Test Sample Chromatograms
Test sample chromatograms
Figure
HP 5890 Test Sample Operating
Conditions
Detector Type TCD(or TCDw/MUG) | FLOW RATES |
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| Temp 300 DEGREES C | Carrier (He) | 20 +/• 1 | ml/min | |||||||
Inlet Type PACKED (OR PURGED | Hydrogen | N/A | ml/min | ||||||||
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| PACKED). |
| Air |
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| N/A | ml/min | |||
| Temp 250 DEGREES C | Makeup (He) | 1•2 | ml/min | |||||||
Operating Mode |
| N/A |
| Split Vent | N/A | ml/min | |||||
Purge Time On |
| N/A | min | Septum Purge | 1•2 | ml/min | |||||
Purge Time Off |
| N/A | min | Reference (He) 30+/•1 | ml/min | ||||||
Oven Temp Programmed (1 ramp) |
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Init Temp | 110 | DEGREES C |
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Init Time | 1 | min |
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Ramp |
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| SAMPLE: |
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Rate |
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| 15 |
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Fin Temp |
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| 150 |
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| Type |
| FID Sample |
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Fin Time |
| 1 |
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| Inj Volume | 3 ¿l |
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Range | 0 |
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| Part No. 18710•60170 |
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| Composition 0.03%(V/V)each |
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COLUMN: |
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| C14,C15,C16 normal paraffin | ||||
Part No. |
| 19095S(#100) | hydrocarbons in hexane |
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Dimensions |
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| 530¿ MID; 5 M |
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Sta Phase | Methyl Silicone |
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| START |
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| .25 |
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| 2.42 | C14 |
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| 3.38 |
| C15 |
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| 3.76 | C16 |
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| ST |
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Thermal Conductivity Detector (TCD)
228