston NosesMaintenance Syringe body Changing the 1 mL Piston Noses Piston NosesChanging the Piston Syringes MaintenanceChanging the 25 mL Piston Noses Changing the 5 mL and 10 mL Piston NosesMaintenance Changing the Syringe Piston and Piston NosesMaintenance Changing the Piston Syringes and Piston NosesTroubleshooting7 Mechanical Problems TroubleshootingMechanical Problems Hydraulic Problems Hydraulic ProblemsTroubleshooting Electrical Problems Electrical ProblemsTroubleshooting Parts & Accessories Lists Appendix A Appendix A-1Parts & Accessories Lists 402 Single SyringeAppendix A 402 Single Syringe402 Dual Syringe with Tee Junction Configuration 402 Dual Syringe with Tee Junction ConfigurationParts & Accessories Lists Appendix AAdditionalAccessories AdditionalAccessoriesParts & Accessories Lists Appendix ASpare Parts Spare PartsParts & Accessories Lists Appendix AParts & Accessories Lists Appendix AAppendix A-6 Chemical Compatibility Appendix B Appendix B-1Chemical Compatibility Chemical CompatibilityAppendix B Materials in Contact with LiquidsTechnical Data Appendix CTechnical Data Minimum VolumeMaximum Volume HydraulicsPerformance Specifications ProtocolTechnical Data Appendix CJunction Tubing Technical DataSee OQ Document for procedure and calculations Appendix CMechanics MechanicsTechnical Data ValvePower Requirements Size and WeightEnvironmental Conformity to NormsError Messages Appendix DError Messages Error MessagesError Messages Appendix DError Messages Error MessagesAppendix D Appendix D-3Error Messages Appendix DAppendix D-4 Index Index-1Index Index-2Index Index-3Index Index-4Page E-mail sales@gilson.com, service@gilson.com, training@gilson.com World HeadquartersGilson, Inc Gilson SAS